#------------------------------------------------------------------------------ #$Date: 2026-06-25 23:46:09 +0100 (Thu, 25 Jun 2026) $ #$Revision: 306651 $ #$URL: svn://www.crystallography.net/cod/cif/1/57/74/1577437.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1577437 loop_ _publ_author_name 'Vashisth, Kanika' 'Thornton, Ragene' 'Yoon, Bohak' 'Martin, Caleb Daniel' _publ_section_title ; Bis(Carboranyl)boryl Anions ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D6SC03158G _journal_year 2026 _chemical_formula_moiety 'C36 H72 K2 O18, 2(C16 H30 B21)' _chemical_formula_sum 'C68 H132 B42 K2 O18' _chemical_formula_weight 1770.610 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_Int_Tables_number 2 _audit_block_doi 10.5517/ccdc.csd.cc2pb68j _audit_creation_date 2025-08-22 _audit_creation_method ; Olex2 1.5 (compiled 2024.01.12 svn.r2f8d729c for OlexSys, GUI svn.r6928) ; _audit_update_record ; 2025-11-20 deposited with the CCDC. 2026-06-19 downloaded from the CCDC. ; _cell_angle_alpha 64.822(2) _cell_angle_beta 76.409(2) _cell_angle_gamma 72.142(2) _cell_formula_units_Z 1 _cell_length_a 11.9698(8) _cell_length_b 14.6251(9) _cell_length_c 16.1758(11) _cell_measurement_reflns_used 5868 _cell_measurement_temperature 273(2) _cell_measurement_theta_max 25.44 _cell_measurement_theta_min 2.41 _cell_volume 2421.2(3) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 273.15 _diffrn_measured_fraction_theta_full 0.9993 _diffrn_measured_fraction_theta_max 0.9981 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1102 _diffrn_reflns_av_unetI/netI 0.0667 _diffrn_reflns_Laue_measured_fraction_full 0.9993 _diffrn_reflns_Laue_measured_fraction_max 0.9981 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 92154 _diffrn_reflns_point_group_measured_fraction_full 0.9993 _diffrn_reflns_point_group_measured_fraction_max 0.9981 _diffrn_reflns_theta_full 25.2417 _diffrn_reflns_theta_max 27.11 _diffrn_reflns_theta_min 2.14 _exptl_absorpt_coefficient_mu 0.158 _exptl_absorpt_correction_T_max 0.933 _exptl_absorpt_correction_T_min 0.918 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADabs _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.214 _exptl_crystal_description block _exptl_crystal_F_000 932.927 _exptl_crystal_size_max 0.216 _exptl_crystal_size_mid 0.112 _exptl_crystal_size_min 0.107 _refine_diff_density_max 0.5591 _refine_diff_density_min -0.4255 _refine_diff_density_rms 0.0927 _refine_ls_d_res_high 0.7799 _refine_ls_d_res_low 9.5008 _refine_ls_goodness_of_fit_ref 1.0362 _refine_ls_matrix_type full _refine_ls_number_constraints 94 _refine_ls_number_parameters 646 _refine_ls_number_reflns 10682 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.0362 _refine_ls_R_factor_all 0.1079 _refine_ls_R_factor_gt 0.0558 _refine_ls_shift/su_max 0.0008 _refine_ls_shift/su_mean 0.0001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0585P)^2^+1.3466P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1270 _refine_ls_wR_factor_ref 0.1585 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 15 _reflns_limit_h_min -14 _reflns_limit_k_max 18 _reflns_limit_k_min -16 _reflns_limit_l_max 20 _reflns_limit_l_min 0 _reflns_number_gt 6460 _reflns_number_total 10682 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL K-crown[1]_a.res in P-1 CELL 0.71073 11.9698 14.6251 16.1758 64.822 76.409 72.142 ZERR 1 0.0008 0.0009 0.0011 0.002 0.002 0.002 LATT 1 SFAC C H B K O UNIT 68 132 42 2 18 EQIV $1 -X,1-Y,-Z L.S. 16 PLAN -5 TEMP 0 HTAB C24 O8_$1 CONF ACTA BOND $H FMAP 2 HTAB MORE -1 OMIT 1 1 0 OMIT 1 1 1 WGHT 0.058521 1.34664 FVAR 0.146483 REM REM REM K1 4 0.13409 0.32727 0.22595 11.00000 0.03943 0.03268 0.03372 = -0.01343 -0.00416 -0.00862 O1 5 0.11191 0.28317 0.41839 11.00000 0.06075 0.05879 0.03945 = -0.02106 0.00263 -0.02747 O12 5 0.10754 0.54173 0.12824 11.00000 0.04177 0.03265 0.04245 = -0.01152 -0.00552 -0.00421 O8 5 -0.21050 0.39871 0.06245 11.00000 0.05449 0.02932 0.03896 = -0.01237 -0.00935 -0.00711 O7 5 -0.09083 0.45794 0.16061 11.00000 0.03970 0.03982 0.05458 = -0.02615 -0.00261 -0.00765 O5 5 0.35806 0.34793 0.12878 11.00000 0.04080 0.04977 0.04636 = -0.02011 0.00130 -0.00486 O4 5 0.20503 0.27405 0.07474 11.00000 0.07090 0.03150 0.03984 = -0.01570 -0.01312 -0.00029 O3 5 0.12687 0.12784 0.23700 11.00000 0.05954 0.03845 0.04559 = -0.01706 -0.01371 -0.01073 O2 5 -0.03361 0.21242 0.35651 11.00000 0.05589 0.04987 0.04387 = -0.01690 0.00074 -0.02131 O6 5 0.33436 0.30209 0.31737 11.00000 0.05390 0.03965 0.04667 = -0.01886 -0.01151 -0.01114 C6 1 0.67369 0.07534 0.46277 11.00000 0.07059 0.06735 0.06707 = -0.05163 -0.00384 -0.00343 AFIX 43 H6 2 0.68348 0.04015 0.42439 11.00000 -1.20000 AFIX 0 C7 1 0.68383 0.02049 0.55588 11.00000 0.06495 0.04495 0.06581 = -0.03513 -0.00330 -0.00523 AFIX 43 H7 2 0.70155 -0.05178 0.58019 11.00000 -1.20000 AFIX 0 C8 1 0.66738 0.07405 0.61246 11.00000 0.04624 0.03694 0.04409 = -0.02154 -0.00066 -0.00467 AFIX 43 H8 2 0.67575 0.03703 0.67461 11.00000 -1.20000 AFIX 0 C3 1 0.63873 0.18162 0.57821 11.00000 0.02815 0.03880 0.03420 = -0.01995 0.00387 -0.00738 C2 1 0.61755 0.23934 0.64056 11.00000 0.02633 0.02676 0.02982 = -0.01134 -0.00094 -0.00333 C1 1 0.47785 0.25951 0.70312 11.00000 0.02593 0.02611 0.02343 = -0.01093 0.00198 -0.00578 B1 3 0.37662 0.21981 0.68366 11.00000 0.03029 0.02478 0.02423 = -0.00947 -0.00091 -0.00795 AFIX 13 H1 2 0.40935 0.20007 0.63048 11.00000 -1.20000 AFIX 0 C16 1 0.25100 0.30357 0.66005 11.00000 0.03154 0.02735 0.02603 = -0.01280 -0.00295 -0.00709 C11 1 0.15250 0.26114 0.70444 11.00000 0.03077 0.02689 0.02828 = -0.01233 -0.00207 -0.00675 C12 1 0.03710 0.31548 0.68888 11.00000 0.02946 0.03730 0.03781 = -0.01575 -0.00205 -0.00990 AFIX 43 H12 2 -0.02559 0.28398 0.71977 11.00000 -1.20000 AFIX 0 C13 1 0.01706 0.41733 0.62658 11.00000 0.02977 0.03610 0.04171 = -0.01542 -0.01143 0.00015 AFIX 43 H13 2 -0.05966 0.45544 0.61544 11.00000 -1.20000 AFIX 0 C4 1 0.63095 0.23584 0.48430 11.00000 0.04531 0.04342 0.03620 = -0.01918 0.00108 -0.00294 AFIX 43 H4 2 0.61358 0.30811 0.45962 11.00000 -1.20000 AFIX 0 C5 1 0.64910 0.18202 0.42771 11.00000 0.05955 0.06982 0.03931 = -0.03042 -0.00517 -0.00048 AFIX 43 H5 2 0.64457 0.21871 0.36500 11.00000 -1.20000 AFIX 0 C9 1 0.33074 0.11832 0.76811 11.00000 0.02771 0.02434 0.03040 = -0.01252 -0.00144 -0.00447 C15 1 0.22701 0.40665 0.59638 11.00000 0.03284 0.02823 0.02991 = -0.00984 -0.00524 -0.00883 AFIX 43 H15 2 0.28933 0.43818 0.56405 11.00000 -1.20000 AFIX 0 C14 1 0.11190 0.46237 0.58080 11.00000 0.03975 0.02874 0.03658 = -0.00828 -0.01192 -0.00471 AFIX 43 H14 2 0.09821 0.53099 0.53900 11.00000 -1.20000 AFIX 0 C10 1 0.18375 0.15161 0.77052 11.00000 0.02697 0.02721 0.03213 = -0.01404 0.00037 -0.00955 C17 1 0.21180 0.26575 0.45991 11.00000 0.07458 0.05035 0.04000 = -0.02252 -0.01582 -0.01310 AFIX 23 H17a 2 0.18688 0.28235 0.51446 11.00000 -1.20000 H17b 2 0.25311 0.19305 0.47846 11.00000 -1.20000 AFIX 0 C40 1 0.19517 0.60104 0.08745 11.00000 0.05026 0.04062 0.04740 = -0.01755 -0.00945 -0.01546 AFIX 23 H40a 2 0.27249 0.55382 0.09665 11.00000 -1.20000 H40b 2 0.18490 0.64659 0.11947 11.00000 -1.20000 AFIX 0 C39 1 0.19306 0.66605 -0.01389 11.00000 0.04729 0.03265 0.04890 = -0.01706 -0.00455 -0.01379 AFIX 23 H39a 2 0.11763 0.71615 -0.02416 11.00000 -1.20000 H39b 2 0.25491 0.70391 -0.03609 11.00000 -1.20000 AFIX 0 C32 1 -0.18823 0.34220 0.15553 11.00000 0.05277 0.03388 0.03995 = -0.00602 -0.00736 -0.01453 AFIX 23 H32a 2 -0.24725 0.30214 0.18933 11.00000 -1.20000 H32b 2 -0.11108 0.29435 0.15834 11.00000 -1.20000 AFIX 0 C31 1 -0.19238 0.41636 0.19771 11.00000 0.04409 0.04446 0.03529 = -0.01053 -0.00255 -0.01132 AFIX 23 H31a 2 -0.19429 0.38064 0.26394 11.00000 -1.20000 H31b 2 -0.26325 0.47200 0.18471 11.00000 -1.20000 AFIX 0 C101 1 0.41337 0.36210 0.25264 11.00000 0.04285 0.04861 0.06886 = -0.01675 -0.01564 -0.01629 AFIX 23 H10a 2 0.48022 0.35291 0.28194 11.00000 -1.20000 H10b 2 0.37331 0.43517 0.23116 11.00000 -1.20000 AFIX 0 C26 1 0.45597 0.32894 0.17297 11.00000 0.04064 0.05567 0.06727 = -0.01994 -0.00329 -0.00920 AFIX 23 H26a 2 0.49463 0.25553 0.19427 11.00000 -1.20000 H26b 2 0.51267 0.36762 0.13023 11.00000 -1.20000 AFIX 0 C25 1 0.38930 0.32824 0.04585 11.00000 0.06573 0.05753 0.04556 = -0.02501 0.01586 -0.01172 AFIX 23 H25a 2 0.43370 0.37715 -0.00001 11.00000 -1.20000 H25b 2 0.43845 0.25851 0.05791 11.00000 -1.20000 AFIX 0 C24 1 0.27953 0.33945 0.01122 11.00000 0.08295 0.04682 0.03554 = -0.01886 -0.00014 -0.00802 AFIX 23 H24a 2 0.30116 0.32456 -0.04421 11.00000 -1.20000 H24b 2 0.23502 0.41117 -0.00552 11.00000 -1.20000 AFIX 0 C100 1 0.25558 0.16517 0.09775 11.00000 0.07216 0.03661 0.04333 = -0.02070 -0.01800 0.00821 AFIX 23 H10c 2 0.28354 0.15047 0.04232 11.00000 -1.20000 H10d 2 0.32178 0.14259 0.13234 11.00000 -1.20000 AFIX 0 C22 1 0.16011 0.11005 0.15461 11.00000 0.07893 0.03300 0.05277 = -0.02009 -0.02243 -0.00235 AFIX 23 H22a 2 0.18863 0.03610 0.16829 11.00000 -1.20000 H22b 2 0.09241 0.13579 0.12094 11.00000 -1.20000 AFIX 0 C21 1 0.03096 0.08213 0.29414 11.00000 0.05452 0.03183 0.06571 = -0.01009 -0.02072 -0.01478 AFIX 23 H21a 2 0.05339 0.00762 0.30989 11.00000 -1.20000 H21b 2 -0.03773 0.11083 0.26114 11.00000 -1.20000 AFIX 0 C20 1 0.00182 0.10422 0.37931 11.00000 0.05324 0.04922 0.04953 = -0.00309 -0.00908 -0.01832 AFIX 23 H20a 2 -0.06140 0.07193 0.41903 11.00000 -1.20000 H20b 2 0.07052 0.07523 0.41231 11.00000 -1.20000 AFIX 0 C19 1 -0.06831 0.24177 0.43494 11.00000 0.05967 0.08023 0.04237 = -0.02798 0.00703 -0.01876 AFIX 23 H19a 2 -0.12348 0.20180 0.47838 11.00000 -1.20000 H19b 2 -0.10936 0.31459 0.41486 11.00000 -1.20000 AFIX 0 C18 1 0.03081 0.22577 0.48215 11.00000 0.07094 0.06957 0.03818 = -0.02468 0.00921 -0.02627 AFIX 23 H18a 2 0.06951 0.15247 0.50660 11.00000 -1.20000 H18b 2 0.00216 0.24891 0.53297 11.00000 -1.20000 AFIX 0 C29 1 -0.00934 0.60309 0.11666 11.00000 0.04604 0.03405 0.05128 = -0.02136 -0.00705 -0.00207 AFIX 23 H29a 2 -0.01844 0.66565 0.12719 11.00000 -1.20000 H29b 2 -0.02417 0.62360 0.05404 11.00000 -1.20000 AFIX 0 C30 1 -0.09617 0.54396 0.18189 11.00000 0.05236 0.04284 0.05172 = -0.02847 0.00072 -0.00711 AFIX 23 H30a 2 -0.17519 0.58877 0.17751 11.00000 -1.20000 H30b 2 -0.07856 0.51962 0.24438 11.00000 -1.20000 AFIX 0 C28 1 0.29190 0.33115 0.39439 11.00000 0.06303 0.04722 0.05409 = -0.02704 -0.02103 -0.00737 AFIX 23 H28a 2 0.35789 0.32250 0.42433 11.00000 -1.20000 H28b 2 0.24990 0.40372 0.37423 11.00000 -1.20000 AFIX 0 B15 3 0.59862 0.17190 0.75764 11.00000 0.03141 0.03062 0.02937 = -0.00767 -0.00357 -0.00663 H15a 2 0.60339 0.09330 0.78464 11.00000 -1.20000 B14 3 0.49761 0.25902 0.80476 11.00000 0.03935 0.03418 0.02459 = -0.01167 -0.00287 -0.01225 H14a 2 0.43760 0.22930 0.86524 11.00000 -1.20000 B18 3 0.65157 0.23754 0.80557 11.00000 0.03858 0.03710 0.03561 = -0.01109 -0.01027 -0.01037 H18 2 0.69613 0.19335 0.86770 11.00000 -1.20000 B3 3 0.11171 0.09670 0.87611 11.00000 0.03725 0.02895 0.03691 = -0.01162 0.00855 -0.01185 H3 2 0.02878 0.13953 0.89516 11.00000 -1.20000 B8 3 0.22659 0.01638 0.94610 11.00000 0.04736 0.02833 0.03311 = -0.00840 0.00274 -0.01249 H8a 2 0.21820 0.00095 1.02171 11.00000 -1.20000 B11 3 0.31205 -0.07823 0.89987 11.00000 0.04641 0.02606 0.03418 = -0.00915 0.00143 -0.01074 H11 2 0.35610 -0.15565 0.94283 11.00000 -1.20000 B6 3 0.37963 -0.01196 0.78763 11.00000 0.04064 0.02187 0.03468 = -0.01261 0.00331 -0.00767 H6a 2 0.46699 -0.04213 0.75451 11.00000 -1.20000 B4 3 0.12633 0.05123 0.78729 11.00000 0.03532 0.03090 0.04861 = -0.01638 -0.00096 -0.01521 H4a 2 0.05010 0.07384 0.75015 11.00000 -1.20000 B10 3 0.24990 -0.05644 0.80157 11.00000 0.04710 0.02624 0.04458 = -0.01662 0.00268 -0.01546 H10 2 0.25122 -0.11747 0.78193 11.00000 -1.20000 B9 3 0.15590 -0.03823 0.89907 11.00000 0.04401 0.03124 0.04592 = -0.01612 0.00942 -0.01966 H9 2 0.10098 -0.08492 0.93934 11.00000 -1.20000 B5 3 0.26394 0.06608 0.71914 11.00000 0.04063 0.02932 0.03305 = -0.01685 -0.00037 -0.01185 H5a 2 0.26733 0.09553 0.64663 11.00000 -1.20000 B2 3 0.24217 0.13926 0.86255 11.00000 0.03503 0.02606 0.02800 = -0.01007 -0.00011 -0.00832 H2 2 0.23917 0.21197 0.87035 11.00000 -1.20000 B7 3 0.36444 0.03293 0.87660 11.00000 0.04140 0.02540 0.02937 = -0.00741 -0.00341 -0.00831 H7a 2 0.44650 0.03515 0.89769 11.00000 -1.20000 B12 3 0.52487 0.36157 0.60945 11.00000 0.02933 0.02403 0.02928 = -0.00944 -0.00076 -0.00619 H12a 2 0.48349 0.39191 0.54675 11.00000 -1.20000 B16 3 0.57595 0.42954 0.65518 11.00000 0.03255 0.02911 0.03481 = -0.01240 -0.00296 -0.00921 H16 2 0.56472 0.51592 0.62124 11.00000 -1.20000 B21 3 0.69948 0.34459 0.71298 11.00000 0.03101 0.03763 0.04165 = -0.01246 -0.00719 -0.01131 H21 2 0.76910 0.37421 0.71733 11.00000 -1.20000 B20 3 0.67942 0.34199 0.60944 11.00000 0.03157 0.03151 0.03398 = -0.01194 0.00049 -0.01002 H20 2 0.73330 0.36136 0.54588 11.00000 -1.20000 B19 3 0.72523 0.22416 0.70156 11.00000 0.02599 0.03472 0.04260 = -0.01292 -0.00703 -0.00415 H19 2 0.80555 0.17530 0.69183 11.00000 -1.20000 B17 3 0.55969 0.36539 0.77703 11.00000 0.04031 0.03551 0.03468 = -0.01686 -0.00407 -0.01285 H17 2 0.53752 0.40636 0.82294 11.00000 -1.20000 B13 3 0.45137 0.37706 0.71267 11.00000 0.03249 0.02806 0.03158 = -0.01459 -0.00317 -0.00664 H13a 2 0.35906 0.42318 0.71177 11.00000 -1.20000 HKLF 4 END Q1 1 0 0.16 0.462963 11 0.05 0.56 Q2 1 0.075 0.34 0.388889 11 0.05 0.54 Q3 1 0.3 0.08 0.87037 11 0.05 0.44 Q4 1 -0.025 0.28 0.444444 11 0.05 0.42 Q5 1 0.15 0.02 0.87037 11 0.05 0.41 Q6 1 -0.025 0.16 0.314815 11 0.05 0.4 Q7 1 -0.075 0.08 0.222222 11 0.05 0.37 REM The information below was added by Olex2. REM REM R1 = 0.0558 for 6460 Fo > 4sig(Fo) and 0.1079 for all 10682 data REM 646 parameters refined using 0 restraints REM Highest difference peak 0.5591, deepest hole -0.4255 REM Mean Shift 0.0001, Max Shift 0.0008. