#------------------------------------------------------------------------------ #$Date: 2016-02-25 13:36:33 +0000 (Thu, 25 Feb 2016) $ #$Revision: 176973 $ #$URL: svn://www.crystallography.net/cod/cif/1/10/02/1100291.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1100291 loop_ _publ_author_name 'Marsch, Michael' 'Harms, Klaus' 'Massa, Werner' 'Boche, Gernot' _publ_section_title ; Crystal Structure of the \h^1^-Allyl-Grignard Compound Bis(allylmagnesium chloride-TMEDA) ; _journal_coden_ASTM ACIEAY _journal_issue 7 _journal_name_full ; Angewandte Chemie, International Edition in English ; _journal_page_first 696 _journal_page_last 697 _journal_paper_doi 10.1002/anie.198706961 _journal_volume 26 _journal_year 1987 _chemical_formula_sum 'C18 H42 Cl2 Mg2 N4' _symmetry_cell_setting monoclinic _symmetry_Int_Tables_number 14 _symmetry_space_group_name_H-M 'P 21/n' _cell_angle_alpha 90 _cell_angle_beta 92.58(1) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 8.445(1) _cell_length_b 11.020(1) _cell_length_c 13.504(1) _cod_database_code 1100291 loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z ? ? ? ?