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Information card for entry 1100871
Preview
| Coordinates | 1100871.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C35 H51 F12 N O2 P2 W |
|---|---|
| Calculated formula | C35 H51 F12 N O2 P2 W |
| Title of publication | Double Phosphaalkyne Insertion to a Tungsten Alkylidene: Formation of a Diphosphametallabicyclobutane |
| Authors of publication | Jamison, Gregory M.; Wheeler, David R.; Loy, Douglas A.; Ziller, Joseph W. |
| Journal of publication | Organometallics |
| Year of publication | 2005 |
| Journal volume | 24 |
| Journal issue | 10 |
| Pages of publication | 2245 - 2247 |
| a | 42.11 ± 0.005 Å |
| b | 10.6323 ± 0.0009 Å |
| c | 20.577 ± 0.002 Å |
| α | 90° |
| β | 117.67 ± 0.006° |
| γ | 90° |
| Cell volume | 8159.4 ± 1.4 Å3 |
| Cell temperature | 163 K |
| Ambient diffraction temperature | 163 K |
| Number of distinct elements | 7 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0467 |
| Residual factor for significantly intense reflections | 0.0317 |
| Weighted residual factors for all reflections | 0.0714 |
| Weighted residual factors for significantly intense reflections | 0.065 |
| Goodness-of-fit parameter for all reflections | 1.06 |
| Goodness-of-fit parameter for significantly intense reflections | 1.085 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
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Users of the data should acknowledge the original authors of the
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