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.1079 REM R1_gt = 0.0558 REM wR_ref = 0.1585 REM GOOF = 1.0362 REM Shift_max = 0.0008 REM Shift_mean = 0.0001 REM Reflections_all = 10682 REM Reflections_gt = 6460 REM Parameters = 646 REM Hole = -0.4255 REM Peak = 0.5591 REM Flack = n/a ; _cod_data_source_file d6sc03158g2.cif _cod_data_source_block K-crown[1] _cod_database_code 1577437 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All B(H) groups, All C(H) groups, All C(H,H) groups 2.a Ternary CH refined with riding coordinates: B1(H1) 2.b Secondary CH2 refined with riding coordinates: C17(H17a,H17b), C40(H40a,H40b), C39(H39a,H39b), C32(H32a,H32b), C31(H31a, H31b), C101(H10a,H10b), C26(H26a,H26b), C25(H25a,H25b), C24(H24a,H24b), C100(H10c,H10d), C22(H22a,H22b), C21(H21a,H21b), C20(H20a,H20b), C19(H19a, H19b), C18(H18a,H18b), C29(H29a,H29b), C30(H30a,H30b), C28(H28a,H28b) 2.c Aromatic/amide H refined with riding coordinates: C6(H6), C7(H7), C8(H8), C12(H12), C13(H13), C4(H4), C5(H5), C15(H15), C14(H14) ; _iucr_refine_fcf_details ; data_K-crown[1]_CCDC1 _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_Int_Tables_number 2 _cell_length_a 11.9698(8) _cell_length_b 14.6251(9) _cell_length_c 16.1758(11) _cell_angle_alpha 64.822(2) _cell_angle_beta 76.409(2) _cell_angle_gamma 72.142(2) _cell_volume 2421.2(3) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -14 -8 1 5.690 40.538 23.255 39.612 o -14 -7 1 0.509 -2.151 32.139 21.663 o -14 -7 2 5.854 17.271 22.962 41.410 o -14 -6 1 37.632 73.068 26.866 28.098 o -14 -6 2 19.411 19.645 21.664 45.052 o -14 -5 1 139.257 139.644 32.823 16.812 o -14 -5 2 57.671 52.185 25.830 29.725 o -14 -5 3 20.006 -9.029 21.203 47.821 o -14 -4 1 22.753 46.803 21.262 45.063 o -14 -4 2 438.227 463.726 43.529 7.040 o -14 -4 3 0.969 12.991 22.802 42.501 o -14 -3 1 114.722 105.335 25.540 26.485 o -14 -3 2 35.771 23.616 25.804 31.440 o -14 -3 3 83.872 46.226 23.713 33.127 o -14 -2 1 0.725 -22.451 12.953 132.910 o -14 -2 2 24.853 19.295 25.491 32.796 o -14 -2 3 0.011 14.271 21.072 49.691 o -14 -1 1 48.229 37.091 25.595 31.012 o -14 -1 2 16.567 13.878 19.951 53.303 o -14 -1 3 7.195 7.857 20.172 53.672 o -14 0 1 30.167 42.407 22.233 41.116 o -14 0 2 1.682 -5.848 16.020 86.715 o -14 0 3 16.177 1.624 22.358 43.421 o -14 1 1 5.561 12.584 17.696 69.094 o -14 1 2 32.133 0.872 19.500 54.453 o -13 -10 1 62.712 127.777 27.945 24.359 o -13 -9 1 124.548 116.730 27.302 23.306 o -13 -9 2 11.480 2.356 18.678 62.099 o -13 -8 1 12.463 29.671 18.376 61.613 o -13 -8 2 8.836 8.675 19.578 56.619 o -13 -8 3 10.610 -7.271 17.874 68.009 o -13 -7 1 98.556 122.897 22.508 32.479 o -13 -7 2 26.134 14.870 18.653 58.942 o -13 -7 3 114.142 72.358 23.593 30.835 o -13 -7 4 32.920 13.609 19.601 53.015 o -13 -6 1 43.523 36.497 18.009 58.059 o -13 -6 2 16.149 29.788 17.847 64.357 o -13 -6 3 0.032 -16.698 17.703 71.425 o -13 -6 4 2.051 27.168 22.966 41.315 o -13 -6 5 5.859 10.455 22.005 45.282 o -13 -5 1 343.520 413.722 38.739 9.115 o -13 -5 2 113.722 146.236 30.638 19.306 o -13 -5 3 23.906 32.630 22.508 41.060 o -13 -5 4 34.979 42.326 20.381 47.569 o -13 -5 5 1.136 -1.979 22.336 44.780 o -13 -4 1 81.017 104.225 20.727 38.857 o -13 -4 2 46.735 22.424 16.642 67.009 o -13 -4 3 65.609 71.722 22.904 35.457 o -13 -4 4 2.207 -7.228 15.433 93.212 o -13 -4 5 32.575 60.290 24.172 34.621 o -13 -4 6 25.440 5.060 19.777 53.630 o -13 -3 1 20.791 10.661 13.665 105.977 o -13 -3 2 19.581 27.658 16.089 77.049 o -13 -3 3 79.952 95.555 22.144 35.541 o -13 -3 4 7.932 3.293 16.063 83.921 o -13 -3 5 16.847 -16.547 17.430 70.094 o -13 -3 6 24.575 62.745 23.304 37.430 o -13 -2 1 229.508 259.028 23.756 20.672 o -13 -2 2 25.130 7.326 15.867 80.271 o -13 -2 3 0.280 5.682 15.277 94.776 o -13 -2 4 0.054 -11.747 14.823 101.854 o -13 -2 5 3.522 -3.694 19.186 60.291 o -13 -2 6 8.928 26.704 20.958 48.667 o -13 -1 1 80.683 59.600 16.400 57.884 o -13 -1 2 74.562 68.774 20.660 41.248 o -13 -1 3 49.528 70.933 22.785 36.911 o -13 -1 4 64.674 35.378 20.365 44.860 o -13 -1 5 14.503 29.694 21.234 46.777 o -13 -1 6 4.214 -18.591 19.245 59.825 o -13 0 1 189.225 229.322 22.808 23.979 o -13 0 2 0.827 -2.075 15.787 89.555 o -13 0 3 92.957 99.650 24.848 28.824 o -13 0 4 2.316 -17.532 17.823 70.007 o -13 0 5 3.882 25.105 21.281 47.829 o -13 0 6 12.129 0.975 17.662 69.194 o -13 1 1 41.062 49.026 16.269 67.818 o -13 1 2 4.351 24.395 16.662 76.427 o -13 1 3 7.920 1.608 17.462 71.551 o -13 1 4 4.037 -8.740 16.166 84.484 o -13 1 5 110.662 132.580 23.006 30.423 o -13 1 6 21.038 -1.488 19.358 56.777 o -13 2 1 5.434 13.336 14.161 105.789 o -13 2 2 0.301 -5.978 14.872 101.083 o -13 2 3 79.478 89.828 19.401 43.753 o -13 2 4 18.694 3.994 15.617 85.080 o -13 2 5 33.083 27.434 21.360 44.627 o -13 3 1 12.616 7.653 18.233 64.400 o -13 3 2 6.347 -0.531 24.246 37.709 o -13 3 3 2.647 3.527 17.815 69.658 o -13 3 4 20.547 24.790 21.523 45.271 o -13 4 1 11.408 -2.732 17.355 71.833 o -13 4 2 3.039 -4.992 17.473 72.669 o -13 4 3 15.531 10.002 24.804 35.291 o -12 -12 1 61.568 64.428 22.181 37.970 o -12 -11 1 47.676 39.729 20.686 45.178 o -12 -11 2 12.096 9.042 19.307 57.680 o -12 -10 1 36.760 26.063 20.586 47.400 o -12 -10 2 96.787 85.851 23.380 31.899 o -12 -10 3 86.864 57.482 23.418 33.287 o -12 -9 1 12.511 28.789 17.003 71.215 o -12 -9 2 3.714 -24.869 16.660 79.689 o -12 -9 3 5.568 22.271 17.990 66.022 o -12 -9 4 15.330 28.358 20.455 50.166 o -12 -8 1 29.306 38.425 17.821 61.377 o -12 -8 2 35.597 27.342 17.954 60.458 o -12 -8 3 103.804 136.822 24.883 27.335 o -12 -8 4 20.166 10.253 19.624 54.762 o -12 -8 5 72.930 107.594 25.154 29.038 o -12 -7 1 8.102 31.893 16.622 74.931 o -12 -7 2 1.966 -16.738 14.076 111.975 o -12 -7 3 82.015 60.674 20.424 41.671 o -12 -7 4 0.378 -8.368 18.758 63.561 o -12 -7 5 1.546 -3.230 17.856 69.905 o -12 -7 6 3.074 -14.232 19.019 61.413 o -12 -6 1 51.316 23.385 16.928 64.110 o -12 -6 2 200.977 161.619 25.439 21.926 o -12 -6 3 11.483 -0.347 15.953 84.477 o -12 -6 4 4.235 10.303 17.860 68.341 o -12 -6 5 28.713 5.681 20.585 49.352 o -12 -6 6 0.085 -2.062 24.123 38.463 o -12 -6 7 4.757 -1.027 23.495 40.239 o -12 -5 1 130.388 141.537 20.803 33.167 o -12 -5 2 20.543 13.735 14.858 90.805 o -12 -5 3 0.039 -7.602 15.014 99.285 o -12 -5 4 11.652 14.511 18.415 62.772 o -12 -5 5 0.284 -16.860 15.633 91.509 o -12 -5 6 41.418 30.429 19.776 50.102 o -12 -5 7 2.102 11.534 19.617 57.111 o -12 -4 1 266.833 270.839 21.756 20.714 o -12 -4 2 40.166 23.941 15.641 75.737 o -12 -4 3 54.941 48.033 20.817 43.577 o -12 -4 4 476.070 546.338 35.262 8.080 o -12 -4 5 54.790 67.224 24.986 31.285 o -12 -4 6 13.208 28.530 19.013 57.801 o -12 -4 7 4.407 -1.093 18.679 63.434 o -12 -3 1 72.241 83.782 15.911 59.625 o -12 -3 2 485.815 587.481 34.514 7.949 o -12 -3 3 19.119 27.914 16.164 76.497 o -12 -3 4 171.294 142.751 24.481 24.686 o -12 -3 5 16.401 11.928 16.117 79.781 o -12 -3 6 9.851 -12.902 16.678 77.963 o -12 -3 7 4.262 -9.431 17.646 71.009 o -12 -3 8 24.440 -12.806 19.608 54.956 o -12 -2 1 164.376 108.857 21.072 31.383 o -12 -2 2 217.338 234.206 23.625 21.763 o -12 -2 3 229.959 284.968 31.998 14.264 o -12 -2 4 105.092 70.213 24.988 28.693 o -12 -2 5 6.192 -12.067 14.809 99.529 o -12 -2 6 386.610 460.723 36.297 9.134 o -12 -2 7 1.843 -1.373 17.705 71.039 o -12 -2 8 145.841 158.510 31.973 17.200 o -12 -1 1 0.017 -5.002 12.362 146.474 o -12 -1 2 124.606 133.810 22.811 29.923 o -12 -1 3 1.838 -21.982 14.344 107.933 o -12 -1 4 237.147 320.658 34.734 12.411 o -12 -1 5 0.010 0.349 14.731 103.077 o -12 -1 6 42.121 41.943 18.635 54.602 o -12 -1 7 21.033 31.090 18.392 59.995 o -12 -1 8 0.153 5.624 18.527 64.716 o -12 0 1 24.817 14.137 15.808 79.932 o -12 0 2 5.783 16.239 14.835 96.143 o -12 0 3 17.866 -1.791 14.048 104.663 o -12 0 4 0.413 -23.160 15.274 95.796 o -12 0 5 1.607 -0.679 14.549 105.046 o -12 0 6 47.114 26.965 18.469 55.811 o -12 0 7 22.137 19.720 17.827 64.310 o -12 0 8 13.080 -11.714 18.449 63.530 o -12 1 1 61.568 90.301 15.792 61.748 o -12 1 2 106.135 84.802 19.056 42.231 o -12 1 3 1.646 35.213 31.298 22.444 o -12 1 4 155.228 147.734 39.843 11.952 o -12 1 5 22.637 18.023 15.874 79.407 o -12 1 6 36.925 64.617 18.424 54.748 o -12 1 7 0.352 -8.259 15.319 95.268 o -12 1 8 5.063 17.691 16.602 77.618 o -12 2 1 1.927 -5.195 11.192 176.283 o -12 2 2 31.071 9.920 13.597 102.121 o -12 2 3 84.052 98.135 20.810 38.627 o -12 2 4 146.092 171.570 25.417 23.915 o -12 2 5 6.112 13.087 14.443 101.662 o -12 2 6 4.734 7.983 16.957 75.761 o -12 2 7 172.550 214.999 55.509 6.485 o -12 2 8 1.226 -1.225 21.505 48.289 o -12 3 1 127.052 126.152 16.834 43.972 o -12 3 2 0.381 -1.395 11.896 157.805 o -12 3 3 59.394 51.793 15.156 70.537 o -12 3 4 0.401 -2.749 13.732 118.496 o -12 3 5 144.985 152.338 27.665 21.560 o -12 3 6 16.142 0.002 19.230 58.194 o -12 3 7 25.809 54.649 23.717 36.429 o -12 4 1 153.940 161.703 23.831 25.951 o -12 4 2 3.092 0.783 12.723 135.654 o -12 4 3 20.060 21.615 14.070 98.565 o -12 4 4 52.450 17.575 19.025 52.968 o -12 4 5 0.725 -32.722 17.193 75.564 o -12 4 6 8.091 -0.565 23.353 40.502 o -12 4 7 78.004 70.105 25.427 29.167 o -12 5 1 0.030 4.460 12.417 143.302 o -12 5 2 0.812 -5.893 12.856 134.841 o -12 5 3 29.467 16.774 16.935 69.316 o -12 5 4 39.011 22.768 20.901 46.066 o -12 5 5 72.670 92.356 25.758 28.277 o -12 5 6 58.324 91.538 25.137 30.177 o -12 6 1 134.436 143.626 28.102 21.532 o -12 6 2 55.588 59.810 18.910 50.254 o -12 6 3 97.143 108.020 28.951 22.194 o -12 6 4 31.072 44.705 21.144 44.826 o -11 -13 1 1.620 6.914 16.081 85.049 o -11 -12 1 38.621 37.570 28.447 25.856 o -11 -12 2 13.184 -11.262 17.410 71.015 o -11 -12 3 104.997 66.094 22.660 33.592 o -11 -11 1 35.271 45.601 18.997 53.536 o -11 -11 2 133.398 126.194 24.188 27.292 o -11 -11 3 41.130 25.924 19.230 52.943 o -11 -11 4 0.010 -5.524 40.413 13.707 o -11 -10 1 108.678 108.836 24.526 28.392 o -11 -10 2 20.096 -5.696 16.965 73.040 o -11 -10 3 3.393 11.322 17.864 68.377 o -11 -10 4 0.042 -11.011 17.284 74.929 o -11 -10 5 61.110 67.114 25.883 29.127 o -11 -9 1 2.627 4.449 15.976 86.222 o -11 -9 2 61.340 23.379 28.368 25.483 o -11 -9 3 0.038 23.311 16.835 76.112 o -11 -9 4 74.926 47.490 30.173 22.081 o -11 -9 5 10.364 26.955 19.579 55.193 o -11 -9 6 97.096 16.126 26.400 27.698 o -11 -8 1 18.657 20.888 20.301 50.929 o -11 -8 2 333.393 269.120 28.332 14.386 o -11 -8 3 4.931 15.578 16.808 76.098 o -11 -8 4 41.377 37.504 18.590 55.261 o -11 -8 5 2.489 -9.772 16.614 80.450 o -11 -8 6 11.416 -9.104 21.838 45.933 o -11 -8 7 53.695 67.368 25.507 30.223 o -11 -7 1 10.973 51.495 19.598 53.415 o -11 -7 2 13.919 30.078 17.924 64.226 o -11 -7 3 7.339 16.524 14.920 94.466 o -11 -7 4 35.260 10.136 16.870 69.246 o -11 -7 5 10.766 -12.585 16.037 83.833 o -11 -7 6 49.373 20.563 17.972 58.608 o -11 -7 7 0.439 -0.768 19.920 56.358 o -11 -6 1 20.628 12.864 11.625 139.434 o -11 -6 2 268.931 266.476 26.215 17.294 o -11 -6 3 9.643 -4.789 15.181 93.558 o -11 -6 4 151.259 185.947 24.398 24.726 o -11 -6 5 25.716 37.933 17.977 61.110 o -11 -6 6 50.455 46.769 19.518 49.140 o -11 -6 7 24.785 31.904 19.364 54.062 o -11 -6 8 10.254 -14.171 17.261 72.847 o -11 -5 1 7.727 16.575 12.964 122.443 o -11 -5 2 88.118 74.392 16.397 55.238 o -11 -5 3 90.517 55.675 25.945 27.958 o -11 -5 4 1.323 -2.262 13.223 127.173 o -11 -5 5 27.722 33.849 20.803 47.041 o -11 -5 6 0.624 -15.387 14.843 101.355 o -11 -5 7 56.502 53.591 20.302 44.994 o -11 -5 8 7.682 -10.367 19.086 60.298 o -11 -5 9 26.703 18.370 23.514 38.131 o -11 -4 1 189.468 190.935 24.960 22.333 o -11 -4 2 56.124 31.594 14.013 83.276 o -11 -4 3 561.165 638.489 48.271 5.206 o -11 -4 4 37.985 36.619 16.620 67.513 o -11 -4 5 72.675 69.250 18.352 49.675 o -11 -4 6 0.772 -13.116 14.744 102.648 o -11 -4 7 34.200 51.096 19.714 50.000 o -11 -4 8 28.501 42.434 19.160 53.878 o -11 -4 9 0.529 -12.224 18.268 66.982 o -11 -3 1 195.821 215.801 20.453 26.925 o -11 -3 2 26.892 -6.870 11.952 133.170 o -11 -3 3 0.492 -29.164 11.788 160.596 o -11 -3 4 1.935 11.988 13.338 120.926 o -11 -3 5 137.146 177.160 26.396 22.913 o -11 -3 6 141.293 138.956 22.313 29.661 o -11 -3 7 167.967 203.915 27.412 20.265 o -11 -3 8 3.173 5.479 17.479 72.005 o -11 -3 9 64.364 82.215 33.117 18.526 o -11 -2 1 0.036 3.242 11.564 165.560 o -11 -2 2 2.063 -1.594 12.947 132.083 o -11 -2 3 408.201 505.652 35.426 8.906 o -11 -2 4 52.447 38.823 18.793 52.607 o -11 -2 5 98.601 101.942 20.530 37.954 o -11 -2 6 0.021 -6.989 14.165 111.560 o -11 -2 7 57.458 68.648 19.989 45.244 o -11 -2 8 2.603 -22.978 16.188 84.665 o -11 -2 9 11.063 3.735 18.867 60.858 o -11 -2 10 11.067 -0.813 20.807 50.526 o -11 -1 1 52.390 30.023 13.138 93.263 o -11 -1 2 38.463 5.393 14.091 94.025 o -11 -1 3 381.410 441.640 33.429 10.128 o -11 -1 4 13.491 20.359 15.796 82.420 o -11 -1 5 91.490 72.449 19.909 41.776 o -11 -1 6 0.615 6.816 17.281 74.056 o -11 -1 7 4.674 -0.141 14.782 100.508 o -11 -1 8 233.729 273.412 37.164 11.643 o -11 -1 9 0.010 12.740 17.872 68.841 o -11 -1 10 60.083 38.346 22.722 37.498 o -11 0 1 37.379 23.438 11.761 120.304 o -11 0 2 15.043 5.782 12.108 137.175 o -11 0 3 21.019 8.297 15.623 83.640 o -11 0 4 120.113 162.816 24.390 26.726 o -11 0 5 8.579 18.295 15.439 87.874 o -11 0 6 51.425 57.348 20.107 46.063 o -11 0 7 80.879 54.067 24.136 32.110 o -11 0 8 0.488 -5.644 17.827 70.341 o -11 0 9 1.845 2.796 17.187 75.038 o -11 0 10 0.752 -4.336 20.465 53.367 o -11 1 1 0.843 -8.460 9.486 246.718 o -11 1 2 6.321 -11.034 11.320 167.207 o -11 1 3 45.390 53.721 16.741 63.403 o -11 1 4 61.186 43.459 17.152 59.049 o -11 1 5 256.699 256.931 36.308 11.845 o -11 1 6 58.084 38.252 14.353 78.715 o -11 1 7 3.388 4.781 12.999 128.491 o -11 1 8 236.752 281.092 28.368 16.458 o -11 1 9 6.127 -4.296 15.352 92.793 o -11 1 10 102.544 110.443 22.449 32.754 o -11 2 1 0.068 12.097 10.460 194.730 o -11 2 2 39.294 22.405 13.732 94.145 o -11 2 3 4.725 -15.345 11.918 152.988 o -11 2 4 20.671 39.515 15.270 82.312 o -11 2 5 125.841 136.159 18.891 38.057 o -11 2 6 123.207 128.021 17.893 41.334 o -11 2 7 53.655 30.865 21.136 43.383 o -11 2 8 87.360 101.361 21.554 36.253 o -11 2 9 33.417 -14.392 19.809 52.783 o -11 2 10 5.129 22.000 24.746 35.690 o -11 3 1 0.191 -10.733 9.333 256.510 o -11 3 2 9.961 2.270 10.101 199.560 o -11 3 3 79.088 75.045 14.882 64.541 o -11 3 4 15.539 15.761 13.992 102.865 o -11 3 5 0.286 12.410 16.493 80.549 o -11 3 6 37.158 39.576 19.951 49.299 o -11 3 7 1.819 10.841 18.493 64.219 o -11 3 8 174.191 176.780 26.298 21.686 o -11 3 9 13.653 12.236 26.269 31.601 o -11 3 10 104.772 81.048 28.465 23.011 o -11 4 1 7.824 16.465 10.493 179.212 o -11 4 2 12.915 -3.372 10.056 198.168 o -11 4 3 20.445 -2.468 12.240 132.603 o -11 4 4 2.776 -6.646 13.728 117.231 o -11 4 5 12.537 -1.233 17.596 69.713 o -11 4 6 54.875 92.172 23.282 34.536 o -11 4 7 114.065 112.836 35.049 15.701 o -11 4 8 19.792 26.206 21.090 47.031 o -11 4 9 43.086 69.179 26.262 29.126 o -11 5 1 103.875 86.287 13.491 64.535 o -11 5 2 55.969 41.753 12.530 95.268 o -11 5 3 62.080 55.729 15.778 65.457 o -11 5 4 51.001 6.332 15.014 80.378 o -11 5 5 154.385 143.090 25.127 24.549 o -11 5 6 355.915 345.442 39.257 9.171 o -11 5 7 0.043 16.741 19.255 59.157 o -11 5 8 46.798 93.622 29.394 23.285 o -11 5 9 46.460 35.171 22.337 39.785 o -11 6 1 135.954 113.987 15.807 46.661 o -11 6 2 3.058 25.393 13.593 112.322 o -11 6 3 15.266 21.781 15.764 81.991 o -11 6 4 0.148 -16.037 13.075 130.840 o -11 6 5 27.688 3.103 22.619 41.519 o -11 6 6 7.029 24.911 29.107 25.872 o -11 6 7 25.351 46.580 28.689 25.721 o -11 6 8 12.457 4.214 21.716 46.159 o -11 7 1 1.412 -1.053 15.351 94.492 o -11 7 2 21.929 13.009 13.183 111.627 o -11 7 3 22.851 20.795 13.533 104.276 o -11 7 4 35.946 26.597 15.067 81.430 o -11 7 5 156.605 181.770 27.670 20.707 o -11 7 6 10.903 -17.191 20.279 53.145 o -11 7 7 236.929 321.253 37.015 11.377 o -11 8 1 17.418 14.992 20.501 50.464 o -11 8 2 34.158 35.873 21.485 43.681 o -11 8 3 119.434 184.946 25.407 24.761 o -11 8 4 1.586 -8.127 16.570 81.112 o -10 -14 1 25.916 -4.502 15.993 79.932 o -10 -13 1 0.424 0.598 13.411 124.014 o -10 -13 2 5.534 3.029 15.613 89.486 o -10 -13 3 59.605 64.400 22.064 38.459 o -10 -12 1 56.462 44.642 19.420 48.952 o -10 -12 2 51.009 32.823 16.265 67.427 o -10 -12 3 34.662 21.911 17.034 66.970 o -10 -12 4 71.328 38.791 20.001 45.313 o -10 -11 1 117.329 102.896 23.342 30.262 o -10 -11 2 109.069 98.503 23.950 29.695 o -10 -11 3 289.577 400.980 44.845 7.948 o -10 -11 4 4.952 -0.145 20.384 53.299 o -10 -11 5 0.085 -19.530 18.824 63.164 o -10 -10 1 94.982 93.233 21.416 36.325 o -10 -10 2 203.445 219.739 29.085 17.535 o -10 -10 3 4.374 6.330 15.893 86.285 o -10 -10 4 244.202 261.930 29.872 15.509 o -10 -10 5 87.376 53.702 19.147 45.776 o -10 -10 6 7.947 10.583 22.616 42.750 o -10 -9 1 9.769 43.626 15.494 82.926 o -10 -9 2 20.953 8.468 15.644 83.431 o -10 -9 3 7.003 -2.675 14.410 104.603 o -10 -9 4 139.904 147.719 24.574 25.869 o -10 -9 5 0.011 -3.197 16.072 86.661 o -10 -9 6 45.969 34.296 25.479 31.445 o -10 -9 7 147.578 175.111 31.755 17.172 o -10 -8 1 5.898 -4.026 12.795 132.411 o -10 -8 2 151.058 122.666 26.248 23.607 o -10 -8 3 