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Information card for entry 1100255
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| Coordinates | 1100255.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | tetrakis(μ~3~-Tricyclohexylphosphoraneiminato)-tetra-potassium |
|---|---|
| Formula | C72 H132 K4 N4 P4 |
| Calculated formula | C77 H143 K4 N4 P4 |
| Title of publication | Phosphaniminate von Alkalimetallen: Die Kristallstrukturen von [KNPCy~3~]~4~, [KNPCy~3~]~4~·2OPCy~3~, [CsNPCy~3~]~4~·4OPCy~3~ und [Li~4~(NPPh~3~)(OSiMe~2~NPPh~3~)~3~(DME)] |
| Authors of publication | Gröb, Thorsten; Chitsaz, Soheila; Harms, Klaus; Dehnicke, Kurt |
| Journal of publication | Zeitschrift fuer Anorganische und Allgemeine Chemie |
| Year of publication | 2002 |
| Journal volume | 628 |
| Journal issue | 2 |
| Pages of publication | 473 - 479 |
| a | 13.8983 ± 0.001 Å |
| b | 14.0806 ± 0.001 Å |
| c | 22.052 ± 0.002 Å |
| α | 78.952 ± 0.01° |
| β | 81.215 ± 0.01° |
| γ | 66.232 ± 0.008° |
| Cell volume | 3862.57 Å3 |
| Ambient diffraction temperature | 193 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for significantly intense reflections | 4.18 |
| Weighted residual factors for significantly intense reflections | 4.18 |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
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