Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 1000510
Preview
| Coordinates | 1000510.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | Methyl (4R*,4aS*,8aS*)-8a-t-butyldimethylsiloxy-4-phenyl-4a,5,6,7,8,8a-hexahydro-4H-chromene-2-carboxylate |
|---|---|
| Formula | C23 H34 O4 Si |
| Calculated formula | C23 H34 O4 Si |
| Title of publication | Lewis Acid Catalysed [4+2] Heterocycloadditions between Ketone Enol Ethers and β-Ethylenic α-Oxo Esters |
| Authors of publication | Martel, A.; Leconte, S.; Dujardin, G.; Brown, E.; Maisonneuve, V.; Retoux, R. |
| Journal of publication | European Journal of Organic Chemistry |
| Year of publication | 2002 |
| Journal volume | 2002 |
| Journal issue | 3 |
| Pages of publication | 514 - 525 |
| a | 9.4586 ± 0.0017 Å |
| b | 11.1593 ± 0.0016 Å |
| c | 12.4892 ± 0.0015 Å |
| α | 89.406 ± 0.01° |
| β | 72.021 ± 0.013° |
| γ | 70.117 ± 0.011° |
| Cell volume | 1172.52 Å3 |
| Ambient diffraction temperature | 293 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for significantly intense reflections | 0.0822 |
| Weighted residual factors for significantly intense reflections | 0.0822 |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
Version history
Version history is temporarily not available due to server issues.
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.