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148.307 162.163 21.928 29.191 o 10 7 14 5.396 13.152 11.616 153.433 o 10 7 15 6.012 14.460 12.237 138.262 o 10 7 16 2.434 28.884 14.276 102.035 o 10 7 17 9.664 8.778 14.880 95.526 o 10 7 18 12.062 11.584 17.407 70.065 o 10 8 0 43.148 49.498 11.870 107.182 o 10 8 1 34.734 38.190 11.709 117.924 o 10 8 2 49.550 69.695 12.424 92.904 o 10 8 3 14.578 1.562 10.323 185.447 o 10 8 4 479.429 494.008 32.061 9.015 o 10 8 5 128.048 131.005 15.926 46.212 o 10 8 6 77.501 56.233 14.140 71.811 o 10 8 7 246.658 303.391 21.296 21.265 o 10 8 8 48.124 31.219 10.723 125.496 o 10 8 9 279.618 259.845 21.061 20.989 o 10 8 10 55.198 55.229 13.298 85.570 o 10 8 11 11.654 -6.060 10.736 177.762 o 10 8 12 9.018 5.739 9.825 208.417 o 10 8 13 127.957 115.063 16.252 46.347 o 10 8 14 293.120 377.123 33.930 11.558 o 10 8 15 163.386 197.406 31.596 16.729 o 10 8 16 3.399 -6.192 14.363 106.918 o 10 8 17 8.513 -17.780 16.442 80.498 o 10 8 18 0.125 -25.910 18.704 63.966 o 10 9 0 0.976 -4.371 9.637 238.767 o 10 9 1 47.314 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109.635 81.434 15.739 53.669 o 11 1 8 2.850 -0.247 9.685 232.309 o 11 1 9 0.543 9.562 8.797 272.315 o 11 1 10 7.581 7.234 15.995 84.128 o 11 1 11 0.194 -11.054 12.961 133.120 o 11 1 12 3.621 -13.935 15.002 98.037 o 11 1 13 17.870 16.286 16.108 78.864 o 11 1 14 45.507 27.214 20.145 48.221 o 11 2 0 0.029 -3.797 12.108 152.676 o 11 2 1 16.060 16.318 11.911 136.081 o 11 2 2 606.389 610.280 32.037 7.199 o 11 2 3 98.745 116.618 19.250 40.769 o 11 2 4 36.029 39.369 14.132 87.978 o 11 2 5 2.794 17.318 11.944 146.171 o 11 2 6 0.548 -5.821 9.933 225.758 o 11 2 7 14.171 1.060 10.227 189.503 o 11 2 8 418.726 397.092 27.967 11.682 o 11 2 9 5.687 12.668 11.950 145.527 o 11 2 10 84.563 74.737 15.344 60.906 o 11 2 11 40.563 35.999 9.717 147.064 o 11 2 12 6.162 10.138 15.354 90.990 o 11 2 13 32.998 35.348 17.307 64.155 o 11 2 14 23.476 29.096 18.410 59.651 o 11 2 15 0.069 -8.842 18.000 69.083 o 11 3 0 162.070 130.004 16.803 39.644 o 11 3 1 159.802 170.852 21.022 29.705 o 11 3 2 717.266 777.962 45.081 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6.838 23.173 12.277 133.431 o 11 4 14 0.066 -6.985 10.605 198.941 o 11 4 15 1.822 -4.171 10.113 215.441 o 11 4 16 9.205 21.370 20.576 50.667 o 11 5 0 3.276 7.468 10.766 183.085 o 11 5 1 59.571 20.930 10.758 120.299 o 11 5 2 239.938 250.172 23.645 20.545 o 11 5 3 112.653 113.149 17.356 45.065 o 11 5 4 398.170 428.133 27.137 12.058 o 11 5 5 260.687 233.319 21.380 22.107 o 11 5 6 89.655 76.372 13.752 68.088 o 11 5 7 15.474 2.270 8.509 255.155 o 11 5 8 41.355 1.170 11.097 136.943 o 11 5 9 265.442 246.677 24.008 19.373 o 11 5 10 2.609 20.906 12.131 140.668 o 11 5 11 38.036 33.971 12.970 100.730 o 11 5 12 1.264 -6.719 11.913 156.483 o 11 5 13 4.234 -5.046 11.684 159.501 o 11 5 14 11.167 13.572 11.406 152.582 o 11 5 15 166.986 137.642 19.468 33.148 o 11 5 16 5.039 16.945 16.988 74.376 o 11 6 0 7.826 25.130 12.729 123.701 o 11 6 1 0.017 7.796 11.355 168.986 o 11 6 2 168.428 164.003 21.759 28.203 o 11 6 3 6.840 4.584 12.855 128.961 o 11 6 4 3.685 12.379 11.926 148.021 o 11 6 5 27.580 9.479 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123.491 o 11 7 14 54.881 34.651 12.124 101.864 o 11 7 15 15.578 -7.057 11.145 161.557 o 11 7 16 11.831 3.556 14.108 105.825 o 11 7 17 31.966 32.473 20.810 46.651 o 11 8 0 16.115 13.347 12.134 132.860 o 11 8 1 73.282 115.478 15.938 56.276 o 11 8 2 26.459 3.275 15.765 81.412 o 11 8 3 65.529 59.823 16.064 62.602 o 11 8 4 35.387 31.051 14.307 88.011 o 11 8 5 99.593 103.388 16.279 51.383 o 11 8 6 37.366 41.463 14.284 85.657 o 11 8 7 196.545 165.962 20.166 28.827 o 11 8 8 27.445 32.367 12.012 120.132 o 11 8 9 184.555 219.493 21.456 26.140 o 11 8 10 24.302 10.232 11.541 139.119 o 11 8 11 148.729 131.307 18.428 37.186 o 11 8 12 5.367 -0.418 12.739 133.922 o 11 8 13 119.371 98.357 18.743 41.010 o 11 8 14 43.295 46.675 14.400 81.718 o 11 8 15 2.388 4.384 13.607 118.253 o 11 8 16 0.203 -15.028 16.604 81.143 o 11 8 17 12.750 5.698 19.308 57.822 o 11 9 0 0.676 -25.228 10.355 207.587 o 11 9 1 4.298 -2.546 10.904 182.328 o 11 9 2 0.026 -1.881 12.797 136.680 o 11 9 3 2.846 8.485 12.698 133.502 o 11 9 4 286.950 266.061 29.955 14.509 o 11 9 5 10.690 46.390 15.110 85.939 o 11 9 6 274.196 271.144 28.154 15.808 o 11 9 7 272.851 298.667 29.320 14.825 o 11 9 8 54.401 38.609 16.551 64.258 o 11 9 9 473.878 523.219 40.580 7.151 o 11 9 10 15.050 22.826 14.243 98.319 o 11 9 11 3.074 1.576 11.724 158.829 o 11 9 12 0.252 -14.235 11.573 166.848 o 11 9 13 76.858 119.314 21.345 36.909 o 11 9 14 66.790 56.119 15.319 67.122 o 11 9 15 29.405 43.447 16.477 69.655 o 11 9 16 156.580 134.900 26.676 22.632 o 11 9 17 2.361 -1.543 19.209 60.321 o 11 10 0 7.257 16.457 12.214 136.968 o 11 10 1 7.528 -7.128 12.647 134.219 o 11 10 2 10.779 -7.575 12.338 138.118 o 11 10 3 45.286 52.828 20.554 45.255 o 11 10 4 19.858 12.827 14.427 96.170 o 11 10 5 5.656 18.626 12.765 126.669 o 11 10 6 6.178 20.705 12.640 127.895 o 11 10 7 45.574 52.637 15.271 73.251 o 11 10 8 162.996 165.003 20.358 30.809 o 11 10 9 96.083 86.873 15.884 54.976 o 11 10 10 58.103 62.323 14.941 70.951 o 11 10 11 71.708 38.524 20.585 43.217 o 11 10 12 194.505 255.528 26.259 19.689 o 11 10 13 148.778 140.278 17.332 39.281 o 11 10 14 226.426 247.586 23.757 21.010 o 11 10 15 19.087 4.672 15.106 90.219 o 11 10 16 27.190 9.121 26.917 29.667 o 11 10 17 0.650 13.870 22.248 44.603 o 11 11 0 113.993 107.781 24.073 28.956 o 11 11 1 3.644 -6.855 11.725 159.017 o 11 11 2 0.060 -6.254 14.643 104.379 o 11 11 3 5.798 -6.375 14.396 105.342 o 11 11 4 4.932 -15.319 13.261 124.141 o 11 11 5 24.029 1.059 12.157 131.100 o 11 11 6 14.650 14.539 12.530 126.173 o 11 11 7 239.202 270.863 27.712 16.985 o 11 11 8 2.409 6.144 12.903 130.566 o 11 11 9 103.029 99.006 17.414 47.069 o 11 11 10 14.229 12.469 10.742 166.567 o 11 11 11 190.304 222.615 22.143 24.886 o 11 11 12 42.245 37.503 13.838 88.860 o 11 11 13 244.047 252.769 24.287 19.788 o 11 11 14 0.015 -17.803 13.075 130.938 o 11 11 15 12.765 25.977 16.172 78.368 o 11 11 16 43.299 30.016 21.158 44.314 o 11 11 17 3.575 2.971 22.319 44.530 o 11 12 0 54.695 41.324 13.606 85.634 o 11 12 1 51.409 52.083 18.641 52.531 o 11 12 2 25.866 62.432 20.302 47.792 o 11 12 3 24.190 -6.297 15.333 86.862 o 11 12 4 0.514 -2.817 14.676 103.715 o 11 12 5 1.922 13.985 13.076 124.994 o 11 12 6 12.290 -6.265 11.543 154.909 o 11 12 7 15.268 4.331 12.008 139.644 o 11 12 8 25.069 25.427 14.004 96.409 o 11 12 9 0.410 8.273 11.915 153.246 o 11 12 10 10.271 5.945 11.072 166.147 o 11 12 11 10.431 21.893 13.330 113.307 o 11 12 12 19.436 -2.552 13.191 116.573 o 11 12 13 25.296 36.098 17.342 65.359 o 11 12 14 147.392 180.393 25.981 22.977 o 11 12 15 7.820 10.630 17.877 67.500 o 11 12 16 148.712 158.900 28.213 20.726 o 11 13 0 26.711 22.602 15.772 78.523 o 11 13 1 1.377 10.238 16.110 84.335 o 11 13 2 1.350 20.184 19.154 59.327 o 11 13 3 9.175 18.520 17.089 72.421 o 11 13 4 51.508 78.733 19.754 46.217 o 11 13 5 183.786 151.424 18.594 32.862 o 11 13 6 0.901 -20.919 10.415 204.838 o 11 13 7 371.670 413.093 34.665 10.040 o 11 13 8 274.398 265.632 20.661 21.425 o 11 13 9 44.606 36.811 16.539 66.597 o 11 13 10 131.726 185.526 25.462 24.161 o 11 13 11 8.527 11.778 16.727 76.386 o 11 13 12 6.608 8.877 16.830 76.310 o 11 13 13 3.899 12.697 17.480 71.085 o 11 13 14 88.019 70.661 23.230 33.235 o 11 13 15 9.814 7.533 25.247 34.445 o 11 13 16 112.719 100.991 25.797 26.258 o 11 14 0 11.127 -7.711 15.804 86.115 o 11 14 1 28.718 30.853 16.873 68.395 o 11 14 2 115.733 118.995 23.656 29.314 o 11 14 3 1.227 -8.343 13.917 114.921 o 11 14 4 99.049 108.946 17.627 46.214 o 11 14 5 0.099 9.744 12.345 142.686 o 11 14 6 1.751 -0.875 16.909 77.863 o 11 14 7 277.922 233.713 27.172 16.832 o 11 14 8 49.368 32.113 17.282 61.514 o 11 14 9 103.685 88.628 23.171 31.839 o 11 14 10 15.364 14.240 17.425 68.969 o 11 14 11 8.910 -9.297 17.260 73.153 o 11 14 12 0.981 18.247 20.765 50.830 o 11 14 13 117.305 159.686 26.713 23.571 o 11 14 14 9.406 3.931 19.901 55.076 o 11 14 15 3.459 30.863 22.844 41.504 o 11 15 2 14.923 18.294 20.632 49.947 o 11 15 3 9.547 -3.545 15.317 91.997 o 11 15 4 20.669 19.627 20.292 50.812 o 11 15 5 12.345 6.386 16.311 79.842 o 11 15 6 51.394 41.298 18.253 55.170 o 11 15 7 52.710 48.229 18.956 51.191 o 11 15 8 41.834 75.143 20.415 44.982 o 11 15 9 1.253 29.656 20.993 49.142 o 11 15 10 11.767 15.685 17.731 67.308 o 11 15 11 70.038 91.402 22.251 36.141 o 11 15 12 69.820 78.371 28.048 24.800 o 11 15 13 18.890 8.705 20.630 50.050 o 11 15 14 2.113 -21.682 21.548 48.015 o 11 16 5 58.107 33.897 23.939 34.492 o 11 16 6 9.613 14.543 17.991 65.982 o 11 16 7 33.867 33.743 18.386 57.770 o 11 16 8 151.806 128.113 23.772 26.977 o 11 16 9 40.367 12.112 17.460 63.997 o 11 16 10 41.861 8.903 18.291 59.004 o 11 16 11 101.510 143.176 25.695 25.993 o 11 16 12 63.816 98.522 31.665 19.923 o 12 -6 0 9.693 17.718 20.312 52.090 o 12 -6 1 247.129 279.122 37.942 11.113 o 12 -6 2 1.800 13.748 19.240 59.207 o 12 -6 3 73.882 64.966 23.290 34.170 o 12 -5 0 24.897 3.122 11.337 145.986 o 12 -5 1 31.165 34.749 15.657 76.587 o 12 -5 2 50.817 65.433 20.809 43.163 o 12 -5 3 33.938 16.078 18.484 58.599 o 12 -5 4 2.605 20.927 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94.318 o 12 -2 7 1.722 -6.513 14.624 103.920 o 12 -2 8 23.302 29.231 17.013 68.735 o 12 -2 9 7.987 42.322 18.478 60.683 o 12 -2 10 9.978 -15.471 16.880 76.132 o 12 -1 0 0.723 8.724 11.136 174.037 o 12 -1 1 116.484 140.845 16.451 45.535 o 12 -1 2 3.385 -3.246 10.736 189.210 o 12 -1 3 8.962 12.243 10.293 186.816 o 12 -1 4 20.519 8.237 11.358 147.229 o 12 -1 5 33.786 20.714 11.447 128.931 o 12 -1 6 551.158 597.546 40.566 6.381 o 12 -1 7 0.033 9.351 16.600 80.004 o 12 -1 8 116.168 113.817 28.187 22.488 o 12 -1 9 34.145 49.243 17.723 60.160 o 12 -1 10 5.898 -12.302 13.975 111.575 o 12 -1 11 0.338 17.582 18.241 65.640 o 12 0 0 90.626 81.577 14.964 60.800 o 12 0 1 23.718 6.717 9.530 192.565 o 12 0 2 6.574 1.282 12.083 146.741 o 12 0 3 60.662 35.303 16.602 63.012 o 12 0 4 250.733 276.391 27.897 16.488 o 12 0 5 4.079 11.325 11.679 154.071 o 12 0 6 264.683 215.547 22.041 21.706 o 12 0 7 7.771 1.609 12.436 137.785 o 12 0 8 3.226 16.553 16.317 80.880 o 12 0 9 75.832 51.802 28.328 24.611 o 12 0 10 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8.042 15.556 15.113 92.125 o 12 10 14 0.186 -5.742 13.983 114.386 o 12 10 15 5.180 -6.480 17.514 71.883 o 12 10 16 120.002 139.775 27.526 22.773 o 12 11 0 36.685 45.212 21.065 44.567 o 12 11 1 108.697 121.938 20.268 36.884 o 12 11 2 42.371 43.875 16.600 65.920 o 12 11 3 48.377 57.705 21.260 42.206 o 12 11 4 4.193 13.742 15.414 90.371 o 12 11 5 6.443 6.355 13.997 109.357 o 12 11 6 17.952 16.097 18.182 63.068 o 12 11 7 96.431 77.024 17.885 47.757 o 12 11 8 68.813 46.825 16.691 59.804 o 12 11 9 30.561 17.351 14.012 95.704 o 12 11 10 138.107 95.760 18.450 39.974 o 12 11 11 116.866 108.113 20.320 36.650 o 12 11 12 98.073 108.722 19.173 41.470 o 12 11 13 248.959 249.327 41.858 9.733 o 12 11 14 138.059 101.024 24.738 26.798 o 12 11 15 50.693 45.465 22.956 37.240 o 12 12 0 33.066 -7.781 21.520 45.274 o 12 12 1 3.555 -15.375 15.112 96.659 o 12 12 2 8.011 16.284 16.551 77.503 o 12 12 3 0.096 -16.002 15.931 88.177 o 12 12 4 0.784 16.425 17.176 73.831 o 12 12 5 6.770 9.672 14.839 96.984 o 12 12 6 44.645 26.381 16.151 70.427 o 12 12 7 29.394 -5.207 13.868 101.739 o 12 12 8 214.710 222.141 23.803 21.934 o 12 12 9 8.209 21.148 15.930 82.559 o 12 12 10 28.761 9.948 15.245 84.657 o 12 12 11 51.930 3.498 14.727 83.077 o 12 12 12 24.286 19.628 16.526 73.276 o 12 12 13 57.953 44.245 18.084 54.777 o 12 12 14 106.798 52.005 31.388 19.788 o 12 12 15 8.063 31.452 19.210 57.215 o 12 13 1 74.933 97.178 19.644 43.050 o 12 13 2 12.618 16.686 17.590 68.062 o 12 13 3 205.793 215.737 29.917 16.877 o 12 13 4 1.982 31.893 26.500 31.143 o 12 13 5 284.541 241.220 31.975 13.684 o 12 13 6 8.800 19.958 15.279 89.246 o 12 13 7 28.412 53.356 16.437 69.035 o 12 13 8 76.751 74.708 18.328 48.860 o 12 13 9 77.216 67.242 17.866 51.178 o 12 13 10 114.361 120.732 22.853 30.852 o 12 13 11 0.089 5.398 17.194 75.085 o 12 13 12 7.372 -18.063 15.989 85.333 o 12 13 13 1.813 -2.245 17.338 74.062 o 12 13 14 0.225 -4.018 17.212 75.515 o 12 14 2 0.213 -10.438 18.857 62.924 o 12 14 3 2.401 27.191 22.879 41.594 o 12 14 4 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0 6 20.403 10.278 12.318 127.435 o 13 0 7 0.247 5.142 10.836 186.599 o 13 0 8 17.982 7.283 18.145 64.077 o 13 0 9 33.619 53.097 23.884 35.533 o 13 0 10 17.049 4.760 19.458 56.441 o 13 1 0 4.864 3.376 10.205 203.351 o 13 1 1 15.107 -6.887 16.586 77.459 o 13 1 2 47.116 29.968 14.470 82.605 o 13 1 3 7.765 6.513 14.765 98.142 o 13 1 4 29.300 34.583 14.616 86.511 o 13 1 5 91.745 72.004 16.638 53.767 o 13 1 6 51.668 48.926 14.652 76.703 o 13 1 7 81.943 67.974 19.156 45.547 o 13 1 8 98.351 88.569 16.175 53.216 o 13 1 9 76.049 86.332 26.122 27.602 o 13 1 10 17.312 -1.963 19.510 56.440 o 13 1 11 14.910 32.657 22.989 40.118 o 13 2 0 8.680 -9.454 13.380 119.759 o 13 2 1 93.769 76.199 18.004 47.732 o 13 2 2 7.418 9.292 14.017 107.870 o 13 2 3 28.055 10.794 12.206 123.872 o 13 2 4 12.220 -33.762 12.440 134.901 o 13 2 5 34.620 38.345 19.254 52.870 o 13 2 6 0.078 10.050 13.523 119.389 o 13 2 7 3.818 -9.924 13.836 114.858 o 13 2 8 65.617 45.159 17.487 56.413 o 13 2 9 1.755 10.354 12.322 141.568 o 13 2 10 22.893 19.333 14.085 97.654 o 13 2 11 5.496 14.730 29.902 24.711 o 13 2 12 36.591 17.180 20.642 47.654 o 13 3 0 69.020 71.916 21.409 39.316 o 13 3 1 62.639 71.136 17.891 52.929 o 13 3 2 52.589 67.967 22.766 36.854 o 13 3 3 209.307 215.449 24.692 21.375 o 13 3 4 50.290 30.619 20.238 47.126 o 13 3 5 57.172 56.851 22.614 37.346 o 13 3 6 0.249 -3.166 14.399 107.858 o 13 3 7 32.309 13.596 15.271 82.719 o 13 3 8 47.518 56.250 17.883 56.469 o 13 3 9 18.084 0.441 15.117 91.202 o 13 3 10 92.175 74.140 16.217 55.348 o 13 3 11 15.121 15.430 13.612 108.360 o 13 3 12 30.248 31.921 14.182 91.052 o 13 4 0 192.097 210.278 25.046 21.763 o 13 4 1 2.213 2.734 13.866 114.502 o 13 4 2 67.465 81.200 19.101 46.674 o 13 4 3 17.235 -8.859 12.593 128.286 o 13 4 4 133.650 116.761 18.589 38.995 o 13 4 5 60.757 60.783 19.435 47.408 o 13 4 6 163.367 191.290 25.184 23.105 o 13 4 7 33.692 16.525 15.612 78.805 o 13 4 8 309.325 336.623 37.234 10.352 o 13 4 9 18.653 -1.119 12.824 123.184 o 13 4 10 118.590 104.091 18.931 40.271 o 13 4 11 50.079 62.196 18.369 53.256 o 13 4 12 0.020 -6.846 13.132 129.804 o 13 4 13 72.663 100.779 35.524 16.042 o 13 5 0 7.306 -10.128 11.435 162.937 o 13 5 1 119.773 129.211 24.253 27.793 o 13 5 2 73.485 75.865 23.163 34.153 o 13 5 3 10.022 13.613 14.885 94.415 o 13 5 4 15.342 26.692 14.742 91.614 o 13 5 5 148.796 208.439 22.048 27.613 o 13 5 6 0.009 1.895 10.720 193.348 o 13 5 7 135.852 145.107 37.487 13.498 o 13 5 8 0.006 8.171 14.692 101.964 o 13 5 9 12.545 14.711 15.781 83.686 o 13 5 10 51.160 76.548 18.992 49.400 o 13 5 11 26.694 32.005 16.432 71.951 o 13 5 12 3.496 -3.682 14.001 112.391 o 13 5 13 9.643 12.001 17.205 72.112 o 13 5 14 4.818 -15.012 23.373 40.652 o 13 6 0 38.175 30.637 15.959 72.903 o 13 6 1 105.392 120.882 21.133 35.124 o 13 6 2 71.823 94.607 18.907 46.060 o 13 6 3 3.595 -20.324 12.004 151.932 o 13 6 4 90.416 87.506 21.846 35.811 o 13 6 5 0.209 11.828 14.198 108.070 o 13 6 6 75.843 93.501 17.487 51.024 o 13 6 7 33.691 17.979 14.712 86.927 o 13 6 8 27.255 31.263 17.780 62.627 o 13 6 9 12.386 3.549 15.806 85.161 o 13 6 10 225.531 300.480 36.464 11.895 o 13 6 11 3.067 13.999 18.578 63.180 o 13 6 12 218.786 269.925 29.376 16.328 o 13 6 13 63.301 89.855 21.478 38.845 o 13 6 14 7.362 26.070 19.522 55.957 o 13 7 0 206.542 223.833 22.723 23.401 o 13 7 1 28.890 22.052 15.656 78.994 o 13 7 2 86.625 67.382 20.233 41.498 o 13 7 3 69.100 81.429 19.149 46.286 o 13 7 4 21.544 17.623 14.527 93.392 o 13 7 5 14.953 1.531 14.136 104.453 o 13 7 6 11.563 4.934 14.004 107.113 o 13 7 7 5.041 2.872 12.944 129.082 o 13 7 8 93.726 85.752 16.076 54.670 o 13 7 9 28.463 29.974 11.255 132.814 o 13 7 10 66.030 36.972 19.592 47.570 o 13 7 11 67.238 86.255 22.182 36.719 o 13 7 12 100.874 78.960 22.519 33.759 o 13 7 13 129.954 148.480 27.390 22.454 o 13 7 14 77.515 97.623 28.052 24.210 o 13 8 0 1.439 12.385 13.306 121.678 o 13 8 1 76.751 67.090 18.901 47.151 o 13 8 2 13.203 5.544 15.072 92.544 o 13 8 3 147.328 182.238 27.942 20.701 o 13 8 4 13.654 -4.828 13.142 120.842 o 13 8 5 77.523 52.834 18.344 50.164 o 13 8 6 10.441 -1.705 13.523 116.346 o 13 8 7 56.524 90.646 19.305 46.647 o 13 8 8 0.305 5.869 14.807 100.757 o 13 8 9 50.495 50.898 18.738 52.296 o 13 8 10 42.460 11.467 12.793 106.366 o 13 8 11 36.717 14.383 11.675 125.297 o 13 8 12 57.730 42.778 20.089 46.239 o 13 8 13 60.093 70.359 21.671 39.343 o 13 8 14 25.237 33.060 20.769 47.479 o 13 9 0 2.385 8.062 17.300 73.369 o 13 9 1 55.667 39.633 17.723 57.322 o 13 9 2 28.761 30.551 18.082 60.596 o 13 9 3 16.132 11.235 22.318 43.188 o 13 9 4 8.047 12.743 15.161 92.079 o 13 9 5 9.382 -3.230 15.161 93.894 o 13 9 6 0.489 -10.082 21.727 47.378 o 13 9 7 52.431 55.352 17.832 56.013 o 13 9 8 26.771 58.055 18.253 57.693 o 13 9 9 3.743 2.937 16.153 84.273 o 13 9 10 4.241 11.391 15.069 94.791 o 13 9 11 0.107 19.363 14.115 107.536 o 13 9 12 36.221 24.789 14.358 88.343 o 13 9 13 13.276 -2.380 15.312 90.765 o 13 9 14 73.314 66.986 19.753 44.466 o 13 10 0 15.365 37.546 23.054 39.697 o 13 10 1 2.141 -5.990 14.573 104.462 o 13 10 2 67.725 56.881 18.821 49.237 o 13 10 3 4.187 -13.387 16.328 82.789 o 13 10 4 21.741 5.064 15.774 82.449 o 13 10 5 121.489 113.025 21.151 34.157 o 13 10 6 7.139 11.264 15.823 85.411 o 13 10 7 118.774 149.342 23.623 28.385 o 13 10 8 9.135 -5.179 14.794 98.537 o 13 10 9 382.297 466.044 42.936 7.532 o 13 10 10 9.801 18.665 16.244 79.495 o 13 10 11 145.488 148.653 24.550 25.624 o 13 10 12 45.802 50.504 17.246 60.683 o 13 10 13 5.448 22.128 17.453 69.988 o 13 10 14 12.345 -12.086 15.816 85.622 o 13 11 0 17.499 26.085 21.622 45.101 o 13 11 1 30.274 52.916 33.090 19.453 o 13 11 2 13.859 30.991 18.224 62.219 o 13 11 3 126.337 83.492 21.173 34.859 o 13 11 4 56.180 65.330 19.602 47.028 o 13 11 5 65.361 28.826 18.973 50.728 o 13 11 6 11.901 25.185 17.039 71.468 o 13 11 7 174.769 215.465 24.998 22.386 o 13 11 8 39.767 35.385 17.259 63.149 o 13 11 9 170.593 213.422 24.733 22.896 o 13 11 10 5.645 -0.786 14.196 108.327 o 13 11 11 19.221 11.680 15.681 83.107 o 13 11 12 3.993 46.130 29.652 24.745 o 13 11 13 14.143 19.706 16.677 74.481 o 13 11 14 35.357 35.006 19.644 51.156 o 13 12 1 6.444 18.530 21.707 46.094 o 13 12 2 43.780 18.616 17.397 63.130 o 13 12 3 3.057 26.237 20.028 53.806 o 13 12 4 13.770 13.242 17.476 69.020 o 13 12 5 12.484 -5.105 14.565 100.117 o 13 12 6 66.493 88.796 22.987 34.616 o 13 12 7 0.946 -4.100 13.964 114.303 o 13 12 8 35.664 24.732 18.108 59.772 o 13 12 9 106.172 122.933 27.108 24.119 o 13 12 10 17.739 11.694 19.067 58.061 o 13 12 11 29.754 -1.144 21.131 47.171 o 13 12 12 9.366 -20.793 18.122 66.434 o 13 12 13 52.358 97.275 23.840 33.186 o 13 13 3 39.915 41.785 21.533 42.729 o 13 13 4 14.122 27.214 19.152 56.981 o 13 13 5 49.266 43.383 21.764 41.071 o 13 13 6 5.467 -15.799 18.647 63.479 o 13 13 7 41.449 5.406 22.607 40.431 o 13 13 8 87.890 73.543 27.061 25.795 o 13 13 9 165.028 177.132 34.577 14.717 o 13 13 10 111.693 180.794 51.460 7.741 o 13 13 11 35.264 40.479 27.108 28.359 o 13 13 12 88.786 78.995 28.428 23.605 o 13 14 6 9.869 21.354 25.570 33.266 o 13 14 7 116.287 138.407 30.256 19.735 o 13 14 8 38.112 9.709 24.137 35.877 o 13 14 9 2.173 -31.346 19.045 61.386 o 13 14 10 14.506 30.411 27.084 29.395 o 14 -2 1 8.562 -12.299 24.783 35.991 o 14 -2 2 0.110 -3.728 42.410 12.446 o 14 -1 0 19.462 52.426 18.241 59.391 o 14 -1 1 0.370 -33.029 30.625 23.860 o 14 -1 2 77.022 61.564 24.256 31.850 o 14 -1 3 10.505 20.735 16.261 78.870 o 14 -1 4 59.281 59.592 19.608 46.979 o 14 -1 5 5.784 10.270 16.535 78.993 o 14 0 0 16.600 6.334 19.589 55.677 o 14 0 1 76.017 116.608 32.380 18.709 o 14 0 2 10.603 15.410 24.323 36.785 o 14 0 3 0.086 -9.545 17.667 71.702 o 14 0 4 32.804 44.771 17.846 60.068 o 14 0 5 1.793 8.618 23.796 39.151 o 14 0 6 9.838 -2.725 16.224 82.244 o 14 0 7 49.689 17.447 22.278 40.411 o 14 1 0 3.887 8.382 17.678 69.982 o 14 1 1 137.155 137.223 22.601 29.456 o 14 1 2 17.642 30.057 20.305 50.506 o 14 1 3 2.618 -15.552 19.704 57.312 o 14 1 4 15.886 18.198 16.900 72.445 o 14 1 5 1.713 -5.337 14.291 108.793 o 14 1 6 28.677 15.535 17.640 64.716 o 14 1 7 45.848 42.822 16.288 67.315 o 14 1 8 14.376 9.792 15.699 84.692 o 14 2 0 0.266 -3.993 16.238 84.820 o 14 2 1 1.184 -12.182 14.092 112.126 o 14 2 2 23.623 34.504 17.750 63.185 o 14 2 3 293.292 276.342 33.530 12.471 o 14 2 4 68.054 38.964 19.762 46.559 o 14 2 5 20.059 31.777 18.030 62.297 o 14 2 6 17.780 9.683 19.591 55.289 o 14 2 7 45.179 33.069 16.287 68.567 o 14 2 8 57.472 51.510 17.357 57.914 o 14 2 9 14.951 38.249 18.524 59.617 o 14 3 0 0.349 -16.003 15.510 92.938 o 14 3 1 96.118 52.107 18.397 47.544 o 14 3 2 168.561 178.800 30.349 17.852 o 14 3 3 97.466 98.375 18.860 43.043 o 14 3 4 157.467 238.542 33.686 14.926 o 14 3 5 6.877 -4.520 20.529 52.340 o 14 3 6 15.981 -2.916 17.726 68.055 o 14 3 7 27.576 31.158 18.510 58.266 o 14 3 8 11.773 -10.039 13.564 114.944 o 14 3 9 131.998 115.286 23.131 29.454 o 14 3 10 1.191 -4.143 16.551 81.400 o 14 4 0 153.118 148.832 26.165 23.134 o 14 4 1 0.738 -7.617 16.728 79.813 o 14 4 2 0.127 6.840 17.124 75.514 o 14 4 3 21.709 -5.748 16.237 78.868 o 14 4 4 24.508 36.838 15.397 80.405 o 14 4 5 1.108 -9.771 17.229 75.158 o 14 4 6 89.458 64.340 22.495 35.102 o 14 4 7 48.306 42.691 20.181 46.911 o 14 4 8 3.116 -5.372 16.791 78.616 o 14 4 9 0.269 -0.819 22.614 43.755 o 14 4 10 37.586 56.722 20.855 44.704 o 14 4 11 1.419 34.320 26.415 31.311 o 14 5 0 44.268 23.185 19.006 53.797 o 14 5 1 251.162 303.458 30.337 14.640 o 14 5 2 52.617 50.191 18.102 55.048 o 14 5 3 17.462 -14.303 14.575 97.938 o 14 5 4 74.603 109.184 19.974 41.428 o 14 5 5 41.656 32.638 15.441 75.731 o 14 5 6 64.612 48.465 30.950 21.326 o 14 5 7 40.956 65.099 23.904 34.675 o 14 5 8 17.374 11.402 17.655 67.180 o 14 5 9 19.167 10.287 18.215 63.147 o 14 5 10 0.731 -11.049 17.730 71.065 o 14 5 11 76.167 85.983 25.567 28.617 o 14 6 0 48.342 54.967 19.488 49.029 o 14 6 1 126.593 101.141 26.148 25.137 o 14 6 2 39.752 33.387 18.349 57.076 o 14 6 3 204.310 216.538 26.401 19.875 o 14 6 4 0.289 -18.128 13.821 117.039 o 14 6 5 20.983 14.920 15.281 86.006 o 14 6 6 0.017 -26.983 11.865 159.004 o 14 6 7 11.466 37.789 19.610 54.174 o 14 6 8 10.549 14.011 18.440 62.834 o 14 6 9 70.231 92.818 23.627 32.745 o 14 6 10 77.278 84.226 24.632 30.432 o 14 6 11 3.256 11.234 21.393 48.065 o 14 6 12 69.466 87.898 34.925 16.692 o 14 7 0 42.624 43.085 30.016 23.202 o 14 7 1 37.106 21.881 20.794 46.730 o 14 7 2 1.535 -46.593 13.748 117.586 o 14 7 3 119.246 115.877 21.785 32.851 o 14 7 4 10.128 -9.569 15.468 90.076 o 14 7 5 9.496 -27.111 13.376 119.338 o 14 7 6 2.841 -12.846 17.767 70.348 o 14 7 7 0.738 -10.508 13.460 123.116 o 14 7 8 0.030 -6.046 13.277 126.969 o 14 7 9 0.399 -10.941 17.286 74.827 o 14 7 10 0.273 -7.570 17.263 75.059 o 14 7 11 0.008 20.014 20.154 53.897 o 14 7 12 0.100 -2.371 21.328 49.201 o 14 8 0 0.057 41.248 24.276 36.787 o 14 8 1 16.335 33.875 18.273 61.254 o 14 8 2 0.346 -32.064 15.094 98.127 o 14 8 3 53.652 50.685 19.459 48.763 o 14 8 4 28.997 31.419 18.113 60.298 o 14 8 5 13.548 13.821 16.635 75.700 o 14 8 6 91.643 69.591 19.374 43.622 o 14 8 7 6.055 -12.842 14.595 102.450 o 14 8 8 16.409 13.082 18.363 62.422 o 14 8 9 45.067 59.804 15.927 67.933 o 14 8 10 93.214 120.737 26.010 26.326 o 14 8 11 141.730 157.385 43.400 10.386 o 14 8 12 0.357 21.880 22.289 44.141 o 14 9 0 22.610 16.106 23.818 37.545 o 14 9 1 0.829 -14.583 16.760 79.479 o 14 9 2 19.879 29.103 18.171 61.688 o 14 9 3 188.558 250.608 32.908 14.780 o 14 9 4 49.215 65.818 21.248 41.807 o 14 9 5 58.812 85.509 22.088 37.639 o 14 9 6 2.217 -20.421 14.652 103.320 o 14 9 7 0.200 0.442 16.172 85.475 o 14 9 8 9.992 16.598 15.525 86.783 o 14 9 9 0.186 -12.184 13.607 120.802 o 14 9 10 23.854 37.877 16.945 68.182 o 14 9 11 2.010 -1.362 16.559 81.100 o 14 9 12 22.869 34.540 20.999 46.690 o 14 10 1 1.818 -31.058 21.329 49.033 o 14 10 2 13.614 31.024 21.703 44.910 o 14 10 3 0.454 15.414 21.165 49.157 o 14 10 4 76.210 82.638 21.888 36.963 o 14 10 5 20.471 4.218 17.045 71.849 o 14 10 6 83.459 71.697 21.172 38.794 o 14 10 7 5.152 13.349 18.167 65.675 o 14 10 8 108.366 89.534 21.499 35.232 o 14 10 9 8.148 -5.460 16.111 83.844 o 14 10 10 40.179 87.412 20.667 43.625 o 14 10 11 5.088 6.409 17.627 70.336 o 14 10 12 10.296 16.485 20.912 49.258 o 14 11 3 0.037 -16.496 22.502 44.206 o 14 11 4 38.733 9.234 21.308 45.148 o 14 11 5 61.293 52.674 24.904 31.503 o 14 11 6 203.213 196.691 92.425 2.501 o 14 11 7 34.941 49.488 22.249 40.407 o 14 11 8 0.056 -21.498 16.363 83.592 o 14 11 9 62.030 18.835 18.712 53.040 o 14 11 10 63.374 91.494 21.818 37.808 o 14 11 11 1.664 10.481 18.103 67.022 o 14 12 5 61.553 96.915 25.367 29.428 o 14 12 6 53.699 27.766 20.156 47.239 o 14 12 7 2.341 -4.758 18.234 66.904 o 14 12 8 199.926 156.383 30.819 16.994 o 14 12 9 9.568 23.708 19.440 56.267 o 14 12 10 144.385 126.242 38.641 12.829 o 15 2 3 100.003 99.039 32.412 18.367 o 15 2 4 0.233 2.330 79.693 3.524 o 15 3 1 0.420 -23.758 18.880 62.732 o 15 3 2 0.076 -8.916 19.521 58.731 o 15 3 3 0.417 -17.499 14.831 101.604 o 15 3 4 0.869 -4.111 22.874 42.720 o 15 3 5 30.692 15.409 21.526 44.766 o 15 3 6 1.650 2.490 21.478 48.256 o 15 4 1 0.018 0.662 18.988 62.038 o 15 4 2 0.738 0.975 16.559 81.308 o 15 4 3 75.191 62.374 19.346 45.969 o 15 4 4 15.377 -5.172 21.176 48.392 o 15 4 5 78.355 99.101 32.078 19.154 o 15 4 6 2.820 -0.820 21.490 48.208 o 15 4 7 0.012 34.002 23.261 40.204 o 15 5 1 82.346 70.702 23.629 32.677 o 15 5 2 17.258 7.036 19.474 56.171 o 15 5 3 3.280 -23.468 15.782 88.826 o 15 5 4 0.145 -28.212 16.085 86.474 o 15 5 5 1.271 -1.170 21.713 47.367 o 15 5 6 4.924 -8.540 21.256 49.063 o 15 5 7 23.714 23.757 30.806 22.775 o 15 5 8 34.691 63.321 24.111 34.567 o 15 6 2 0.157 -25.300 16.977 77.631 o 15 6 3 2.218 -1.247 18.229 66.964 o 15 6 4 29.528 22.061 18.177 60.613 o 15 6 5 0.740 0.263 15.421 93.830 o 15 6 6 0.135 -14.001 19.007 61.946 o 15 6 7 0.047 -10.398 19.384 59.573 o 15 6 8 18.111 -7.183 19.342 57.272 o 15 7 2 9.644 18.395 21.657 46.015 o 15 7 3 36.400 18.344 19.473 52.889 o 15 7 4 0.322 -16.191 16.989 77.478 o 15 7 5 57.150 30.783 18.710 52.895 o 15 7 6 1.708 -23.338 16.327 83.496 o 15 7 7 14.027 24.930 16.766 73.169 o 15 7 8 29.666 -0.899 20.188 51.399 o 15 8 3 5.380 9.441 21.776 46.307 o 15 8 4 6.655 0.894 18.665 63.087 o 15 8 5 2.396 -8.848 16.969 77.162 o 15 8 6 1.544 -7.244 16.433 82.474 o 15 8 7 12.068 11.343 21.106 48.468 o 15 8 8 7.720 2.334 16.689 78.104 o 15 9 5 154.705 167.050 33.131 16.014 o 15 9 6 1.405 -0.048 19.189 60.590 o 15 9 7 3.533 -19.374 17.005 76.565 o ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy K1 K 0.13409(5) 0.32727(4) 0.22595(4) 0.03502(16) Uani 1.000000 O1 O 0.11191(19) 0.28317(16) 0.41839(13) 0.0505(5) Uani 1.000000 O12 O 0.10754(16) 0.54173(13) 0.12824(13) 0.0410(5) Uani 1.000000 O8 O -0.21050(17) 0.39871(13) 0.06245(12) 0.0412(5) Uani 1.000000 O7 O -0.09083(16) 0.45794(14) 0.16061(14) 0.0428(5) Uani 1.000000 O5 O 0.35806(17) 0.34793(15) 0.12878(14) 0.0476(5) Uani 1.000000 O4 O 0.20503(19) 0.27405(14) 0.07474(13) 0.0484(5) Uani 1.000000 O3 O 0.12687(18) 0.12784(14) 0.23700(14) 0.0463(5) Uani 1.000000 O2 O -0.03361(18) 0.21242(16) 0.35651(14) 0.0493(5) Uani 1.000000 O6 O 0.33436(18) 0.30209(14) 0.31737(13) 0.0449(5) Uani 1.000000 C6 C 0.6737(3) 0.0753(3) 0.4628(3) 0.0630(9) Uani 1.000000 H6 H 0.6835(3) 0.0401(3) 0.4244(3) 0.0756(11) Uiso 1.000000 C7 C 0.6838(3) 0.0205(2) 0.5559(2) 0.0563(9) Uani 1.000000 H7 H 0.7016(3) -0.0518(2) 0.5802(2) 0.0676(10) Uiso 1.000000 C8 C 0.6674(3) 0.0741(2) 0.6125(2) 0.0424(7) Uani 1.000000 H8 H 0.6757(3) 0.0370(2) 0.6746(2) 0.0509(8) Uiso 1.000000 C3 C 0.6387(2) 0.1816(2) 0.57821(18) 0.0331(6) Uani 1.000000 C2 C 0.6175(2) 0.23934(18) 0.64056(17) 0.0286(5) Uani 1.000000 C1 C 0.4778(2) 0.25951(17) 0.70312(15) 0.0256(5) Uani 1.000000 B1 B 0.3766(2) 0.2198(2) 0.68366(19) 0.0265(6) Uani 1.000000 H1 H 0.4094(2) 0.2001(2) 0.63048(19) 0.0318(7) Uiso 1.000000 C16 C 0.2510(2) 0.30357(18) 0.66005(16) 0.0274(5) Uani 1.000000 C11 C 0.1525(2) 0.26114(18) 0.70444(16) 0.0283(5) Uani 1.000000 C12 C 0.0371(2) 0.3155(2) 0.68888(18) 0.0342(6) Uani 1.000000 H12 H -0.0256(2) 0.2840(2) 0.71977(18) 0.0411(7) Uiso 1.000000 C13 C 0.0171(2) 0.4173(2) 0.62658(18) 0.0363(6) Uani 1.000000 H13 H -0.0597(2) 0.4554(2) 0.61544(18) 0.0435(7) Uiso 1.000000 C4 C 0.6309(3) 0.2358(2) 0.48430(19) 0.0432(7) Uani 1.000000 H4 H 0.6136(3) 0.3081(2) 0.45962(19) 0.0518(8) Uiso 1.000000 C5 C 0.6491(3) 0.1820(3) 0.4277(2) 0.0566(9) Uani 1.000000 H5 H 0.6446(3) 0.2187(3) 0.3650(2) 0.0679(10) Uiso 1.000000 C9 C 0.3307(2) 0.11832(17) 0.76811(16) 0.0275(5) Uani 1.000000 C15 C 0.2270(2) 0.40665(18) 0.59638(17) 0.0301(6) Uani 1.000000 H15 H 0.2893(2) 0.43818(18) 0.56405(17) 0.0361(7) Uiso 1.000000 C14 C 0.1119(2) 0.4624(2) 0.58080(18) 0.0360(6) Uani 1.000000 H14 H 0.0982(2) 0.5310(2) 0.53900(18) 0.0432(7) Uiso 1.000000 C10 C 0.1837(2) 0.15161(18) 0.77052(17) 0.0277(5) Uani 1.000000 C17 C 0.2118(3) 0.2657(2) 0.4599(2) 0.0518(8) Uani 1.000000 H17a H 0.1869(3) 0.2824(2) 0.5145(2) 0.0622(10) Uiso 1.000000 H17b H 0.2531(3) 0.1930(2) 0.4785(2) 0.0622(10) Uiso 1.000000 C40 C 0.1952(3) 0.6010(2) 0.0874(2) 0.0440(7) Uani 1.000000 H40a H 0.2725(3) 0.5538(2) 0.0966(2) 0.0528(8) Uiso 1.000000 H40b H 0.1849(3) 0.6466(2) 0.1195(2) 0.0528(8) Uiso 1.000000 C39 C 0.1931(3) 0.6661(2) -0.01389(19) 0.0416(7) Uani 1.000000 H39a H 0.1176(3) 0.7161(2) -0.02416(19) 0.0499(8) Uiso 1.000000 H39b H 0.2549(3) 0.7039(2) -0.03609(19) 0.0499(8) Uiso 1.000000 C32 C -0.1882(3) 0.3422(2) 0.15553(19) 0.0437(7) Uani 1.000000 H32a H -0.1111(3) 0.2943(2) 0.15834(19) 0.0525(8) Uiso 1.000000 H32b H -0.2472(3) 0.3021(2) 0.18933(19) 0.0525(8) Uiso 1.000000 C31 C -0.1924(3) 0.4164(2) 0.19771(19) 0.0432(7) Uani 1.000000 H31a H -0.2633(3) 0.4720(2) 0.18471(19) 0.0518(8) Uiso 1.000000 H31b H -0.1943(3) 0.3806(2) 0.26394(19) 0.0518(8) Uiso 1.000000 C101 C 0.4134(3) 0.3621(2) 0.2526(2) 0.0525(8) Uani 1.000000 H10a H 0.4802(3) 0.3529(2) 0.2819(2) 0.0630(10) Uiso 1.000000 H10b H 0.3733(3) 0.4352(2) 0.2312(2) 0.0630(10) Uiso 1.000000 C26 C 0.4560(3) 0.3289(3) 0.1730(2) 0.0569(9) Uani 1.000000 H26a H 0.5127(3) 0.3676(3) 0.1302(2) 0.0683(10) Uiso 1.000000 H26b H 0.4946(3) 0.2555(3) 0.1943(2) 0.0683(10) Uiso 1.000000 C25 C 0.3893(3) 0.3282(3) 0.0458(2) 0.0592(9) Uani 1.000000 H25a H 0.4385(3) 0.2585(3) 0.0579(2) 0.0711(11) Uiso 1.000000 H25b H 0.4337(3) 0.3771(3) -0.0000(2) 0.0711(11) Uiso 1.000000 C24 C 0.2795(3) 0.3394(2) 0.0112(2) 0.0571(9) Uani 1.000000 H24a H 0.3012(3) 0.3246(2) -0.0442(2) 0.0685(11) Uiso 1.000000 H24b H 0.2350(3) 0.4112(2) -0.0055(2) 0.0685(11) Uiso 1.000000 C100 C 0.2556(3) 0.1652(2) 0.0977(2) 0.0519(8) Uani 1.000000 H10c H 0.3218(3) 0.1426(2) 0.1323(2) 0.0623(10) Uiso 1.000000 H10d H 0.2835(3) 0.1505(2) 0.0423(2) 0.0623(10) Uiso 1.000000 C22 C 0.1601(3) 0.1101(2) 0.1546(2) 0.0536(8) Uani 1.000000 H22a H 0.0924(3) 0.1358(2) 0.1209(2) 0.0643(10) Uiso 1.000000 H22b H 0.1886(3) 0.0361(2) 0.1683(2) 0.0643(10) Uiso 1.000000 C21 C 0.0310(3) 0.0821(2) 0.2941(2) 0.0501(8) Uani 1.000000 H21a H 0.0534(3) 0.0076(2) 0.3099(2) 0.0602(10) Uiso 1.000000 H21b H -0.0377(3) 0.1108(2) 0.2611(2) 0.0602(10) Uiso 1.000000 C20 C 0.0018(3) 0.1042(2) 0.3793(2) 0.0543(8) Uani 1.000000 H20a H -0.0614(3) 0.0719(2) 0.4190(2) 0.0651(10) Uiso 1.000000 H20b H 0.0705(3) 0.0752(2) 0.4123(2) 0.0651(10) Uiso 1.000000 C19 C -0.0683(3) 0.2418(3) 0.4349(2) 0.0610(9) Uani 1.000000 H19a H -0.1235(3) 0.2018(3) 0.4784(2) 0.0732(11) Uiso 1.000000 H19b H -0.1094(3) 0.3146(3) 0.4149(2) 0.0732(11) Uiso 1.000000 C18 C 0.0308(3) 0.2258(3) 0.4821(2) 0.0586(9) Uani 1.000000 H18a H 0.0022(3) 0.2489(3) 0.5330(2) 0.0703(11) Uiso 1.000000 H18b H 0.0695(3) 0.1525(3) 0.5066(2) 0.0703(11) Uiso 1.000000 C29 C -0.0093(3) 0.6031(2) 0.1167(2) 0.0436(7) Uani 1.000000 H29a H -0.0184(3) 0.6657(2) 0.1272(2) 0.0523(8) Uiso 1.000000 H29b H -0.0242(3) 0.6236(2) 0.0540(2) 0.0523(8) Uiso 1.000000 C30 C -0.0962(3) 0.5440(2) 0.1819(2) 0.0475(7) Uani 1.000000 H30a H -0.1752(3) 0.5888(2) 0.1775(2) 0.0570(9) Uiso 1.000000 H30b H -0.0786(3) 0.5196(2) 0.2444(2) 0.0570(9) Uiso 1.000000 C28 C 0.2919(3) 0.3311(2) 0.3944(2) 0.0508(8) Uani 1.000000 H28a H 0.3579(3) 0.3225(2) 0.4243(2) 0.0610(9) Uiso 1.000000 H28b H 0.2499(3) 0.4037(2) 0.3742(2) 0.0610(9) Uiso 1.000000 B15 B 0.5986(3) 0.1719(2) 0.7576(2) 0.0320(6) Uani 1.000000 H15a H 0.603(2) 0.093(2) 0.7846(18) 0.0384(8) Uiso 1.000000 B14 B 0.4976(3) 0.2590(2) 0.8048(2) 0.0318(6) Uani 1.000000 H14a H 0.438(2) 0.229(2) 0.8652(18) 0.0382(8) Uiso 1.000000 B18 B 0.6516(3) 0.2375(2) 0.8056(2) 0.0367(7) Uani 1.000000 H18 H 0.696(2) 0.193(2) 0.8677(19) 0.0440(8) Uiso 1.000000 B3 B 0.1117(3) 0.0967(2) 0.8761(2) 0.0361(7) Uani 1.000000 H3 H 0.029(2) 0.140(2) 0.8952(19) 0.0433(8) Uiso 1.000000 B8 B 0.2266(3) 0.0164(2) 0.9461(2) 0.0380(7) Uani 1.000000 H8a H 0.218(2) 0.001(2) 1.022(2) 0.0456(9) Uiso 1.000000 B11 B 0.3120(3) -0.0782(2) 0.8999(2) 0.0370(7) Uani 1.000000 H11 H 0.356(2) -0.156(2) 0.9428(19) 0.0444(9) Uiso 1.000000 B6 B 0.3796(3) -0.0120(2) 0.7876(2) 0.0331(7) Uani 1.000000 H6a H 0.467(2) -0.042(2) 0.7545(18) 0.0397(8) Uiso 1.000000 B4 B 0.1263(3) 0.0512(2) 0.7873(2) 0.0368(7) Uani 1.000000 H4a H 0.050(2) 0.074(2) 0.7501(19) 0.0441(8) Uiso 1.000000 B10 B 0.2499(3) -0.0564(2) 0.8016(2) 0.0380(7) Uani 1.000000 H10 H 0.251(2) -0.117(2) 0.7819(19) 0.0456(9) Uiso 1.000000 B9 B 0.1559(3) -0.0382(2) 0.8991(2) 0.0400(8) Uani 1.000000 H9 H 0.101(2) -0.085(2) 0.9393(19) 0.0480(9) Uiso 1.000000 B5 B 0.2639(3) 0.0661(2) 0.7191(2) 0.0324(7) Uani 1.000000 H5a H 0.267(2) 0.096(2) 0.6466(19) 0.0389(8) Uiso 1.000000 B2 B 0.2422(3) 0.1393(2) 0.8626(2) 0.0302(6) Uani 1.000000 H2 H 0.239(2) 0.212(2) 0.8704(17) 0.0362(7) Uiso 1.000000 B7 B 0.3644(3) 0.0329(2) 0.8766(2) 0.0332(7) Uani 1.000000 H7a H 0.446(2) 0.035(2) 0.8977(18) 0.0398(8) Uiso 1.000000 B12 B 0.5249(3) 0.3616(2) 0.6095(2) 0.0283(6) Uani 1.000000 H12a H 0.483(2) 0.3919(19) 0.5468(17) 0.0340(7) Uiso 1.000000 B16 B 0.5759(3) 0.4295(2) 0.6552(2) 0.0318(6) Uani 1.000000 H16 H 0.565(2) 0.516(2) 0.6212(17) 0.0382(8) Uiso 1.000000 B21 B 0.6995(3) 0.3446(2) 0.7130(2) 0.0364(7) Uani 1.000000 H21 H 0.769(2) 0.374(2) 0.7173(18) 0.0437(8) Uiso 1.000000 B20 B 0.6794(3) 0.3420(2) 0.6094(2) 0.0327(7) Uani 1.000000 H20 H 0.733(2) 0.361(2) 0.5459(19) 0.0393(8) Uiso 1.000000 B19 B 0.7252(3) 0.2242(2) 0.7016(2) 0.0353(7) Uani 1.000000 H19 H 0.806(2) 0.175(2) 0.6918(18) 0.0424(8) Uiso 1.000000 B17 B 0.5597(3) 0.3654(2) 0.7770(2) 0.0347(7) Uani 1.000000 H17 H 0.538(2) 0.406(2) 0.8229(18) 0.0417(8) Uiso 1.000000 B13 B 0.4514(3) 0.3771(2) 0.7127(2) 0.0298(6) Uani 1.000000 H13a H 0.359(2) 0.4232(19) 0.7118(17) 0.0358(7) Uiso 1.000000 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 K1 0.0394(3) 0.0327(3) 0.0337(3) -0.0086(2) -0.0042(3) -0.0134(2) O1 0.0608(14) 0.0588(13) 0.0394(11) -0.0275(11) 0.0026(10) -0.0211(10) O12 0.0418(11) 0.0326(10) 0.0425(11) -0.0042(8) -0.0055(9) -0.0115(8) O8 0.0545(12) 0.0293(9) 0.0390(11) -0.0071(9) -0.0093(9) -0.0124(8) O7 0.0397(11) 0.0398(10) 0.0546(12) -0.0077(9) -0.0026(9) -0.0262(9) O5 0.0408(12) 0.0498(12) 0.0464(12) -0.0049(9) 0.0013(9) -0.0201(10) O4 0.0709(15) 0.0315(10) 0.0398(11) -0.0003(10) -0.0131(10) -0.0157(9) O3 0.0595(13) 0.0384(11) 0.0456(12) -0.0107(10) -0.0137(10) -0.0171(9) O2 0.0559(13) 0.0499(12) 0.0439(12) -0.0213(10) 0.0007(10) -0.0169(10) O6 0.0539(13) 0.0396(11) 0.0467(12) -0.0111(9) -0.0115(10) -0.0189(9) C6 0.071(2) 0.067(2) 0.067(2) -0.0034(18) -0.0038(19) -0.052(2) C7 0.065(2) 0.0449(18) 0.066(2) -0.0052(16) -0.0033(18) -0.0351(17) C8 0.0462(17) 0.0369(15) 0.0441(17) -0.0047(13) -0.0007(13) -0.0215(13) C3 0.0281(13) 0.0388(14) 0.0342(14) -0.0074(11) 0.0039(11) -0.0199(12) C2 0.0263(13) 0.0268(12) 0.0298(13) -0.0033(10) -0.0009(10) -0.0113(10) C1 0.0259(12) 0.0261(12) 0.0234(12) -0.0058(10) 0.0020(10) -0.0109(10) B1 0.0303(15) 0.0248(13) 0.0242(14) -0.0080(11) -0.0009(11) -0.0095(11) C16 0.0315(13) 0.0274(12) 0.0260(12) -0.0071(10) -0.0029(10) -0.0128(10) C11 0.0308(13) 0.0269(12) 0.0283(13) -0.0067(10) -0.0021(11) -0.0123(10) C12 0.0295(14) 0.0373(14) 0.0378(15) -0.0099(11) -0.0021(12) -0.0158(12) C13 0.0298(14) 0.0361(14) 0.0417(15) 0.0001(11) -0.0114(12) -0.0154(12) C4 0.0453(17) 0.0434(16) 0.0362(15) -0.0029(13) 0.0011(13) -0.0192(13) C5 0.060(2) 0.070(2) 0.0393(17) -0.0005(17) -0.0052(15) -0.0304(17) C9 0.0277(13) 0.0243(12) 0.0304(13) -0.0045(10) -0.0014(10) -0.0125(10) C15 0.0328(14) 0.0282(12) 0.0299(13) -0.0088(10) -0.0052(11) -0.0098(11) C14 0.0398(16) 0.0287(13) 0.0366(14) -0.0047(11) -0.0119(12) -0.0083(11) C10 0.0270(13) 0.0272(12) 0.0321(13) -0.0095(10) 0.0004(10) -0.0140(10) C17 0.075(2) 0.0504(18) 0.0400(17) -0.0131(16) -0.0158(16) -0.0225(15) C40 0.0503(18) 0.0406(16) 0.0474(17) -0.0155(14) -0.0094(14) -0.0176(13) C39 0.0473(17) 0.0326(14) 0.0489(17) -0.0138(12) -0.0045(14) -0.0171(13) C32 0.0528(18) 0.0339(14) 0.0399(16) -0.0145(13) -0.0074(14) -0.0060(12) C31 0.0441(17) 0.0445(16) 0.0353(15) -0.0113(13) -0.0026(13) -0.0105(13) C101 0.0428(18) 0.0486(18) 0.069(2) -0.0163(14) -0.0156(16) -0.0167(16) C26 0.0406(18) 0.056(2) 0.067(2) -0.0092(15) -0.0033(16) -0.0199(17) C25 0.066(2) 0.058(2) 0.0456(18) -0.0117(17) 0.0159(17) -0.0250(16) C24 0.083(3) 0.0468(18) 0.0355(17) -0.0080(17) -0.0001(17) -0.0189(14) C100 0.072(2) 0.0366(15) 0.0433(17) 0.0082(15) -0.0180(16) -0.0207(14) C22 0.079(2) 0.0330(15) 0.0528(19) -0.0023(15) -0.0224(17) -0.0201(14) C21 0.0545(19) 0.0318(15) 0.066(2) -0.0148(14) -0.0207(16) -0.0101(14) C20 0.053(2) 0.0492(18) 0.0495(19) -0.0183(15) -0.0091(15) -0.0031(15) C19 0.060(2) 0.080(2) 0.0424(18) -0.0188(19) 0.0070(16) -0.0280(18) C18 0.071(2) 0.070(2) 0.0382(17) -0.0263(19) 0.0092(16) -0.0247(16) C29 0.0460(17) 0.0340(15) 0.0513(18) -0.0021(13) -0.0070(14) -0.0214(13) C30 0.0524(19) 0.0428(16) 0.0517(18) -0.0071(14) 0.0007(15) -0.0285(15) C28 0.063(2) 0.0472(17) 0.0541(19) -0.0074(15) -0.0210(16) -0.0270(15) B15 0.0314(16) 0.0306(15) 0.0294(15) -0.0066(12) -0.0036(12) -0.0077(12) B14 0.0393(17) 0.0342(15) 0.0246(14) -0.0122(13) -0.0029(13) -0.0117(12) B18 0.0386(18) 0.0371(16) 0.0356(16) -0.0104(14) -0.0103(14) -0.0111(14) B3 0.0373(18) 0.0289(15) 0.0369(17) -0.0119(13) 0.0086(14) -0.0116(13) B8 0.0474(19) 0.0283(15) 0.0331(16) -0.0125(14) 0.0027(14) -0.0084(13) B11 0.0464(19) 0.0261(15) 0.0342(16) -0.0107(13) 0.0014(14) -0.0092(13) B6 0.0406(18) 0.0219(13) 0.0347(16) -0.0077(12) 0.0033(14) -0.0126(12) B4 0.0353(17) 0.0309(15) 0.0486(19) -0.0152(13) -0.0010(15) -0.0164(14) B10 0.0471(19) 0.0262(15) 0.0446(18) -0.0155(13) 0.0027(15) -0.0166(14) B9 0.0440(19) 0.0312(16) 0.0459(19) -0.0197(14) 0.0094(15) -0.0161(14) B5 0.0406(18) 0.0293(15) 0.0330(16) -0.0118(13) -0.0004(13) -0.0169(13) B2 0.0350(16) 0.0261(14) 0.0280(14) -0.0083(12) -0.0001(12) -0.0101(12) B7 0.0414(18) 0.0254(14) 0.0294(15) -0.0083(13) -0.0034(13) -0.0074(12) B12 0.0293(15) 0.0240(13) 0.0293(15) -0.0062(11) -0.0008(12) -0.0094(12) B16 0.0325(16) 0.0291(15) 0.0348(16) -0.0092(12) -0.0030(13) -0.0124(13) B21 0.0310(16) 0.0376(16) 0.0416(17) -0.0113(13) -0.0072(14) -0.0125(14) B20 0.0316(16) 0.0315(15) 0.0340(16) -0.0100(12) 0.0005(13) -0.0119(13) B19 0.0260(15) 0.0347(16) 0.0426(18) -0.0042(13) -0.0070(14) -0.0129(14) B17 0.0403(18) 0.0355(16) 0.0347(16) -0.0129(13) -0.0041(14) -0.0169(13) B13 0.0325(16) 0.0281(14) 0.0316(15) -0.0066(12) -0.0032(13) -0.0146(12) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source B 0.00156 0.00068 2.05450 1.33260 1.09790 0.70680 23.21850 1.02100 60.34980 0.14030 -0.19320 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' C 0.00313 0.00162 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.21560 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.00304 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' K 0.20133 0.25084 8.21860 7.43980 1.05190 0.86590 12.79490 0.77480 213.18700 41.68410 1.42280 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' O 0.01085 0.00610 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.25080 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' loop_ _citation_id _citation_doi _citation_year 1 10.26434/chemrxiv-2025-04xgt 2025 loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u -2 0 0 120.64 5.52 -2 0 0 121.65 5.43 -2 0 0 118.31 5.42 -2 0 0 119.17 5.28 -2 0 0 119.25 5.34 -2 0 0 117.66 5.35 -2 0 0 118.62 5.36 2 0 0 114.85 5.5 2 0 0 114.65 5.41 2 0 0 111.28 5.39 2 0 0 117.38 5.25 2 0 0 112.35 5.32 2 0 0 121.65 5.39 2 0 0 114.25 5.34 -3 0 0 12.11 1.29 -3 0 0 11.3 1.1 -3 0 0 10.7 1.05 -3 0 0 11.73 0.86 -3 0 0 12.17 0.94 -3 0 0 11.33 0.94 -3 0 0 12.36 1.08 3 0 0 11.3 0.85 3 0 0 11.42 1.08 3 0 0 13.16 1.05 3 0 0 8.73 0.89 3 0 0 10.76 1.01 3 0 0 11.19 1.22 3 0 0 11.55 1.1 -4 0 0 42.87 2.64 -4 0 0 43.29 2.23 -4 0 0 43.89 2.37 -4 0 0 39.72 2.31 -4 0 0 37.93 2.42 -4 0 0 41.2 2.45 -4 0 0 39.93 2.34 4 0 0 43.64 2.5 4 0 0 38.26 2.58 4 0 0 41.88 2.44 4 0 0 42.67 2.19 4 0 0 43.76 2.31 4 0 0 42.38 2.42 4 0 0 41.07 2.34 -5 0 0 0.39 0.35 -5 0 0 -0.04 0.35 -5 0 0 0.44 0.41 -5 0 0 0.28 0.35 -5 0 0 0.41 0.4 -5 0 0 -0.31 0.34 -5 0 0 -0.33 0.46 5 0 0 0.07 0.36 5 0 0 0.06 0.41 5 0 0 0.05 0.41 5 0 0 0.78 0.55 5 0 0 0.4 0.32 5 0 0 -0.01 0.31 5 0 0 -0.6 0.23 -6 0 0 20.39 1.97 -6 0 0 17.01 1.43 -6 0 0 18.58 1.53 -6 0 0 17.65 1.36 -6 0 0 16.1 1.76 -6 0 0 20.59 2.24 -6 0 0 17.97 1.51 6 0 0 17.94 1.93 6 0 0 16.16 1.28 6 0 0 17.22 2.03 6 0 0 18.79 1.62 6 0 0 17 1.8 6 0 0 15.55 1.54 -7 0 0 1.32 0.52 -7 0 0 0.83 0.56 -7 0 0 1.34 0.58 -7 0 0 0.19 0.65 -7 0 0 2.34 0.8 -7 0 0 0.9 0.59 -7 0 0 2.04 0.75 7 0 0 1.81 0.61 7 0 0 1.22 0.57 7 0 0 1.5 0.67 7 0 0 1.95 0.85 7 0 0 1.97 0.76 7 0 0 1.84 0.53 7 0 0 1.89 0.67 -8 0 0 18.5 2.26 -8 0 0 15.35 2.2 -8 0 0 18.76 1.58 -8 0 0 13.08 1.7 -8 0 0 17.03 1.83 -8 0 0 21.31 2.18 -8 0 0 18.64 2.18 8 0 0 18.3 1.49 8 0 0 19.95 1.66 8 0 0 15.86 2 8 0 0 21.26 2.68 8 0 0 23.78 2.39 8 0 0 22.86 1.86 -9 0 0 13.28 1.81 -9 0 0 8.27 1.47 -9 0 0 11.67 1.48 -9 0 0 12.73 1.66 -9 0 0 12.08 1.8 -9 0 0 14.08 2.3 -9 0 0 12.06 1.82 9 0 0 11.59 1.75 9 0 0 6.86 1.6 9 0 0 11.99 1.51 9 0 0 13.12 1.97 9 0 0 11.55 1.82 9 0 0 15.19 1.88 9 0 0 13.05 1.41 -10 0 0 0.74 0.73 -10 0 0 -0.68 0.42 -10 0 0 -0.21 0.63 -10 0 0 -0.95 0.88 -10 0 0 0.17 0.58 10 0 0 0.85 0.78 10 0 0 -0.05 0.57 10 0 0 -0.77 0.39 10 0 0 0.81 0.76 10 0 0 -0.53 0.47 -11 0 0 0.03 0.59 -11 0 0 1.49 1.41 -11 0 0 -0.38 0.6 11 0 0 -0.18 0.57 11 0 0 -0.34 0.6 11 0 0 0.43 0.8 11 0 0 0.3 0.73 11 0 0 -0.47 0.49 11 0 0 0.1 0.5 -12 0 0 1.87 1.47 -12 0 0 1.71 1.17 -12 0 0 1.37 0.89 -12 0 0 0.16 0.74 -12 0 0 4.08 1.38 12 0 0 1.54 0.93 12 0 0 1.61 0.65 12 0 0 1.61 1.07 12 0 0 3.76 1.42 -13 0 0 0.96 1.04 -13 0 0 -1.77 0.76 -13 0 0 -0.53 0.75 -13 0 0 1.53 0.93 13 0 0 1.12 0.93 13 0 0 1.75 0.76 13 0 0 0.41 0.54 13 0 0 0.42 1.09 13 0 0 1.21 1.18 -14 0 0 0.5 0.91 14 0 0 0.08 1.04 14 0 0 -0.27 0.82 14 0 0 0.24 0.7 14 -1 0 2 1.08 14 -1 0 1.57 1.19 14 -1 0 0.29 0.55 -14 1 0 2.07 1.26 -14 1 0 0.87 1.23 -14 1 0 0.78 1.65 13 -1 0 0.67 1.22 13 -1 0 1.23 0.7 13 -1 0 0.61 0.99 -13 1 0 -0.23 0.8 -13 1 0 0.69 1.47 -13 1 0 0.47 1.01 -13 1 0 0.88 0.87 12 -1 0 0.04 0.57 12 -1 0 -0.84 0.69 12 -1 0 1.12 0.98 12 -1 0 0.08 0.68 12 -1 0 -0.11 0.53 -12 1 0 -0.25 0.88 -12 1 0 0.02 0.75 -12 1 0 -0.77 1.07 -12 1 0 2.52 1.12 -12 1 0 0.95 0.73 11 -1 0 -0.18 0.79 11 -1 0 -0.41 0.51 11 -1 0 1.17 0.66 11 -1 0 -0.24 0.53 11 -1 0 1.17 0.97 11 -1 0 0.45 0.7 -11 1 0 -0.07 0.66 -11 1 0 0.7 1.34 -11 1 0 0.26 0.72 -11 1 0 0.26 0.63 -11 1 0 -0.27 1 10 -1 0 -0.12 0.48 10 -1 0 -0.41 0.48 10 -1 0 -0.38 0.52 10 -1 0 0 0.46 10 -1 0 -0.24 0.7 10 -1 0 0.34 0.71 -10 1 0 -0.52 0.6 -10 1 0 0.3 0.63 -10 1 0 -0.3 0.46 -10 1 0 0.22 0.64 -10 1 0 0.08 0.62 -10 1 0 0.51 1.11 9 -1 0 5.4 1.3 9 -1 0 6.28 1.1 9 -1 0 4.76 1.44 9 -1 0 6.18 0.99 9 -1 0 5.4 1.25 9 -1 0 5.34 1.39 9 -1 0 6.32 0.96 9 -1 0 8.09 1.31 -9 1 0 3.76 1.04 -9 1 0 4.1 1.04 -9 1 0 5.19 1.24 -9 1 0 5.24 1.26 -9 1 0 6.14 1.28 -9 1 0 4.1 1.44 8 -1 0 5.17 0.85 8 -1 0 4.78 0.93 8 -1 0 4.93 1.26 8 -1 0 4.67 0.98 8 -1 0 4.29 1.06 -8 1 0 3.62 0.98 -8 1 0 2.66 1.2 -8 1 0 5.9 1.28 -8 1 0 6.53 1.17 -8 1 0 5.53 1.2 -8 1 0 5.61 0.95 -8 1 0 5.51 1.12 7 -1 0 0.78 0.43 7 -1 0 0.41 0.61 7 -1 0 0.94 0.56 7 -1 0 1.78 0.76 7 -1 0 2.45 0.59 7 -1 0 1.27 0.61 7 -1 0 2.84 0.85 -7 1 0 1.41 0.7 -7 1 0 1.56 0.65 -7 1 0 3.09 0.65 -7 1 0 1.37 0.95 -7 1 0 2.71 0.82 -7 1 0 2.23 0.87 -7 1 0 2.73 0.75 6 -1 0 2.05 0.51 6 -1 0 3.47 0.87 6 -1 0 1.87 0.64 6 -1 0 2.37 0.56 6 -1 0 3.95 0.99 6 -1 0 2.44 0.74 6 -1 0 3.91 0.77 -6 1 0 1.23 0.66 -6 1 0 2.22 0.67 -6 1 0 1.42 0.56 -6 1 0 3.83 0.89 -6 1 0 3.76 0.86 -6 1 0 1.81 0.65 -6 1 0 2.61 0.56 5 -1 0 0.2 0.34 5 -1 0 0.2 0.31 5 -1 0 1.43 0.67 5 -1 0 0.8 0.57 5 -1 0 0.34 0.38 5 -1 0 0.78 0.44 5 -1 0 0.59 0.46 -5 1 0 -0.39 0.3 -5 1 0 1.27 0.52 -5 1 0 -0.13 0.48 -5 1 0 -0.07 0.3 -5 1 0 0.65 0.47 -5 1 0 1.03 0.49 -5 1 0 0.66 0.49 4 -1 0 12.52 0.93 4 -1 0 12.95 1.49 4 -1 0 8.7 1.05 4 -1 0 10.55 0.85 4 -1 0 11.81 1.37 4 -1 0 14 1.3 4 -1 0 13.86 1.02 -4 1 0 11.09 1.09 -4 1 0 11.11 1.38 -4 1 0 10.75 0.85 -4 1 0 9.99 1.09 -4 1 0 9.45 1.03 -4 1 0 10.58 1.21 -4 1 0 13.44 1.31 3 -1 0 158.25 7.11 3 -1 0 161.72 7.53 3 -1 0 155.56 7.48 3 -1 0 164 7.32 3 -1 0 156.17 7.21 3 -1 0 156.81 7.34 3 -1 0 157.67 7.16 -3 1 0 156.69 7.53 -3 1 0 156.85 7.33 -3 1 0 150.06 7.09 -3 1 0 162.46 7.34 -3 1 0 156.03 7.23 -3 1 0 161.95 7.43 -3 1 0 157.91 7.22 2 -1 0 14.79 0.93 2 -1 0 14.22 0.99 2 -1 0 14.94 0.89 2 -1 0 12.87 1.12 2 -1 0 14.16 1 2 -1 0 15.45 0.93 2 -1 0 13.33 1.11 -2 1 0 15.95 0.91 -2 1 0 16.38 1.22 -2 1 0 14.58 0.95 -2 1 0 15.71 1.13 -2 1 0 15.9 0.94 -2 1 0 14 0.99 -2 1 0 14.05 0.97 1 -1 0 46.59 1.98 1 -1 0 47.26 2.25 1 -1 0 47.02 2.05 1 -1 0 44.93 1.99 1 -1 0 47.47 2.17 1 -1 0 46.24 2.06 -1 1 0 36.48 2.02 -1 1 0 37.59 2.17 -1 1 0 38.26 2.03 -1 -1 0 -0.01 0.09 -1 -1 0 0.02 0.07 -1 -1 0 -0.01 0.07 -1 -1 0 -0.08 0.05 -1 -1 0 0.09 0.11 -1 -1 0 0.06 0.07 -1 -1 0 0.09 0.09 1 1 0 -0.06 0.06 1 1 0 -0.05 0.06 1 1 0 -0.03 0.06 1 1 0 -0.09 0.09 1 1 0 0.01 0.07 1 1 0 0.05 0.08 -2 -1 0 309.5 13.24 -2 -1 0 308.18 13.26 -2 -1 0 294.36 13.27 -2 -1 0 290.83 13.17 2 1 0 294.16 13.22 2 1 0 291.61 13.15 2 1 0 292.96 13.16 2 1 0 299.64 13.25 2 1 0 299.09 13.27 2 1 0 292.32 13.02 2 1 0 307.24 13.17 -3 -1 0 85.3 4.46 -3 -1 0 90.53 4.41 -3 -1 0 93.41 4.3 -3 -1 0 87.43 4.28 -3 -1 0 89.86 4.27 -3 -1 0 89.21 4.39 3 1 0 87.8 4.4 3 1 0 87.14 4.36 3 1 0 92.74 4.28 3 1 0 92.68 4.5 3 1 0 83.5 4.21 3 1 0 86.88 4.29 -4 -1 0 4.79 0.77 -4 -1 0 4.07 0.75 -4 -1 0 4.78 0.74 -4 -1 0 6.82 0.85 -4 -1 0 4.95 0.64 -4 -1 0 6.71 0.81 -4 -1 0 4.36 0.87 4 1 0 7.24 0.85 4 1 0 4.93 0.77 4 1 0 6.17 0.74 4 1 0 5.56 0.7 4 1 0 7.12 1.07 4 1 0 6.32 0.87 4 1 0 6.8 0.82 -5 -1 0 1.25 0.56 -5 -1 0 0.78 0.45 -5 -1 0 0.2 0.36 -5 -1 0 0.89 0.47 -5 -1 0 0.8 0.38 -5 -1 0 1.11 0.74 -5 -1 0 1.35 0.48 5 1 0 0.38 0.38 5 1 0 0.26 0.46 5 1 0 -0.01 0.38 5 1 0 0.88 0.49 5 1 0 -0.01 0.36 5 1 0 1.55 0.58 5 1 0 1.06 0.71 -6 -1 0 80.42 4.4 -6 -1 0 84.96 4.41 -6 -1 0 77.63 4.14 -6 -1 0 78.71 4.54 -6 -1 0 79.24 4.23 6 1 0 75.99 4.44 6 1 0 85.97 4.41 6 1 0 81.48 4.14 6 1 0 88.85 4.65 6 1 0 86.35 4.33 6 1 0 78.1 4.28 6 1 0 82.28 4.76 -7 -1 0 4 0.81 -7 -1 0 3.39 0.91 -7 -1 0 2.7 0.87 -7 -1 0 3.01 0.8 -7 -1 0 3.73 0.89 -7 -1 0 2.66 0.96 7 1 0 3.16 0.68 7 1 0 4.12 1.08 7 1 0 2.84 0.74 7 1 0 3.56 0.86 7 1 0 3.12 0.85 7 1 0 2.55 0.75 7 1 0 2.62 0.83 -8 -1 0 0.09 0.56 -8 -1 0 0.33 0.47 -8 -1 0 0.19 0.48 -8 -1 0 -0.94 0.56 -8 -1 0 0.21 0.48 8 1 0 0.34 0.42 8 1 0 0.56 0.53 8 1 0 0.06 0.5 8 1 0 0.51 0.43 8 1 0 0.2 0.51 8 1 0 0.22 0.52 8 1 0 1 0.72 -9 -1 0 44.29 3.67 -9 -1 0 42.01 3.3 -9 -1 0 50.29 3.27 -9 -1 0 48.86 3.49 -9 -1 0 40.69 2.88 -9 -1 0 45.12 3.17 9 1 0 45.52 3.2 9 1 0 44.01 3.63 9 1 0 42.14 2.74 9 1 0 49.75 3.51 9 1 0 43.76 2.97 9 1 0 41.53 3.22 -10 -1 0 23.22 2.31 -10 -1 0 20.65 2.93 -10 -1 0 26.49 2.79 -10 -1 0 24.72 2.79 -10 -1 0 30.32 3.11 10 1 0 25 2.51 10 1 0 24.9 2.69 10 1 0 25.32 2.61 10 1 0 25.98 1.98 10 1 0 22.99 2.83 -11 -1 0 1.48 0.98 -11 -1 0 1.4 1.16 -11 -1 0 2.73 1.24 -11 -1 0 1.15 0.8 -11 -1 0 1.69 1.46 11 1 0 1.97 1 11 1 0 0.44 0.72 11 1 0 1.58 0.79 11 1 0 1.09 0.88 -12 -1 0 2.19 1.12 -12 -1 0 3.31 1.21 -12 -1 0 1.09 1.24 -12 -1 0 4.75 1.74 -12 -1 0 3.01 1.09 12 1 0 4.56 1.44 12 1 0 0.11 0.88 12 1 0 1.14 1.01 12 1 0 1.63 0.58 12 1 0 2.36 0.83 -13 -1 0 -0.17 0.97 -13 -1 0 -0.7 0.72 -13 -1 0 0.29 0.82 -13 -1 0 -0.13 0.85 13 1 0 0.54 0.53 13 1 0 0.47 0.66 13 1 0 1.18 1.02 13 1 0 -0.18 0.44 13 1 0 -0.5 0.82 13 1 0 0.07 0.81 -14 -1 0 0.88 1.17 -14 -1 0 0.63 1.36 -14 -1 0 0.19 1 14 1 0 -0.4 0.88 14 1 0 0.77 0.99 14 1 0 -0.39 0.65 13 -2 0 0.22 0.99 13 -2 0 0.69 0.69 13 -2 0 -0.18 0.68 -13 2 0 1.72 1.04 -13 2 0 1.44 1.09 -13 2 0 0.82 1.48 -13 2 0 1.2 1.23 -13 2 0 2.39 1.21 -13 2 0 2.01 0.93 12 -2 0 5.39 1.75 12 -2 0 0.74 0.96 12 -2 0 2.88 0.99 12 -2 0 6.32 1.2 12 -2 0 2.95 0.95 -12 2 0 2.45 1.18 -12 2 0 2.72 1.56 -12 2 0 5.23 1.14 -12 2 0 0.78 1.64 -12 2 0 2.21 0.96 -12 2 0 1.44 1.04 11 -2 0 0.28 0.6 11 -2 0 1.27 0.72 11 -2 0 1.29 0.78 11 -2 0 2.32 0.77 11 -2 0 1.37 1.17 11 -2 0 1.75 0.93 -11 2 0 1.16 0.77 -11 2 0 0.58 1.03 -11 2 0 1.2 0.86 -11 2 0 0.99 0.7 -11 2 0 0.37 0.66 -11 2 0 -0.11 0.72 10 -2 0 0.05 0.54 10 -2 0 -0.31 0.46 10 -2 0 0.59 0.54 10 -2 0 0.06 0.67 10 -2 0 -0.07 0.77 10 -2 0 1.11 0.67 -10 2 0 0.05 0.87 -10 2 0 -0.4 0.54 -10 2 0 1.82 0.84 -10 2 0 1.3 0.83 -10 2 0 -0.2 0.46 9 -2 0 -0.16 0.72 9 -2 0 1.09 1.34 9 -2 0 0.64 0.55 9 -2 0 1.33 0.58 9 -2 0 1.21 0.67 9 -2 0 2.2 0.98 9 -2 0 1 0.64 -9 2 0 0.61 0.69 -9 2 0 -0.18 0.59 -9 2 0 1.06 0.82 -9 2 0 0.79 0.69 -9 2 0 0.1 0.92 -9 2 0 0.61 0.66 8 -2 0 9.75 1.3 8 -2 0 8.55 1.16 8 -2 0 8.5 1.24 8 -2 0 4.76 1.33 8 -2 0 8.89 1.16 8 -2 0 5.27 1.14 8 -2 0 9.91 1.84 8 -2 0 7.61 1.39 -8 2 0 9.28 1.43 -8 2 0 11.5 1.71 -8 2 0 8.24 1.32 -8 2 0 9.1 1.36 -8 2 0 9.24 1.52 -8 2 0 11.69 2 -8 2 0 8.78 1.14 7 -2 0 4.16 0.83 7 -2 0 4.31 0.77 7 -2 0 2.53 0.8 7 -2 0 3.76 1.14 7 -2 0 3.5 0.74 7 -2 0 3.83 0.84 7 -2 0 3.26 0.82 7 -2 0 2.93 1.01 -7 2 0 2.98 0.86 -7 2 0 2.41 0.84 -7 2 0 3.39 0.85 -7 2 0 4.63 0.9 -7 2 0 1.99 0.97 -7 2 0 3.22 0.8 -7 2 0 4.14 0.78 6 -2 0 9.45 1.04 6 -2 0 10.39 1.35 6 -2 0 8.33 1.09 6 -2 0 7.27 1.31 6 -2 0 10.48 1.31 6 -2 0 9.35 1.61 -6 2 0 8.27 1.47 -6 2 0 8.06 0.94 -6 2 0 8.41 1.17 -6 2 0 9.51 1.41 -6 2 0 6.96 1.11 -6 2 0 7.57 1.14 -6 2 0 8.02 1.1 5 -2 0 0.54 0.63 5 -2 0 0.91 0.55 5 -2 0 1.15 0.47 5 -2 0 0.46 0.36 5 -2 0 1.1 0.47 5 -2 0 0.44 0.43 5 -2 0 1.3 0.44 -5 2 0 0.77 0.52 -5 2 0 1.03 0.63 -5 2 0 0.65 0.45 -5 2 0 0.7 0.45 -5 2 0 1.01 0.39 -5 2 0 0.66 0.43 4 -2 0 37.23 2.29 4 -2 0 41.16 2.09 4 -2 0 39.01 2.13 4 -2 0 43.68 2.71 4 -2 0 37.22 2.54 4 -2 0 38.35 2.46 4 -2 0 40.12 2.14 -4 2 0 34.71 2.17 -4 2 0 36.72 2.29 -4 2 0 39.62 2.1 -4 2 0 35.55 2.28 -4 2 0 37.44 2.18 -4 2 0 38.4 2.5 -4 2 0 38.57 2.12 3 -2 0 46.39 2.78 3 -2 0 46.59 2.69 3 -2 0 44.6 2.42 3 -2 0 44.72 2.44 3 -2 0 44.74 2.24 3 -2 0 43.04 2.27 3 -2 0 45.83 2.36 -3 2 0 44.9 2.34 -3 2 0 44.3 2.36 -3 2 0 46.61 2.69 -3 2 0 44.15 2.32 -3 2 0 45.37 2.31 -3 2 0 45.65 2.44 -3 2 0 43.08 2.42 -3 2 0 47.76 2.69 2 -2 0 163.38 7.45 2 -2 0 172.13 7.74 2 -2 0 169.71 7.62 2 -2 0 168.17 7.58 2 -2 0 172.37 7.83 2 -2 0 165.56 7.43 2 -2 0 170.72 7.6 2 -2 0 170.46 7.99 -2 2 0 162.85 7.6 -2 2 0 167.94 7.52 -2 2 0 167.3 7.58 -2 2 0 166.03 7.8 -2 2 0 170.43 7.53 -2 2 0 168.91 7.93 -2 2 0 171.08 7.62 -2 2 0 166.35 7.6 1 -2 0 42.29 2.37 1 -2 0 47.02 2.26 1 -2 0 41.09 1.99 1 -2 0 42.43 2.12 1 -2 0 38.18 2.07 -1 2 0 40.96 1.99 -1 2 0 41.39 1.91 -1 2 0 40.57 2.32 -1 2 0 41.66 1.91 -1 2 0 39.8 2.17 -1 2 0 41.85 2.08 -1 2 0 42.26 2.12 -1 2 0 39.91 1.99 -1 2 0 39.22 2.07 0 -2 0 212.79 9.32 0 -2 0 205.78 9.55 0 -2 0 210.26 9.29 0 -2 0 209.1 9.5 0 2 0 210.72 9.28 0 2 0 208.38 9.55 0 2 0 215.35 9.26 0 2 0 215.06 9.24 0 2 0 213.34 9.51 0 2 0 216.88 9.32 0 2 0 212.46 9.22 0 2 0 211.53 9.29 0 2 0 211.52 9.44 -1 -2 0 60.67 2.75 -1 -2 0 57.12 2.8 -1 -2 0 56.01 2.72 -1 -2 0 59.2 2.75 -1 -2 0 60.78 2.83 1 2 0 62.35 2.77 1 2 0 62.32 2.77 1 2 0 60.94 2.82 1 2 0 58.85 2.9 1 2 0 56.62 2.82 1 2 0 57.39 2.73 -2 -2 0 239.76 10.71 -2 -2 0 228.82 10.7 -2 -2 0 233.7 10.61 -2 -2 0 242.09 10.63 -2 -2 0 242.39 10.8 -2 -2 0 238.5 10.69 2 2 0 242.11 10.7 2 2 0 252.03 10.64 2 2 0 231.47 10.62 2 2 0 240.79 10.62 2 2 0 238.93 10.79 2 2 0 239.52 10.68 2 2 0 232.17 10.72 -3 -2 0 35.7 2.04 -3 -2 0 31.04 1.89 -3 -2 0 34.03 2.04 -3 -2 0 34.06 2.03 -3 -2 0 31.46 2 -3 -2 0 35.93 1.94 3 2 0 33.35 1.99 3 2 0 35.33 2.05 3 2 0 34.48 1.81 3 2 0 32.31 1.92 3 2 0 33.31 2.04 3 2 0 35.4 1.93 3 2 0 35.66 2.03 -4 -2 0 42.01 2.48 -4 -2 0 39.44 2.26 -4 -2 0 41.18 2.4 -4 -2 0 39.81 2.4 -4 -2 0 41.05 2.33 -4 -2 0 38.48 2.25 4 2 0 40.15 2.47 4 2 0 38.6 2.02 4 2 0 36.37 2.31 4 2 0 38.16 2.25 4 2 0 36.69 2.36 4 2 0 39.02 2.28 4 2 0 38.82 2.22 4 2 0 36.55 2.01 -5 -2 0 35.65 2.25 -5 -2 0 34.85 2.24 -5 -2 0 38.97 2.47 -5 -2 0 40.22 2.34 -5 -2 0 33 2.37 -5 -2 0 35.74 2.52 5 2 0 41.18 2.44 5 2 0 35.14 2.21 5 2 0 36.34 2.21 5 2 0 34.32 2.44 5 2 0 34.37 2.02 5 2 0 33.45 2.37 -6 -2 0 25.8 1.81 -6 -2 0 26.86 2.04 -6 -2 0 21.15 2.26 -6 -2 0 21.45 1.75 -6 -2 0 23.33 1.94 6 2 0 23.18 1.74 6 2 0 23.45 2.26 6 2 0 24.15 2.05 6 2 0 22.58 1.81 6 2 0 20.96 1.58 6 2 0 22.4 1.68 6 2 0 24.84 1.92 -7 -2 0 -0.37 0.31 -7 -2 0 0.43 0.49 -7 -2 0 0.37 0.45 -7 -2 0 0.53 0.55 -7 -2 0 0.09 0.57 -7 -2 0 0.07 0.44 7 2 0 0.23 0.51 7 2 0 0.44 0.43 7 2 0 0.43 0.63 7 2 0 0.23 0.39 7 2 0 0.68 0.49 7 2 0 0.37 0.46 -8 -2 0 -0.14 0.44 -8 -2 0 -1.52 0.53 -8 -2 0 0.14 0.44 -8 -2 0 0.17 0.57 -8 -2 0 0.44 0.54 -8 -2 0 0.76 0.7 8 2 0 0.98 0.64 8 2 0 0.36 0.45 8 2 0 -0.14 0.41 8 2 0 0.13 0.44 8 2 0 0.3 0.57 8 2 0 0.52 0.54 8 2 0 -0.12 0.49 -9 -2 0 52.36 4.05 -9 -2 0 52.64 3.5 -9 -2 0 53.62 3.76 -9 -2 0 53.39 3.73 -9 -2 0 43.6 3.29 -9 -2 0 51.24 3.34 9 2 0 52.18 3.34 9 2 0 52.87 3.45 9 2 0 49.84 3.91 9 2 0 46.91 3.08 9 2 0 50.79 3.58 9 2 0 49.95 3.69 -10 -2 0 9.7 1.62 -10 -2 0 9.28 1.78 -10 -2 0 8.55 1.51 -10 -2 0 9.71 2.14 -10 -2 0 14.21 2.46 10 2 0 11.46 2 10 2 0 8.97 1.51 10 2 0 11.87 1.81 10 2 0 10.74 2.08 10 2 0 11.26 1.67 -11 -2 0 0.69 1.26 -11 -2 0 0.15 0.76 -11 -2 0 -0.01 0.89 -11 -2 0 -0.75 0.65 -11 -2 0 -0.25 0.68 11 2 0 0.51 0.65 11 2 0 -0.36 0.72 11 2 0 -0.24 0.65 -12 -2 0 0.48 1.16 -12 -2 0 -0.44 0.7 -12 -2 0 -0.33 0.66 -12 -2 0 0.77 0.9 12 2 0 0.34 0.44 12 2 0 1.15 0.85 12 2 0 0.36 0.63 12 2 0 -0.27 0.83 12 2 0 0.42 0.85 -13 -2 0 -1.1 0.64 -13 -2 0 0.88 1.34 -13 -2 0 0.65 0.89 13 2 0 0.44 0.91 13 2 0 -0.02 0.73 13 2 0 -0.26 0.61 13 2 0 -1.05 0.69 -14 -2 0 -0.77 0.77 -14 -2 0 0.55 1.04 -14 -2 0 -1.28 1.22 14 2 0 1.69 1.14 14 2 0 0.87 1.17 14 2 0 -0.2 0.8 14 2 0 -0.7 0.63 13 -3 0 -0.47 0.85 13 -3 0 -0.08 0.65 13 -3 0 -0.56 0.6 -13 3 0 0.15 0.94 -13 3 0 -1.25 0.96 -13 3 0 2.88 1.26 -13 3 0 -1.48 1.15 12 -3 0 -0.02 0.79 12 -3 0 0.89 1.05 12 -3 0 -0.17 0.58 12 -3 0 -0.22 0.69 -12 3 0 0.27 1.38 -12 3 0 0.36 0.85 -12 3 0 0.35 0.88 -12 3 0 0.48 0.72 -12 3 0 0.4 0.92 11 -3 0 1.78 0.74 11 -3 0 0.44 1.09 11 -3 0 3.91 1.41 11 -3 0 4 0.99 11 -3 0 3.19 1.01 -11 3 0 0.93 1.26 -11 3 0 1.98 1.08 -11 3 0 3.02 0.88 -11 3 0 2.24 1.08 -11 3 0 -0.06 0.67 -11 3 0 2.44 0.91 10 -3 0 1.58 0.89 10 -3 0 1.73 0.64 10 -3 0 2.12 0.83 10 -3 0 2.41 1.16 10 -3 0 2.65 0.82 -10 3 0 -0.15 0.68 -10 3 0 1.15 0.79 -10 3 0 0.51 1.12 -10 3 0 1.95 0.84 -10 3 0 2.03 0.74 9 -3 0 11.78 1.61 9 -3 0 12.13 1.36 9 -3 0 11.01 1.44 9 -3 0 10.88 2.15 9 -3 0 9.44 1.69 -9 3 0 10.95 1.43 -9 3 0 13.02 2.27 -9 3 0 11.98 1.79 -9 3 0 7.38 1.4 -9 3 0 8.89 1.55 -9 3 0 10.16 1.93 -9 3 0 13.22 1.81 8 -3 0 2.57 0.9 8 -3 0 1.53 0.97 8 -3 0 2.92 1.22 8 -3 0 1.31 0.72 8 -3 0 3.24 0.71 8 -3 0 3.15 0.75 8 -3 0 2.54 0.95 -8 3 0 2.49 0.84 -8 3 0 0.8 0.99 -8 3 0 3.57 1.07 -8 3 0 1.08 0.55 -8 3 0 1.02 0.55 -8 3 0 3 0.88 -8 3 0 0.69 0.68 7 -3 0 -0.62 0.29 7 -3 0 0.46 0.7 7 -3 0 0.15 0.36 7 -3 0 -0.57 0.54 7 -3 0 -0.45 0.4 7 -3 0 0.44 0.43 7 -3 0 0.3 0.38 -7 3 0 0.96 0.77 -7 3 0 -0.34 0.52 -7 3 0 0.24 0.44 -7 3 0 0.55 0.42 -7 3 0 -0.42 0.39 -7 3 0 0.55 0.52 -7 3 0 0.22 0.38 -7 3 0 0.03 0.4 6 -3 0 25.56 1.7 6 -3 0 26.84 2.01 6 -3 0 28.07 2.11 6 -3 0 27.47 1.8 6 -3 0 27.73 2.03 6 -3 0 28.04 2.86 6 -3 0 29.92 2.52 -6 3 0 27.31 1.84 -6 3 0 29.53 2.5 -6 3 0 26.8 1.97 -6 3 0 26.41 1.95 -6 3 0 26.43 1.76 -6 3 0 28.41 2.12 -6 3 0 29.13 2.11 -6 3 0 31.12 2.42 5 -3 0 0.53 0.35 5 -3 0 1.5 0.48 5 -3 0 1 0.48 5 -3 0 0.36 0.56 5 -3 0 0.18 0.58 5 -3 0 0.25 0.29 5 -3 0 0.6 0.51 -5 3 0 0.5 0.38 -5 3 0 0.1 0.34 -5 3 0 0.28 0.42 -5 3 0 -0.59 0.52 -5 3 0 0.86 0.61 -5 3 0 0.49 0.69 -5 3 0 0.03 0.33 4 -3 0 44.89 2.65 4 -3 0 44.53 2.73 4 -3 0 46.31 2.37 4 -3 0 49.48 3.16 4 -3 0 41.56 2.89 4 -3 0 46.9 2.62 4 -3 0 43.3 2.31 -4 3 0 48.96 2.67 -4 3 0 45.85 2.56 -4 3 0 46.85 3.01 -4 3 0 47.02 2.53 -4 3 0 43.13 2.89 -4 3 0 47.35 2.54 -4 3 0 47.76 2.66 -4 3 0 47.67 2.51 3 -3 0 0.74 0.23 3 -3 0 1.33 0.52 3 -3 0 0.7 0.52 3 -3 0 1.32 0.25 3 -3 0 0.13 0.39 3 -3 0 0.87 0.36 3 -3 0 0.9 0.36 -3 3 0 0.72 0.3 -3 3 0 0.86 0.35 -3 3 0 1.02 0.36 -3 3 0 -0.04 0.34 -3 3 0 0.94 0.34 -3 3 0 0.4 0.47 -3 3 0 0.5 0.46 -3 3 0 0.8 0.35 2 -3 0 62.8 2.75 2 -3 0 64.21 3.05 2 -3 0 61.19 2.75 2 -3 0 58.52 3.08 2 -3 0 63.33 3.24 2 -3 0 60.19 3.29 2 -3 0 63.54 3.58 2 -3 0 61.28 3.02 -2 3 0 62.59 3.12 -2 3 0 61.17 3.02 -2 3 0 61.14 2.93 -2 3 0 60.38 2.93 -2 3 0 64.12 3.26 -2 3 0 60.98 3.02 -2 3 0 58.17 3.44 1 -3 0 143.77 6.48 1 -3 0 141.44 6.7 1 -3 0 138.39 6.35 1 -3 0 149.3 6.91 1 -3 0 139.94 6.55 -1 3 0 139.08 6.46 -1 3 0 141.85 6.48 -1 3 0 140.3 6.24 -1 3 0 140.09 6.54 -1 3 0 139.54 6.26 -1 3 0 140.12 6.35 -1 3 0 147.24 6.68 -1 3 0 141.1 6.35 -1 3 0 140.15 6.84 0 -3 0 299.04 13.3 0 -3 0 301.07 13.61 0 -3 0 289.96 13.49 0 -3 0 311.24 13.34 0 3 0 303.6 13.29 0 3 0 306.93 13.34 0 3 0 296.67 13.68 0 3 0 308.59 13.28 0 3 0 301.21 13.52 0 3 0 308.96 13.25 0 3 0 306.56 13.22 0 3 0 300.26 13.2 0 3 0 301.92 13.62 -1 -3 0 12.41 1.08 -1 -3 0 12.18 0.77 -1 -3 0 12.04 0.78 -1 -3 0 12.9 0.77 -1 -3 0 11.69 0.84 -1 -3 0 12.46 0.87 1 3 0 11.51 0.87 1 3 0 11.74 0.79 1 3 0 12.52 0.85 1 3 0 13.57 1.08 1 3 0 12.18 0.74 1 3 0 12.41 0.8 -2 -3 0 20.75 1.27 -2 -3 0 21.48 1.36 -2 -3 0 22.03 1.42 -2 -3 0 22.14 1.29 -2 -3 0 21.25 1.3 2 3 0 23.52 1.38 2 3 0 22.09 1.42 2 3 0 20.5 1.28 2 3 0 23.88 1.43 2 3 0 19.27 1.51 2 3 0 20.06 1.28 2 3 0 21.48 1.29 -3 -3 0 93.16 4.41 -3 -3 0 92.24 4.57 -3 -3 0 87.62 4.63 -3 -3 0 88.21 4.56 -3 -3 0 90.05 4.52 -3 -3 0 88.8 4.42 -3 -3 0 88.2 4.41 3 3 0 91.26 4.42 3 3 0 93.42 4.55 3 3 0 90.81 4.5 3 3 0 93.47 4.46 3 3 0 95.3 4.45 3 3 0 95.21 4.61 3 3 0 91.65 4.63 -4 -3 0 18.63 1.43 -4 -3 0 19.1 1.51 -4 -3 0 18.56 1.55 -4 -3 0 19 1.53 -4 -3 0 21.66 1.64 -4 -3 0 20.72 1.44 4 3 0 21.34 1.59 4 3 0 21.17 1.56 4 3 0 23.14 1.51 4 3 0 18.78 1.48 4 3 0 18.77 1.32 4 3 0 21.18 1.44 4 3 0 22.1 1.59 -5 -3 0 -0.34 0.33 -5 -3 0 0.32 0.51 -5 -3 0 -0.06 0.43 -5 -3 0 0.12 0.49 -5 -3 0 0.06 0.34 -5 -3 0 0.06 0.34 5 3 0 0.23 0.4 5 3 0 -0.62 0.31 5 3 0 0.36 0.39 5 3 0 0.41 0.34 5 3 0 -0.02 0.35 5 3 0 0.25 0.35 5 3 0 -0.24 0.22 -6 -3 0 5.66 0.99 -6 -3 0 5.6 1.05 -6 -3 0 6.29 1.02 -6 -3 0 5.77 1.08 -6 -3 0 4.39 1.1 6 3 0 7.42 1.26 6 3 0 4.84 0.96 6 3 0 6.07 0.79 6 3 0 6.67 1.19 6 3 0 4.34 0.82 6 3 0 7.52 0.84 6 3 0 7.04 1.15 6 3 0 6.83 1.04 -7 -3 0 28.8 2.28 -7 -3 0 23.2 2.03 -7 -3 0 26.88 2.03 -7 -3 0 22.27 2.5 -7 -3 0 27.45 2.07 -7 -3 0 24.37 2.13 7 3 0 25.47 2.6 7 3 0 26.78 1.98 7 3 0 24.41 1.9 7 3 0 25.06 1.73 7 3 0 26.52 1.65 7 3 0 27.07 2.6 7 3 0 22.19 1.94 7 3 0 25.43 2.51 -8 -3 0 13.03 2.03 -8 -3 0 13.99 1.94 -8 -3 0 12.07 1.68 -8 -3 0 14.45 1.8 -8 -3 0 11.06 1.5 -8 -3 0 10.49 1.66 8 3 0 13.68 1.48 8 3 0 10.19 1.48 8 3 0 14.73 1.65 8 3 0 14.16 1.98 8 3 0 16.31 1.77 8 3 0 13.88 1.12 8 3 0 9.54 1.58 8 3 0 10.59 1.57 -9 -3 0 6.5 1.27 -9 -3 0 4.91 1.22 -9 -3 0 4.55 1.18 -9 -3 0 7.64 1.45 -9 -3 0 13.58 2.02 -9 -3 0 4.13 1.32 9 3 0 6.63 0.9 9 3 0 7.66 1.49 9 3 0 11.41 1.6 9 3 0 7.28 1.19 9 3 0 7.33 1.58 9 3 0 6.07 1.52 9 3 0 8.07 1.45 -10 -3 0 0.9 0.94 -10 -3 0 0 0.67 -10 -3 0 0.94 1.04 -10 -3 0 1.78 0.86 -10 -3 0 1.07 0.81 10 3 0 1.56 0.77 10 3 0 0.96 0.81 10 3 0 1.44 0.76 10 3 0 1 0.78 10 3 0 1.05 0.9 10 3 0 1.14 0.75 -11 -3 0 3.77 1.5 -11 -3 0 0.21 0.92 -11 -3 0 3.02 1.13 11 3 0 2.37 0.71 11 3 0 3.24 1.04 11 3 0 5.54 1.58 11 3 0 2.77 1.06 11 3 0 2.92 0.96 -12 -3 0 9.26 1.67 -12 -3 0 10.5 2.31 -12 -3 0 10.12 1.99 -12 -3 0 13.12 2.32 12 3 0 9.77 1.91 12 3 0 11.01 1.59 12 3 0 7.44 1.79 12 3 0 9.75 1.04 -13 -3 0 1.27 1.35 -13 -3 0 2.29 1.16 -13 -3 0 1.65 1.25 13 3 0 0.02 0.73 13 3 0 5.77 1.74 13 3 0 1.6 1.07 13 3 0 0.6 0.8 -14 -3 0 -0.01 0.99 -14 -3 0 -0.38 1.32 -14 -3 0 0.23 0.94 14 3 0 -1.09 0.74 14 3 0 -0.37 0.88 14 3 0 -0.5 0.69 14 3 0 -0.01 0.96 13 -4 0 1.46 0.71 13 -4 0 1.49 1.18 13 -4 0 0.79 0.91 -13 4 0 1.24 1.11 -13 4 0 0.4 1.03 12 -4 0 0.3 0.84 12 -4 0 0.89 0.97 12 -4 0 0.75 0.65 12 -4 0 0.4 0.58 -12 4 0 -1.15 0.94 -12 4 0 0.55 1.1 -12 4 0 0.75 0.76 -12 4 0 -1.14 0.66 -12 4 0 0.43 1.02 -12 4 0 -0.42 0.77 11 -4 0 0.7 0.89 11 -4 0 0.06 0.45 11 -4 0 -0.2 0.79 11 -4 0 0.33 0.53 -11 4 0 0.53 0.69 -11 4 0 2.36 1.35 -11 4 0 0.66 0.89 -11 4 0 0.42 0.85 -11 4 0 1.14 0.75 -11 4 0 1.07 0.93 10 -4 0 0.26 0.45 10 -4 0 1.58 1.21 10 -4 0 0.66 0.49 10 -4 0 -0.32 0.57 10 -4 0 1.17 1.03 -10 4 0 0.89 0.76 -10 4 0 -0.53 1.01 -10 4 0 -0.22 0.66 -10 4 0 0.16 0.59 -10 4 0 1.13 0.69 -10 4 0 0.18 0.57 9 -4 0 0.42 0.69 9 -4 0 -0.19 0.39 9 -4 0 -0.4 0.49 9 -4 0 2.02 1.21 9 -4 0 0.09 0.42 -9 4 0 0.47 0.66 -9 4 0 -0.49 0.47 -9 4 0 0.86 0.64 -9 4 0 -0.06 0.46 -9 4 0 -1.51 0.68 -9 4 0 -0.11 0.55 -9 4 0 -0.39 0.59 8 -4 0 5.75 0.84 8 -4 0 3.33 1.33 8 -4 0 4.4 1.27 8 -4 0 3.3 1.01 8 -4 0 2.46 0.91 8 -4 0 7.2 1.35 8 -4 0 5.05 0.82 -8 4 0 6.96 1.58 -8 4 0 4.09 0.98 -8 4 0 3.73 1.01 -8 4 0 4.79 0.92 -8 4 0 4.59 1.1 -8 4 0 2.93 0.91 7 -4 0 31.03 2.39 7 -4 0 30.1 1.87 7 -4 0 35.77 2.9 7 -4 0 32.48 2.43 7 -4 0 31.21 1.93 7 -4 0 36.04 2.42 7 -4 0 30.41 3.41 -7 4 0 29.33 2.35 -7 4 0 31.78 2.38 -7 4 0 32.6 2.75 -7 4 0 32.61 2.31 -7 4 0 31.52 3.29 -7 4 0 26.76 2.04 -7 4 0 27.61 2.21 -7 4 0 28.89 2.03 6 -4 0 8.14 1.18 6 -4 0 7.78 1.14 6 -4 0 6.91 0.83 6 -4 0 4.33 1.1 6 -4 0 8.64 1.31 6 -4 0 6.53 0.76 6 -4 0 6.42 1.56 -6 4 0 5.88 1.03 -6 4 0 6.17 1.01 -6 4 0 5.94 1.33 -6 4 0 5.08 0.92 -6 4 0 6.33 0.95 -6 4 0 8.48 1.04 -6 4 0 4.81 0.97 -6 4 0 9.66 1.68 5 -4 0 17.65 2.05 5 -4 0 17.75 1.85 5 -4 0 18.44 1.16 5 -4 0 17.14 1.1 5 -4 0 17.16 1.43 5 -4 0 13.71 1.99 5 -4 0 16.64 1.46 -5 4 0 19.8 2.01 -5 4 0 19.42 2.23 -5 4 0 15.19 1.32 -5 4 0 19.93 1.54 -5 4 0 18.81 1.57 -5 4 0 18.99 1.43 -5 4 0 18.71 1.4 4 -4 0 10.59 1.35 4 -4 0 9.97 0.7 4 -4 0 10.82 1.17 4 -4 0 9.76 0.69 4 -4 0 11.9 1.51 4 -4 0 11.72 1.2 4 -4 0 12.29 1.83 -4 4 0 9.86 1.4 -4 4 0 9.91 1.06 -4 4 0 11.77 1.2 -4 4 0 12.1 1 -4 4 0 10.39 1.13 -4 4 0 14.27 1.5 -4 4 0 13.56 1.78 -4 4 0 10.6 1.12 3 -4 0 77.27 3.84 3 -4 0 76.14 3.86 3 -4 0 82.02 4.63 3 -4 0 75.5 4.22 3 -4 0 76.37 4.14 3 -4 0 76.3 3.91 -3 4 0 76.4 4.18 -3 4 0 75.06 3.77 -3 4 0 78.8 3.87 -3 4 0 77.41 3.77 -3 4 0 81.47 4.02 -3 4 0 79.11 3.96 -3 4 0 75.26 4 -3 4 0 77.34 3.86 -3 4 0 76.28 4.44 2 -4 0 36.9 1.93 2 -4 0 35.34 2.3 2 -4 0 31.94 2.21 2 -4 0 34.28 2.51 2 -4 0 35.37 2.08 2 -4 0 36.36 2.14 -2 4 0 36.52 2.14 -2 4 0 35.26 2.08 -2 4 0 36.7 1.84 -2 4 0 34.37 1.81 -2 4 0 33.57 2.39 -2 4 0 34.12 1.9 -2 4 0 36.21 1.92 -2 4 0 36.44 2.07 1 -4 0 95.93 4.63 1 -4 0 93.95 4.96 1 -4 0 102.97 4.85 1 -4 0 98.21 4.55 -1 4 0 97.98 4.53 -1 4 0 98.21 4.54 -1 4 0 100.63 4.67 -1 4 0 98.54 4.95 -1 4 0 97.84 4.46 -1 4 0 99.2 4.69 -1 4 0 97.92 4.42 -1 4 0 98.09 4.79 -1 4 0 95.18 5.12 0 -4 0 39.23 2.22 0 -4 0 34.82 1.92 0 -4 0 35.81 2.31 0 -4 0 37.93 1.99 0 4 0 38.4 1.93 0 4 0 38.95 1.94 0 4 0 38.89 1.88 0 4 0 37.5 1.87 0 4 0 37.28 2.3 0 4 0 37.28 1.83 0 4 0 40.18 2.01 0 4 0 39.87 2.42 -1 -4 0 109.71 4.82 -1 -4 0 104.49 4.96 -1 -4 0 107.13 4.89 -1 -4 0 106.58 5.23 -1 -4 0 108.49 5.3 -1 -4 0 105.04 4.98 -1 -4 0 106.65 4.81 1 4 0 103.16 4.89 1 4 0 104 4.76 1 4 0 102.47 4.95 1 4 0 105.88 4.88 1 4 0 106.86 4.87 1 4 0 112.46 5.01 -2 -4 0 1.2 0.49 -2 -4 0 0.09 0.27 -2 -4 0 0.22 0.25 -2 -4 0 0.74 0.34 -2 -4 0 0.34 0.27 -2 -4 0 1 0.3 2 4 0 0.92 0.54 2 4 0 0.46 0.29 2 4 0 0.65 0.28 2 4 0 0.51 0.4 2 4 0 0.41 0.26 2 4 0 1.41 0.38 2 4 0 0.29 0.29 -3 -4 0 52.93 2.95 -3 -4 0 55.98 3.07 -3 -4 0 58.59 2.97 -3 -4 0 55.39 3.1 -3 -4 0 58.53 3.03 3 4 0 57.31 3 3 4 0 54.37 3.07 3 4 0 61.17 3.19 3 4 0 57.62 3.11 3 4 0 57.73 3.36 3 4 0 59.92 3 3 4 0 59.78 3.02 -4 -4 0 17.98 1.39 -4 -4 0 18.51 1.57 -4 -4 0 20.59 1.45 -4 -4 0 20.32 1.59 -4 -4 0 20.62 1.57 -4 -4 0 19.57 1.44 4 4 0 21.58 1.63 4 4 0 19.64 1.54 4 4 0 23.66 1.52 4 4 0 18.22 1.63 4 4 0 22.71 1.6 4 4 0 20.3 1.48 -5 -4 0 4.7 0.86 -5 -4 0 3.77 0.87 -5 -4 0 6.78 0.97 -5 -4 0 3.5 0.87 -5 -4 0 5.27 1.06 -5 -4 0 5.27 0.97 5 4 0 5.79 1.01 5 4 0 4.22 0.76 5 4 0 2.84 0.8 5 4 0 3.31 0.87 5 4 0 3.71 0.81 5 4 0 4.1 0.75 5 4 0 2.53 1.15 -6 -4 0 5.63 1.04 -6 -4 0 4.89 1.02 -6 -4 0 4.37 0.85 -6 -4 0 7.13 1.25 -6 -4 0 5.38 1.09 -6 -4 0 7.05 1.23 6 4 0 7.85 1.12 6 4 0 8.02 0.97 6 4 0 7.37 1.13 6 4 0 6.39 1.14 6 4 0 6.01 1.14 6 4 0 6.31 1.22 6 4 0 5.88 0.7 6 4 0 4.41 0.9 -7 -4 0 1.38 0.78 -7 -4 0 0.94 0.55 -7 -4 0 1.05 0.6 -7 -4 0 0.8 0.68 -7 -4 0 0.66 0.5 -7 -4 0 1.45 0.68 7 4 0 1.72 0.83 7 4 0 1.27 0.65 7 4 0 1.02 0.75 7 4 0 2.39 0.89 7 4 0 2.62 0.77 7 4 0 2.28 0.79 7 4 0 1.42 0.63 7 4 0 2.13 0.49 -8 -4 0 5.68 1.26 -8 -4 0 5.03 1.09 -8 -4 0 8.12 1.54 -8 -4 0 4.68 1.25 -8 -4 0 5.37 1.14 -8 -4 0 5.09 1.18 8 4 0 6.56 1.19 8 4 0 5.13 0.84 8 4 0 2.19 0.97 8 4 0 3.25 1.07 8 4 0 3.62 0.98 8 4 0 5.04 0.97 8 4 0 3.5 1.02 -9 -4 0 36.3 3.7 -9 -4 0 26.27 2.95 -9 -4 0 35.2 2.73 -9 -4 0 28.8 2.92 -9 -4 0 30.95 2.59 -9 -4 0 41.82 5.33 9 4 0 33.32 2.28 9 4 0 34.62 2.59 9 4 0 24.61 2.9 9 4 0 38.54 2.8 9 4 0 36.88 2.64 9 4 0 35.7 3.04 9 4 0 34.88 2.85 9 4 0 36.25 2.24 -10 -4 0 0.97 1.1 -10 -4 0 2.35 1.02 -10 -4 0 -0.68 0.67 -10 -4 0 0.82 0.76 -10 -4 0 0.69 0.85 10 4 0 0.11 0.74 10 4 0 -0.16 0.49 10 4 0 0.2 0.48 10 4 0 0.59 0.73 10 4 0 1.29 0.73 10 4 0 0.1 0.98 -11 -4 0 0.6 1.01 -11 -4 0 0.44 0.78 11 4 0 0.4 0.77 11 4 0 0.94 0.75 11 4 0 0.35 0.61 11 4 0 1.05 0.96 -12 -4 0 0.85 0.9 -12 -4 0 2.43 1.51 -12 -4 0 3.53 1.48 12 4 0 3.4 0.77 12 4 0 2.3 1.09 12 4 0 1.37 0.83 12 4 0 2.51 1.03 -13 -4 0 8.51 2.35 -13 -4 0 3.82 1.57 -13 -4 0 3.83 1.32 13 4 0 3.1 1.27 13 4 0 4.84 1.22 13 4 0 4.03 1.46 13 4 0 4.5 1.36 -14 -4 0 1.19 1.32 -14 -4 0 4.08 1.54 -14 -4 0 0.03 1.37 14 4 0 3.08 1.49 14 4 0 3.91 1.36 14 4 0 5.77 1.36 14 4 0 3.36 1.37 12 -5 0 0.48 0.48 12 -5 0 0.34 0.95 12 -5 0 -0.54 0.76 12 -5 0 0.03 0.53 -12 5 0 0.03 0.83 -12 5 0 -0.11 0.95 -12 5 0 1.19 1.01 -12 5 0 -1.57 1.16 -12 5 0 0.25 0.73 11 -5 0 8.68 1.67 11 -5 0 8.06 1.19 11 -5 0 10.44 2 11 -5 0 11.31 1.19 -11 5 0 8.36 1.34 -11 5 0 8.62 1.74 -11 5 0 11.8 2.06 -11 5 0 8.24 1.43 -11 5 0 7.32 1.73 -11 5 0 13.2 2.62 10 -5 0 0.53 0.76 10 -5 0 0.18 0.66 10 -5 0 0.22 0.41 -10 5 0 -0.39 0.58 -10 5 0 0.38 1.23 -10 5 0 0.2 0.69 -10 5 0 0.01 0.56 -10 5 0 -0.62 0.58 -10 5 0 0.82 0.79 9 -5 0 5.24 1.27 9 -5 0 3.43 0.64 9 -5 0 2.75 1.28 9 -5 0 5.05 1.21 9 -5 0 2.95 0.6 -9 5 0 3.3 1.23 -9 5 0 3.33 0.93 -9 5 0 4.29 1.53 -9 5 0 3.64 0.99 -9 5 0 2.83 0.82 -9 5 0 4.01 1.09 -9 5 0 4.32 1.19 8 -5 0 1.36 1.05 8 -5 0 3.35 0.59 8 -5 0 2.97 0.89 8 -5 0 2.65 0.87 8 -5 0 3.29 0.99 8 -5 0 2.5 0.52 8 -5 0 1.46 1.04 -8 5 0 0.91 0.63 -8 5 0 1.69 0.68 -8 5 0 1.28 0.72 -8 5 0 1.89 1.03 -8 5 0 3.45 1 -8 5 0 2.48 0.88 -8 5 0 2.38 0.87 7 -5 0 -0.87 0.69 7 -5 0 -0.39 0.41 7 -5 0 0.45 0.66 7 -5 0 0.64 0.31 7 -5 0 0.81 1.02 7 -5 0 1.14 0.37 -7 5 0 0.42 0.53 -7 5 0 -0.24 0.42 -7 5 0 0.28 0.46 -7 5 0 0.76 0.54 -7 5 0 0.43 0.58 -7 5 0 -0.71 0.38 -7 5 0 0.92 0.91 6 -5 0 0.5 0.24 6 -5 0 0.28 0.59 6 -5 0 1.38 0.6 6 -5 0 1.46 0.77 6 -5 0 0.39 0.78 6 -5 0 1.18 0.3 6 -5 0 0.93 0.54 -6 5 0 1.48 0.61 -6 5 0 -0.1 0.39 -6 5 0 0.55 0.52 -6 5 0 0.99 0.57 -6 5 0 0.39 0.86 -6 5 0 0.76 0.75 -6 5 0 0.44 0.44 -6 5 0 0.73 0.78 5 -5 0 87.61 4.53 5 -5 0 89.16 4.91 5 -5 0 94.48 5.04 5 -5 0 88.62 4.52 5 -5 0 82.18 5.33 -5 5 0 85.27 5 -5 5 0 79.99 4.43 -5 5 0 82.16 4.48 -5 5 0 87.68 4.46 -5 5 0 82.87 5.13 -5 5 0 80 4.48 -5 5 0 84.68 4.41 -5 5 0 86.06 4.5 4 -5 0 0.02 0.48 4 -5 0 -0.46 0.38 4 -5 0 1.02 0.69 4 -5 0 0.19 0.3 4 -5 0 -0.17 0.23 -4 5 0 0.39 0.35 -4 5 0 0.23 0.38 -4 5 0 0.26 0.32 -4 5 0 0.34 0.5 -4 5 0 0.12 0.44 -4 5 0 0.17 0.28 -4 5 0 -0.06 0.32 -4 5 0 1.39 0.72 -4 5 0 0.17 0.36 3 -5 0 0.42 0.58 3 -5 0 1.84 0.54 3 -5 0 1.84 0.52 3 -5 0 0 0.64 3 -5 0 0.54 0.47 3 -5 0 1.17 0.37 -3 5 0 1.12 0.38 -3 5 0 1.07 0.59 -3 5 0 0.77 0.45 -3 5 0 1.44 0.41 -3 5 0 0.45 0.37 -3 5 0 0.52 0.51 -3 5 0 0.57 0.31 -3 5 0 0.44 0.31 -3 5 0 0.41 0.52 2 -5 0 9.91 1.38 2 -5 0 14.19 1.39 2 -5 0 14.44 1.35 2 -5 0 14.47 0.98 -2 5 0 10.45 0.9 -2 5 0 12.93 1.28 -2 5 0 12.07 0.88 -2 5 0 13.53 0.96 -2 5 0 15.98 1.44 -2 5 0 13.19 1.69 -2 5 0 11.61 0.85 -2 5 0 13.11 1.34 1 -5 0 165.49 7.85 1 -5 0 164.39 7.48 1 -5 0 165.34 8.05 1 -5 0 162.56 7.55 -1 5 0 168.05 7.59 -1 5 0 163.57 7.46 -1 5 0 165.18 7.66 -1 5 0 165.18 7.81 -1 5 0 163.42 8.21 -1 5 0 171.42 7.41 -1 5 0 165.22 7.34 -1 5 0 153.43 7.94 -1 5 0 163.71 7.45 0 -5 0 13.54 0.96 0 -5 0 10.98 0.87 0 -5 0 11.7 0.92 0 -5 0 14.85 1.47 0 -5 0 13.42 1.54 0 5 0 15.39 1.55 0 5 0 13 0.82 0 5 0 11.18 0.92 0 5 0 12.69 0.8 0 5 0 8.85 1.29 0 5 0 11.95 0.87 0 5 0 13.62 0.91 0 5 0 13.62 0.84 -1 -5 0 0.33 0.23 -1 -5 0 0 0.15 -1 -5 0 -0.47 0.25 -1 -5 0 0.22 0.24 -1 -5 0 0.34 0.44 -1 -5 0 0.56 0.28 -1 -5 0 0.17 0.17 1 5 0 0 0.2 1 5 0 0.14 0.42 1 5 0 -0.45 0.32 1 5 0 -0.06 0.2 1 5 0 0.22 0.22 1 5 0 -0.13 0.19 1 5 0 0 0.14 1 5 0 0.12 0.25 -2 -5 0 0.94 0.28 -2 -5 0 2 0.65 -2 -5 0 1.17 0.34 -2 -5 0 0.75 0.36 -2 -5 0 1.19 0.32 -2 -5 0 1.42 0.41 -2 -5 0 0.77 0.31 2 5 0 0.28 0.43 2 5 0 0.69 0.28 2 5 0 1.16 0.37 2 5 0 0.98 0.34 2 5 0 2.09 0.47 2 5 0 0.79 0.4 -3 -5 0 44.35 2.63 -3 -5 0 45 2.71 -3 -5 0 43.96 2.41 -3 -5 0 44.43 2.41 -3 -5 0 45.7 2.61 -3 -5 0 43.76 2.43 3 5 0 42.76 2.66 3 5 0 50.23 3.02 3 5 0 45.14 2.5 3 5 0 44.16 2.46 3 5 0 41.86 2.4 3 5 0 42.93 2.55 3 5 0 47.35 2.67 -4 -5 0 110.58 5.22 -4 -5 0 103.04 5.21 -4 -5 0 103.39 5.4 -4 -5 0 104.79 5.33 -4 -5 0 102.45 5.41 -4 -5 0 103.2 5.26 4 5 0 103.55 5.43 4 5 0 102.09 5.33 4 5 0 108.31 5.24 4 5 0 111.78 5.29 4 5 0 102.02 5.61 4 5 0 105.83 5.26 4 5 0 105.28 5.37 -5 -5 0 71.15 4.04 -5 -5 0 70.11 3.8 -5 -5 0 71.27 3.86 -5 -5 0 68.98 3.94 -5 -5 0 71.88 4.07 5 5 0 71.18 4.17 5 5 0 72.16 3.97 5 5 0 64.24 3.77 5 5 0 73.17 3.85 5 5 0 71.54 3.88 -6 -5 0 12.27 1.59 -6 -5 0 15.08 1.75 -6 -5 0 11.68 1.38 -6 -5 0 11.21 1.34 -6 -5 0 8.21 1.32 6 5 0 11.47 1.37 6 5 0 9.81 1.3 6 5 0 12.28 1.53 6 5 0 14.28 1.73 6 5 0 13.04 1.63 6 5 0 10.46 1.43 6 5 0 11.4 1.29 -7 -5 0 34.7 2.73 -7 -5 0 37.32 2.81 -7 -5 0 33.57 2.49 -7 -5 0 39.85 2.83 -7 -5 0 36.88 2.5 7 5 0 36.64 2.48 7 5 0 34.76 2 7 5 0 34.39 2.64 7 5 0 33.86 2.52 7 5 0 40.38 2.83 7 5 0 31.41 2.57 7 5 0 35.68 2.75 7 5 0 34.38 2.27 -8 -5 0 0.93 0.54 -8 -5 0 0.4 0.6 -8 -5 0 0.23 0.54 -8 -5 0 -0.36 0.54 -8 -5 0 -0.23 0.48 8 5 0 0.19 0.41 8 5 0 0.44 0.68 8 5 0 -0.12 0.28 8 5 0 0.7 0.61 8 5 0 0.39 0.61 8 5 0 0.36 0.59 8 5 0 0.04 0.63 -9 -5 0 1.44 0.8 -9 -5 0 1.09 0.7 -9 -5 0 -0.17 0.67 -9 -5 0 -0.25 0.83 -9 -5 0 0.4 0.58 9 5 0 0.28 0.69 9 5 0 -0.63 0.49 9 5 0 1.01 0.66 9 5 0 -0.29 0.37 9 5 0 -0.88 0.54 9 5 0 1.71 1.07 9 5 0 0.8 0.54 9 5 0 0.33 0.63 -10 -5 0 0.34 0.68 -10 -5 0 -0.05 0.68 -10 -5 0 1.07 1 -10 -5 0 0.01 0.65 10 5 0 -1.41 0.48 10 5 0 0.47 0.72 10 5 0 0.48 0.93 10 5 0 0.74 0.54 10 5 0 1.33 0.61 10 5 0 0.36 0.76 -11 -5 0 0.33 0.75 -11 -5 0 0.68 1.06 -11 -5 0 -0.36 0.84 11 5 0 0.56 0.84 11 5 0 0.17 0.45 11 5 0 0.48 0.76 11 5 0 -0.27 0.47 11 5 0 0.09 0.7 -12 -5 0 0.23 0.9 -12 -5 0 -0.79 0.94 -12 -5 0 0.78 0.92 12 5 0 -0.41 0.57 12 5 0 1.19 0.88 12 5 0 0.08 0.74 12 5 0 0.36 0.84 -13 -5 0 -0.38 0.77 -13 -5 0 -0.5 1.25 -13 -5 0 -0.9 0.77 13 5 0 0.62 0.76 13 5 0 -0.06 0.4 13 5 0 -0.24 0.82 13 5 0 -1.09 0.75 13 5 0 0.66 0.86 -14 -5 0 -1.38 1.25 -14 -5 0 0.43 1.01 -14 -5 0 2.67 1.32 14 5 0 -0.23 1.06 14 5 0 0.22 0.91 14 5 0 1.95 1.05 14 5 0 0.08 0.89 12 -6 0 1.86 1.19 12 -6 0 0.09 0.87 -12 6 0 0.3 0.9 -12 6 0 0.25 0.86 -12 6 0 -0.45 1.24 11 -6 0 0.25 0.98 -11 6 0 -2.24 0.93 -11 6 0 -0.52 0.76 -11 6 0 -0.95 0.58 -11 6 0 1.11 1.06 -11 6 0 -0.21 0.68 -11 6 0 -0.71 0.65 10 -6 0 4.33 1.34 10 -6 0 0.25 0.72 -10 6 0 -0.46 1.11 -10 6 0 2.59 1.05 -10 6 0 1.15 1.02 -10 6 0 1.68 0.96 -10 6 0 2.03 0.9 -10 6 0 1.92 0.86 9 -6 0 1.63 0.86 9 -6 0 1.43 0.93 -9 6 0 1.91 0.94 -9 6 0 1.38 0.88 -9 6 0 1.03 0.72 -9 6 0 1.56 0.77 -9 6 0 3.46 1.5 -9 6 0 2.17 0.97 -9 6 0 1.62 0.77 8 -6 0 1.95 0.97 8 -6 0 1.73 1.12 8 -6 0 1.37 0.78 -8 6 0 1 0.64 -8 6 0 1.7 0.75 -8 6 0 1.07 0.79 -8 6 0 0.1 0.57 -8 6 0 1.08 0.96 -8 6 0 0.5 0.66 -8 6 0 1.45 0.74 7 -6 0 0.89 0.78 7 -6 0 0.3 0.81 7 -6 0 -0.59 0.49 7 -6 0 -0.59 0.38 -7 6 0 0.51 0.6 -7 6 0 0.85 0.6 -7 6 0 -0.44 0.48 -7 6 0 0.27 0.58 -7 6 0 0.61 0.83 -7 6 0 -1.09 0.33 -7 6 0 -0.43 0.49 6 -6 0 0.33 0.66 6 -6 0 0.77 0.51 6 -6 0 -0.21 0.35 6 -6 0 -0.65 0.65 6 -6 0 0.7 0.78 -6 6 0 1 0.66 -6 6 0 0.2 0.8 -6 6 0 0.17 0.49 -6 6 0 0.04 0.44 -6 6 0 -0.03 0.45 -6 6 0 -0.45 0.38 5 -6 0 0.16 0.63 5 -6 0 0 0.36 5 -6 0 0.64 0.41 5 -6 0 1.18 0.81 5 -6 0 -0.08 0.55 -5 6 0 -0.11 0.45 -5 6 0 0.21 0.4 -5 6 0 0.42 0.43 -5 6 0 -0.01 0.44 -5 6 0 -0.74 0.32 -5 6 0 0.1 0.36 -5 6 0 -0.3 0.66 -5 6 0 0.83 0.74 -5 6 0 0.45 0.42 4 -6 0 19.63 2.18 4 -6 0 21.46 1.6 4 -6 0 20.81 2.08 4 -6 0 19.69 1.44 4 -6 0 18.54 1.4 -4 6 0 18.16 1.37 -4 6 0 22.41 2.54 -4 6 0 17.84 1.38 -4 6 0 17.69 1.39 -4 6 0 21.98 2.11 -4 6 0 14.65 1.32 -4 6 0 18.89 1.56 -4 6 0 17.94 1.88 -4 6 0 16.07 1.77 3 -6 0 2.72 0.55 3 -6 0 3.84 1.02 3 -6 0 3.25 0.78 3 -6 0 3.72 0.82 -3 6 0 2.08 0.6 -3 6 0 2.25 0.49 -3 6 0 1.31 0.79 -3 6 0 2.51 0.75 -3 6 0 1.91 0.46 -3 6 0 3.02 0.54 -3 6 0 2.72 0.69 -3 6 0 3.02 0.79 -3 6 0 3.51 0.57 2 -6 0 23.27 1.68 2 -6 0 25.13 1.82 2 -6 0 23.23 2.31 2 -6 0 26.55 1.55 -2 6 0 24.57 1.49 -2 6 0 24.78 1.43 -2 6 0 24.76 1.82 -2 6 0 24.21 2.51 -2 6 0 25.47 1.51 -2 6 0 23.06 1.7 -2 6 0 25.34 1.48 -2 6 0 23.17 1.74 1 -6 0 190.31 9.14 1 -6 0 187.07 8.67 1 -6 0 180.8 9.34 -1 6 0 189.61 8.88 -1 6 0 191.14 8.54 -1 6 0 188.41 9.1 -1 6 0 203.15 8.67 -1 6 0 190.34 8.6 -1 6 0 192.73 8.66 -1 6 0 189.64 9.3 -1 6 0 196.17 8.78 -1 6 0 186.55 9.5 0 -6 0 0.58 0.35 0 -6 0 0.36 0.59 0 -6 0 1.53 0.54 0 -6 0 0.67 0.32 0 6 0 0.89 0.29 0 6 0 0.33 0.54 0 6 0 -0.1 0.29 0 6 0 0.99 0.3 0 6 0 0.33 0.26 0 6 0 0.56 0.25 0 6 0 0.51 0.29 0 6 0 0.48 0.51 -1 -6 0 55.63 2.83 -1 -6 0 56.87 3.27 -1 -6 0 54.41 2.54 -1 -6 0 54.85 2.54 -1 -6 0 50.2 3.33 -1 -6 0 53.14 2.86 -1 -6 0 56.78 2.91 1 6 0 57.35 2.87 1 6 0 52.95 2.88 1 6 0 59.19 2.88 1 6 0 54.29 2.57 1 6 0 56.31 2.78 1 6 0 55.78 2.58 1 6 0 50.78 3.3 1 6 0 49.19 3.28 1 6 0 58.54 2.81 -2 -6 0 2.93 0.5 -2 -6 0 3.04 0.47 -2 -6 0 2.99 0.6 -2 -6 0 2.35 0.45 -2 -6 0 1.97 0.71 -2 -6 0 3.36 0.61 -2 -6 0 1.63 0.72 2 6 0 3.04 0.56 2 6 0 2.43 0.51 2 6 0 2.38 0.54 2 6 0 2.51 0.41 2 6 0 1.41 0.68 2 6 0 2.1 0.55 -3 -6 0 5.7 0.74 -3 -6 0 4.48 0.93 -3 -6 0 3.94 0.63 -3 -6 0 4.9 0.67 -3 -6 0 5.65 0.88 -3 -6 0 4 0.67 -3 -6 0 4.47 0.82 3 6 0 6.56 0.8 3 6 0 6.29 1.09 3 6 0 7.17 0.97 3 6 0 7.94 0.93 3 6 0 5.25 1.14 3 6 0 6.33 0.94 3 6 0 6.81 0.87 -4 -6 0 31.66 1.97 -4 -6 0 28.9 2.15 -4 -6 0 28.82 2.09 -4 -6 0 30.52 2.13 -4 -6 0 29.59 1.93 4 6 0 31.57 2.02 4 6 0 33.06 2.22 4 6 0 32.15 2.51 4 6 0 28.71 1.93 4 6 0 30.39 2.09 4 6 0 27.74 2.12 4 6 0 28.69 1.93 -5 -6 0 33.43 2.27 -5 -6 0 33.11 2.39 -5 -6 0 34.5 2.42 -5 -6 0 34.93 2.18 -5 -6 0 33.01 2.2 -5 -6 0 33.2 2.28 5 6 0 35.28 2.36 5 6 0 28.05 2.17 5 6 0 30.39 2.49 5 6 0 33.78 2.2 5 6 0 31.93 2.49 5 6 0 36.77 2.5 5 6 0 37.23 3.87 -6 -6 0 1.85 0.67 -6 -6 0 3.34 0.84 -6 -6 0 1.58 0.59 -6 -6 0 2.01 0.75 -6 -6 0 0.65 0.61 6 6 0 2.45 0.65 6 6 0 1.51 0.6 6 6 0 2.99 0.83 6 6 0 1.44 0.86 6 6 0 1.81 0.69 6 6 0 1.1 0.67 6 6 0 2.52 0.73 -7 -6 0 33.48 2.66 -7 -6 0 33.95 2.41 -7 -6 0 37.1 2.54 -7 -6 0 30.38 2.59 -7 -6 0 33.59 2.67 7 6 0 35.97 2.66 7 6 0 31.48 2.56 7 6 0 31.28 2.36 7 6 0 31.29 2.66 7 6 0 36.19 2.37 7 6 0 31.43 2.45 7 6 0 34.39 2.7 -8 -6 0 1.54 0.78 -8 -6 0 0.51 0.63 -8 -6 0 0.89 0.84 -8 -6 0 -0.18 0.48 8 6 0 -0.24 0.63 8 6 0 -0.05 0.59 8 6 0 -0.44 0.56 8 6 0 0.22 0.57 8 6 0 0.33 0.46 8 6 0 0.03 0.49 8 6 0 0.5 0.37 8 6 0 0.16 0.52 -9 -6 0 -0.02 0.54 -9 -6 0 0.45 0.63 -9 -6 0 -0.03 0.55 -9 -6 0 -0.8 0.56 -9 -6 0 -0.04 0.44 9 6 0 0.48 0.71 9 6 0 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3 12 19 -0.68 0.87 -4 -12 -19 -0.23 1.39 4 12 19 0.39 0.77 4 12 19 0.23 0.87 4 12 19 -0.52 1.02 -5 -12 -19 2.04 1.31 5 12 19 0.47 0.73 5 12 19 0.46 0.98 5 12 19 4.74 1.77 -6 -12 -19 6.19 1.86 6 12 19 5.59 1.53 6 12 19 1.49 1.44 6 12 19 3.36 1.03 -7 -12 -19 0.93 1.18 -7 -12 -19 1.25 1.53 -7 -12 -19 -0.47 0.72 7 12 19 0.04 0.94 7 12 19 0.59 0.79 7 12 19 -0.19 0.99 -8 -12 -19 0.43 1.37 -8 -12 -19 1.15 1.07 -8 -12 -19 0.27 0.94 8 12 19 -0.07 0.91 8 12 19 -0.05 1.15 8 12 19 -0.47 0.63 -2 -13 -19 -0.23 0.82 2 13 19 -0.77 0.97 2 13 19 -0.02 0.79 2 13 19 0.19 0.89 -3 -13 -19 5.07 1.59 3 13 19 7.02 2.19 3 13 19 5.37 1.28 -4 -13 -19 -0.19 1.38 -4 -13 -19 -0.07 0.98 4 13 19 0.23 0.74 4 13 19 0.42 1.13 4 13 19 1.74 1.57 -5 -13 -19 1.82 1.19 5 13 19 1.09 1.35 5 13 19 0.06 0.94 5 13 19 1.57 0.82 -6 -13 -19 2.17 1.46 -6 -13 -19 0.51 1.08 -6 -13 -19 -0.29 0.8 6 13 19 -0.79 0.79 6 13 19 -0.16 0.61 6 13 19 1.34 1.26 -7 -13 -19 -0.72 1.19 -7 -13 -19 0.46 0.99 -7 -13 -19 1.46 1.12 7 13 19 0.75 1.05 7 13 19 1.76 1.7 7 13 19 0.88 0.77 -4 -14 -19 1.74 1.17 -4 -14 -19 -0.73 0.93 -5 -14 -19 0.88 1.25 -5 -14 -19 0.59 1.24 -5 -14 -19 0.11 1.01 5 14 19 0.93 1.4 -1 -4 -20 0.4 1.01 -1 -4 -20 0.8 1.51 -1 -4 -20 1.08 1.26 1 4 20 1.34 0.89 1 4 20 1.52 1.34 1 4 20 1.27 1.07 -2 -4 -20 2.37 1.49 -2 -4 -20 0.23 1.07 -2 -4 -20 1.25 1.46 2 4 20 0.92 0.74 2 4 20 1.78 1.25 2 4 20 0.36 0.96 2 4 20 2.58 1.5 -3 -4 -20 3.18 1.37 -3 -4 -20 1.51 1.83 -3 -4 -20 0.09 1.37 3 4 20 1.91 1.24 3 4 20 0.19 0.63 3 4 20 1.56 1.31 3 4 20 0.81 0.96 -4 -4 -20 -0.41 0.89 -4 -4 -20 0.27 1.17 -4 -4 -20 1.58 1.45 4 4 20 0.16 0.95 4 4 20 0.19 1.09 4 4 20 1.61 0.7 4 4 20 2.22 1.29 0 -5 -20 1.81 1.27 0 -5 -20 1.9 1.36 0 5 20 0.51 1.3 -1 -5 -20 5.13 1.65 -1 -5 -20 4.56 1.86 -1 -5 -20 2.95 1.46 1 5 20 3.19 1.12 1 5 20 2.34 1.33 1 5 20 0.59 1.4 -2 -5 -20 1.77 1.26 -2 -5 -20 2.11 1.8 -2 -5 -20 3.33 1.62 2 5 20 5.49 1.86 2 5 20 4.96 1.66 2 5 20 5 1.31 -3 -5 -20 4.44 1.51 -3 -5 -20 1.49 1.33 -3 -5 -20 3.42 2.35 3 5 20 1.51 1.27 3 5 20 2.62 0.96 3 5 20 4.33 1.58 3 5 20 1.52 1.22 -4 -5 -20 1.89 1.22 -4 -5 -20 0.98 1.3 4 5 20 0.52 1.05 4 5 20 0.74 1.07 4 5 20 -0.21 1.01 4 5 20 0.39 0.67 4 5 20 0 0.92 -5 -5 -20 3.36 1.53 -5 -5 -20 2.1 1.63 -5 -5 -20 2.68 1.27 5 5 20 0.24 1.02 5 5 20 1.47 1.24 5 5 20 1.36 1.16 5 5 20 2.41 0.84 6 5 20 -0.08 0.94 0 -6 -20 -0.12 1.06 0 -6 -20 -0.09 1.03 0 6 20 0.57 1.11 0 6 20 -0.37 0.86 0 6 20 0.86 1.25 -1 -6 -20 -0.23 0.85 -1 -6 -20 1.11 1.43 -1 -6 -20 1.92 2 1 6 20 0.51 1.27 1 6 20 0.55 0.88 1 6 20 -0.3 0.95 -2 -6 -20 0.97 1.53 -2 -6 -20 0.07 1.16 -2 -6 -20 0.5 1.01 2 6 20 -0.59 0.89 2 6 20 0.15 0.77 2 6 20 -1.03 0.78 -3 -6 -20 3.13 1.35 -3 -6 -20 1.8 1.4 3 6 20 1.9 1.3 3 6 20 1.77 1.16 3 6 20 1.85 1.04 -4 -6 -20 -0.17 0.81 -4 -6 -20 -0.18 1.24 4 6 20 1.19 0.98 4 6 20 1.61 1.24 4 6 20 1.38 0.88 -5 -6 -20 -0.87 0.84 -5 -6 -20 -0.17 1.24 -5 -6 -20 0.92 1.4 5 6 20 -0.76 0.91 5 6 20 0.15 0.98 5 6 20 0.8 0.77 5 6 20 -0.05 1.02 -6 -6 -20 0.79 1.19 -6 -6 -20 0.68 1.48 -6 -6 -20 2.01 1.12 -6 -6 -20 3.42 1.85 6 6 20 1.1 1.24 6 6 20 1.24 0.76 6 6 20 3.21 1.39 6 6 20 2.78 1.58 0 -7 -20 -0.76 0.99 0 -7 -20 0.57 0.98 0 7 20 -0.05 0.77 0 7 20 0.46 0.98 0 7 20 0.38 1.18 -1 -7 -20 -0.08 1.33 -1 -7 -20 1.14 1.27 1 7 20 -0.8 0.93 1 7 20 1.14 0.98 1 7 20 0.19 0.93 -2 -7 -20 1.67 1.44 -2 -7 -20 0.84 1.1 -2 -7 -20 0.68 1.43 2 7 20 2.12 1.23 2 7 20 0.15 1.15 2 7 20 0.35 0.82 -3 -7 -20 0.53 1.1 -3 -7 -20 -1.15 1.04 3 7 20 0.65 1.15 3 7 20 0.94 0.88 3 7 20 0.4 0.95 -4 -7 -20 1.4 1.22 -4 -7 -20 0.9 1.49 4 7 20 1.27 1.11 4 7 20 0.82 0.79 -5 -7 -20 -1.07 0.69 -5 -7 -20 1.88 1.39 5 7 20 1.58 1.31 5 7 20 -0.59 0.9 5 7 20 -0.02 0.73 -6 -7 -20 1.49 1.39 -6 -7 -20 3.82 1.66 -6 -7 -20 2.03 1.61 -6 -7 -20 0.81 1.12 6 7 20 -0.7 0.97 6 7 20 0.89 0.83 6 7 20 2.11 1.17 -7 -7 -20 1.76 1.64 -7 -7 -20 0.9 1.01 -7 -7 -20 1.81 1.21 7 7 20 1.85 1.34 7 7 20 0.04 1.09 0 -8 -20 1.72 1.32 0 -8 -20 0.14 1.03 0 -8 -20 -0.27 1.43 0 8 20 0.35 1.15 0 8 20 0.06 0.93 0 8 20 -0.06 1.03 -1 -8 -20 -0.92 0.81 -1 -8 -20 1.14 1.1 -1 -8 -20 0.04 1.3 1 8 20 -1.06 0.85 1 8 20 1.48 1.11 1 8 20 0.93 1.36 -2 -8 -20 -1.26 1.18 -2 -8 -20 -0.06 0.95 2 8 20 0.24 0.91 2 8 20 -0.1 0.86 2 8 20 -0.08 1.1 -3 -8 -20 1.4 1.23 -3 -8 -20 2.68 1.7 3 8 20 2.01 1.16 3 8 20 2.71 1.47 3 8 20 3.95 2.23 -4 -8 -20 -0.14 0.92 -4 -8 -20 1.69 1.5 4 8 20 0.72 0.92 4 8 20 -0.44 1 4 8 20 1.85 1.09 -5 -8 -20 6.11 1.93 -5 -8 -20 2.36 1.22 -5 -8 -20 4.12 2.36 5 8 20 0.55 0.97 5 8 20 2.27 1.06 5 8 20 4.99 1.74 -6 -8 -20 2.96 1.3 -6 -8 -20 2.25 1.27 -6 -8 -20 -0.2 1.2 6 8 20 1.99 1.4 6 8 20 2.78 1.07 6 8 20 3.43 1.28 -7 -8 -20 -0.03 1.47 -7 -8 -20 -0.89 1.22 -7 -8 -20 -0.82 0.8 7 8 20 0.68 0.87 7 8 20 -0.1 0.96 7 8 20 0.49 1.17 -1 -9 -20 2.63 2.36 -1 -9 -20 -0.42 0.95 -1 -9 -20 1.34 1.21 1 9 20 0.33 1.09 1 9 20 1.17 1.05 1 9 20 -0.72 0.78 -2 -9 -20 0.52 1.22 -2 -9 -20 0.95 1.41 -2 -9 -20 0.21 0.89 2 9 20 0.34 0.98 2 9 20 -0.1 1.17 2 9 20 1.03 1.03 -3 -9 -20 1.65 1.28 -3 -9 -20 1.29 1.42 3 9 20 1.72 1.4 3 9 20 2.46 1.16 3 9 20 2.62 1.12 -4 -9 -20 0.09 1.31 -4 -9 -20 0.04 1.05 4 9 20 0.45 1.04 4 9 20 1.27 0.96 4 9 20 -0.41 0.69 -5 -9 -20 0.94 1.17 -5 -9 -20 0.03 1.33 -5 -9 -20 1.14 1.22 5 9 20 0.08 0.92 5 9 20 -0.45 0.8 5 9 20 -0.58 0.94 -6 -9 -20 -0.76 0.76 -6 -9 -20 0.54 1.34 6 9 20 -0.82 0.89 6 9 20 0.21 0.83 6 9 20 0.22 0.78 -7 -9 -20 -0.52 0.94 -7 -9 -20 1.28 1.1 -7 -9 -20 -1.19 1.98 7 9 20 1.29 1.01 7 9 20 0.31 0.9 7 9 20 0.93 1.3 -1 -10 -20 2.39 1.9 -1 -10 -20 1.36 1.19 -1 -10 -20 1.87 1.28 1 10 20 3.05 1.44 1 10 20 3.01 1.72 1 10 20 2.2 1.28 -2 -10 -20 -0.2 0.97 -2 -10 -20 0.44 1.05 -2 -10 -20 0.84 1.54 2 10 20 1.21 1.09 2 10 20 0.62 0.99 2 10 20 0.9 1.31 -3 -10 -20 -0.29 0.91 -3 -10 -20 -1.38 0.79 -3 -10 -20 -1.54 1.16 3 10 20 0.3 0.93 3 10 20 -0.11 1.04 -4 -10 -20 1.67 1.45 -4 -10 -20 2.62 1.79 4 10 20 1.76 1.17 4 10 20 0.8 0.94 4 10 20 2.35 1.51 -5 -10 -20 -0.28 0.96 -5 -10 -20 0.01 0.97 5 10 20 -0.24 0.85 5 10 20 -0.18 1 5 10 20 -0.75 0.73 -6 -10 -20 -0.64 0.84 -6 -10 -20 -0.4 0.96 -6 -10 -20 0.64 1.22 6 10 20 0.35 0.89 6 10 20 -0.17 0.77 6 10 20 0.2 1.19 -7 -10 -20 1.01 1.15 -7 -10 -20 0.01 0.96 7 10 20 0.6 1.24 7 10 20 -0.22 0.79 -2 -11 -20 1.07 1.28 -2 -11 -20 0.36 1.03 2 11 20 1.87 1.84 2 11 20 0.1 1.03 2 11 20 -0.43 1.21 -3 -11 -20 2.86 1.45 -3 -11 -20 1.85 1.56 -3 -11 -20 -0.02 0.87 3 11 20 1.01 1.05 3 11 20 -0.94 1.02 3 11 20 1.59 1.03 -4 -11 -20 1.05 1.15 4 11 20 0.76 1.05 4 11 20 2.92 1.59 4 11 20 4.16 1.29 -5 -11 -20 -1.12 0.79 -5 -11 -20 0.71 1.17 5 11 20 0.69 1.33 5 11 20 -0.64 0.79 5 11 20 0.7 0.89 -6 -11 -20 1.34 1.36 -6 -11 -20 -0.41 0.99 -6 -11 -20 1.22 1.32 6 11 20 -0.02 1.16 6 11 20 -0.35 0.84 6 11 20 0.51 0.85 -4 -12 -20 -0.04 1.04 4 12 20 2.64 1.63 -5 -12 -20 -0.63 0.81 -5 -12 -20 -1.1 0.91 5 12 20 -0.83 1.02 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O12 K1 O1 108.92(6) . . ? O7 K1 O1 107.56(6) . . ? O7 K1 O12 59.59(5) . . ? O5 K1 O1 115.58(6) . . ? O5 K1 O12 75.62(6) . . ? O5 K1 O7 125.51(6) . . ? O4 K1 O1 153.40(6) . . ? O4 K1 O12 96.16(6) . . ? O4 K1 O7 92.51(6) . . ? O4 K1 O5 61.50(6) . . ? O3 K1 O1 98.90(6) . . ? O3 K1 O12 150.25(6) . . ? O3 K1 O7 102.48(6) . . ? O3 K1 O5 102.06(6) . . ? O3 K1 O4 58.85(6) . . ? O2 K1 O1 58.53(6) . . ? O2 K1 O12 129.93(6) . . ? O2 K1 O7 77.61(6) . . ? O2 K1 O5 154.31(6) . . ? O2 K1 O4 111.38(6) . . ? O2 K1 O3 57.91(6) . . ? O6 K1 O1 57.61(6) . . ? O6 K1 O12 94.80(6) . . ? O6 K1 O7 146.49(6) . . ? O6 K1 O5 57.98(6) . . ? O6 K1 O4 112.85(6) . . ? O6 K1 O3 109.23(6) . . ? O6 K1 O2 110.36(6) . . ? C24 K1 O1 156.50(8) . . ? C24 K1 O12 78.01(7) . . ? C24 K1 O7 95.37(7) . . ? C24 K1 O5 42.97(7) . . ? C24 K1 O4 23.07(7) . . ? C24 K1 O3 80.64(7) . . ? C24 K1 O2 134.36(7) . . ? C24 K1 O6 100.09(8) . . ? C30 K1 O1 94.80(7) . . ? C30 K1 O12 43.49(6) . . ? C30 K1 O7 24.09(6) . . ? C30 K1 O5 118.56(7) . . ? C30 K1 O4 109.83(7) . . ? C30 K1 O3 125.49(7) . . ? C30 K1 O2 87.12(7) . . ? C30 K1 O6 122.43(7) . . ? C30 K1 C24 104.62(8) . . ? C17 O1 K1 120.24(17) . . ? C18 O1 K1 121.26(17) . . ? C18 O1 C17 110.6(2) . . ? C40 O12 K1 129.68(16) . . ? C29 O12 K1 117.02(15) . . ? C29 O12 C40 113.3(2) . . ? C32 O8 C39 112.9(2) . 2_565 ? C31 O7 K1 118.20(15) . . ? C30 O7 K1 99.03(16) . . ? C30 O7 C31 113.8(2) . . ? C26 O5 K1 122.27(18) . . ? C25 O5 K1 117.59(18) . . ? C25 O5 C26 113.7(2) . . ? C24 O4 K1 107.72(16) . . ? C100 O4 K1 113.10(16) . . ? C100 O4 C24 114.5(2) . . ? C22 O3 K1 116.65(16) . . ? C21 O3 K1 118.89(17) . . ? C21 O3 C22 112.7(2) . . ? C20 O2 K1 114.53(17) . . ? C19 O2 K1 109.88(18) . . ? C19 O2 C20 114.0(2) . . ? C101 O6 K1 109.30(16) . . ? C28 O6 K1 110.02(16) . . ? C28 O6 C101 111.8(2) . . ? C7 C6 H6 120.26(19) . . ? C5 C6 H6 120.26(19) . . ? C5 C6 C7 119.5(3) . . ? H7 C7 C6 120.20(19) . . ? C8 C7 C6 119.6(3) . . ? C8 C7 H7 120.20(19) . . ? H8 C8 C7 119.37(19) . . ? C3 C8 C7 121.3(3) . . ? C3 C8 H8 119.37(16) . . ? C2 C3 C8 121.0(2) . . ? C4 C3 C8 118.6(3) . . ? C4 C3 C2 120.4(2) . . ? C1 C2 C3 118.84(19) . . ? B15 C2 C3 118.7(2) . . ? B15 C2 C1 60.01(15) . . ? B12 C2 C3 117.8(2) . . ? B12 C2 C1 60.20(14) . . ? B12 C2 B15 111.18(19) . . ? B20 C2 C3 120.8(2) . . ? B20 C2 C1 110.57(18) . . ? B20 C2 B15 113.1(2) . . ? B20 C2 B12 62.66(16) . . ? B19 C2 C3 121.3(2) . . ? B19 C2 C1 110.45(19) . . ? B19 C2 B15 62.66(17) . . ? B19 C2 B12 113.1(2) . . ? B19 C2 B20 62.14(17) . . ? B1 C1 C2 116.37(19) . . ? B15 C1 C2 59.12(14) . . ? B15 C1 B1 121.24(19) . . ? B14 C1 C2 107.57(18) . . ? B14 C1 B1 128.2(2) . . ? B14 C1 B15 61.59(16) . . ? B12 C1 C2 59.05(14) . . ? B12 C1 B1 114.12(19) . . ? B12 C1 B15 109.47(18) . . ? B12 C1 B14 111.24(19) . . ? B13 C1 C2 107.56(18) . . ? B13 C1 B1 123.14(19) . . ? B13 C1 B15 111.47(19) . . ? B13 C1 B14 62.00(16) . . ? B13 C1 B12 61.45(15) . . ? H1 B1 C1 107.01(13) . . ? C16 B1 C1 116.7(2) . . ? C16 B1 H1 107.01(13) . . ? C9 B1 C1 117.47(19) . . ? C9 B1 H1 107.01(13) . . ? C9 B1 C16 100.94(19) . . ? C11 C16 B1 113.5(2) . . ? C15 C16 B1 130.3(2) . . ? C15 C16 C11 115.9(2) . . ? C12 C11 C16 123.6(2) . . ? C10 C11 C16 113.3(2) . . ? C10 C11 C12 123.1(2) . . ? H12 C12 C11 120.64(15) . . ? C13 C12 C11 118.7(2) . . ? C13 C12 H12 120.64(15) . . ? H13 C13 C12 120.18(15) . . ? C14 C13 C12 119.6(2) . . ? C14 C13 H13 120.18(15) . . ? H4 C4 C3 120.02(16) . . ? C5 C4 C3 120.0(3) . . ? C5 C4 H4 120.02(18) . . ? C4 C5 C6 121.0(3) . . ? H5 C5 C6 119.48(19) . . ? H5 C5 C4 119.48(18) . . ? C10 C9 B1 104.61(17) . . ? B6 C9 B1 129.6(2) . . ? B6 C9 C10 108.67(19) . . ? B5 C9 B1 107.70(19) . . ? B5 C9 C10 60.37(15) . . ? B5 C9 B6 61.35(17) . . ? B2 C9 B1 117.21(19) . . ? B2 C9 C10 60.32(15) . . ? B2 C9 B6 111.95(19) . . ? B2 C9 B5 111.7(2) . . ? B7 C9 B1 137.6(2) . . ? B7 C9 C10 108.12(19) . . ? B7 C9 B6 62.00(16) . . ? B7 C9 B5 111.54(19) . . ? B7 C9 B2 61.06(16) . . ? H15 C15 C16 119.43(15) . . ? C14 C15 C16 121.1(2) . . ? C14 C15 H15 119.43(15) . . ? C15 C14 C13 121.0(2) . . ? H14 C14 C13 119.50(15) . . ? H14 C14 C15 119.50(15) . . ? C9 C10 C11 106.83(18) . . ? B3 C10 C11 127.2(2) . . ? B3 C10 C9 113.4(2) . . ? B4 C10 C11 127.9(2) . . ? B4 C10 C9 112.94(19) . . ? B4 C10 B3 63.15(18) . . ? B5 C10 C11 113.7(2) . . ? B5 C10 C9 61.88(16) . . ? B5 C10 B3 114.78(19) . . ? B5 C10 B4 62.42(17) . . ? B2 C10 C11 112.86(19) . . ? B2 C10 C9 61.52(15) . . ? B2 C10 B3 63.34(17) . . ? B2 C10 B4 115.1(2) . . ? B2 C10 B5 113.9(2) . . ? H17a C17 O1 109.69(16) . . ? H17b C17 O1 109.69(15) . . ? H17b C17 H17a 108.2 . . ? C28 C17 O1 109.9(2) . . ? C28 C17 H17a 109.69(16) . . ? C28 C17 H17b 109.69(18) . . ? H40a C40 O12 108.53(14) . . ? H40b C40 O12 108.53(15) . . ? H40b C40 H40a 107.5 . . ? C39 C40 O12 115.0(2) . . ? C39 C40 H40a 108.53(16) . . ? C39 C40 H40b 108.53(15) . . ? C40 C39 O8 109.7(2) . 2_565 ? H39a C39 O8 109.73(14) . 2_565 ? H39a C39 C40 109.73(16) . . ? H39b C39 O8 109.73(14) . 2_565 ? H39b C39 C40 109.73(15) . . ? H39b C39 H39a 108.2 . . ? H32a C32 O8 109.82(15) . . ? H32b C32 O8 109.82(14) . . ? H32b C32 H32a 108.3 . . ? C31 C32 O8 109.3(2) . . ? C31 C32 H32a 109.82(16) . . ? C31 C32 H32b 109.82(16) . . ? C32 C31 O7 109.0(2) . . ? H31a C31 O7 109.89(14) . . ? H31a C31 C32 109.89(16) . . ? H31b C31 O7 109.89(14) . . ? H31b C31 C32 109.89(15) . . ? H31b C31 H31a 108.3 . . ? H10a C101 O6 109.66(15) . . ? H10b C101 O6 109.66(15) . . ? H10b C101 H10a 108.2 . . ? C26 C101 O6 110.0(3) . . ? C26 C101 H10a 109.66(17) . . ? C26 C101 H10b 109.66(18) . . ? C101 C26 O5 108.6(3) . . ? H26a C26 O5 109.97(16) . . ? H26a C26 C101 109.97(17) . . ? H26b C26 O5 109.97(16) . . ? H26b C26 C101 109.97(18) . . ? H26b C26 H26a 108.3 . . ? H25a C25 O5 109.91(16) . . ? H25b C25 O5 109.91(16) . . ? H25b C25 H25a 108.3 . . ? C24 C25 O5 108.9(3) . . ? C24 C25 H25a 109.91(18) . . ? C24 C25 H25b 109.91(18) . . ? O4 C24 K1 49.21(13) . . ? C25 C24 K1 87.08(18) . . ? C25 C24 O4 114.6(3) . . ? H24a C24 K1 157.60(6) . . ? H24a C24 O4 108.60(15) . . ? H24a C24 C25 108.60(17) . . ? H24b C24 K1 81.15(5) . . ? H24b C24 O4 108.60(16) . . ? H24b C24 C25 108.60(18) . . ? H24b C24 H24a 107.6 . . ? H10c C100 O4 110.34(16) . . ? H10d C100 O4 110.34(15) . . ? H10d C100 H10c 108.6 . . ? C22 C100 O4 106.9(3) . . ? C22 C100 H10c 110.34(17) . . ? C22 C100 H10d 110.34(16) . . ? C100 C22 O3 108.8(2) . . ? H22a C22 O3 109.93(16) . . ? H22a C22 C100 109.93(17) . . ? H22b C22 O3 109.93(14) . . ? H22b C22 C100 109.93(16) . . ? H22b C22 H22a 108.3 . . ? H21a C21 O3 109.83(14) . . ? H21b C21 O3 109.83(14) . . ? H21b C21 H21a 108.3 . . ? C20 C21 O3 109.2(2) . . ? C20 C21 H21a 109.83(16) . . ? C20 C21 H21b 109.83(17) . . ? C21 C20 O2 109.8(2) . . ? H20a C20 O2 109.70(16) . . ? H20a C20 C21 109.70(17) . . ? H20b C20 O2 109.70(16) . . ? H20b C20 C21 109.70(17) . . ? H20b C20 H20a 108.2 . . ? H19a C19 O2 108.78(17) . . ? H19b C19 O2 108.78(17) . . ? H19b C19 H19a 107.7 . . ? C18 C19 O2 113.9(3) . . ? C18 C19 H19a 108.78(18) . . ? C18 C19 H19b 108.8(2) . . ? C19 C18 O1 108.7(3) . . ? H18a C18 O1 109.95(16) . . ? H18a C18 C19 109.95(19) . . ? H18b C18 O1 109.95(18) . . ? H18b C18 C19 109.9(2) . . ? H18b C18 H18a 108.3 . . ? H29a C29 O12 109.55(14) . . ? H29b C29 O12 109.55(15) . . ? H29b C29 H29a 108.1 . . ? C30 C29 O12 110.5(2) . . ? C30 C29 H29a 109.55(16) . . ? C30 C29 H29b 109.55(17) . . ? O7 C30 K1 56.88(13) . . ? C29 C30 K1 86.98(16) . . ? C29 C30 O7 109.5(2) . . ? H30a C30 K1 162.18(5) . . ? H30a C30 O7 109.76(15) . . ? H30a C30 C29 109.76(16) . . ? H30b C30 K1 69.93(5) . . ? H30b C30 O7 109.76(15) . . ? H30b C30 C29 109.76(17) . . ? H30b C30 H30a 108.2 . . ? C17 C28 O6 109.6(2) . . ? H28a C28 O6 109.75(15) . . ? H28a C28 C17 109.75(17) . . ? H28b C28 O6 109.75(15) . . ? H28b C28 C17 109.75(18) . . ? H28b C28 H28a 108.2 . . ? C1 B15 C2 60.87(14) . . ? H15a B15 C2 120.7(15) . . ? H15a B15 C1 120.2(14) . . ? B14 B15 C2 106.6(2) . . ? B14 B15 C1 58.56(15) . . ? B14 B15 H15a 123.5(15) . . ? B18 B15 C2 105.3(2) . . ? B18 B15 C1 106.5(2) . . ? B18 B15 H15a 125.4(15) . . ? B18 B15 B14 60.10(18) . . ? B19 B15 C2 58.37(16) . . ? B19 B15 C1 107.73(19) . . ? B19 B15 H15a 122.3(15) . . ? B19 B15 B14 107.7(2) . . ? B19 B15 B18 59.51(18) . . ? B15 B14 C1 59.86(16) . . ? H14a B14 C1 118.5(14) . . ? H14a B14 B15 119.0(14) . . ? B18 B14 C1 107.7(2) . . ? B18 B14 B15 60.32(18) . . ? B18 B14 H14a 123.8(14) . . ? B17 B14 C1 107.1(2) . . ? B17 B14 B15 108.2(2) . . ? B17 B14 H14a 125.7(14) . . ? B17 B14 B18 60.23(18) . . ? B13 B14 C1 59.15(15) . . ? B13 B14 B15 107.8(2) . . ? B13 B14 H14a 121.6(14) . . ? B13 B14 B18 108.4(2) . . ? B13 B14 B17 60.17(16) . . ? B14 B18 B15 59.58(17) . . ? H18 B18 B15 119.9(14) . . ? H18 B18 B14 123.8(14) . . ? B21 B18 B15 107.7(2) . . ? B21 B18 B14 107.2(2) . . ? B21 B18 H18 122.2(14) . . ? B19 B18 B15 60.37(18) . . ? B19 B18 B14 108.0(2) . . ? B19 B18 H18 118.5(15) . . ? B19 B18 B21 59.99(18) . . ? B17 B18 B15 107.3(2) . . ? B17 B18 B14 59.76(17) . . ? B17 B18 H18 125.3(15) . . ? B17 B18 B21 59.36(17) . . ? B17 B18 B19 107.6(2) . . ? H3 B3 C10 118.3(15) . . ? B8 B3 C10 104.3(2) . . ? B8 B3 H3 127.7(15) . . ? B4 B3 C10 58.61(16) . . ? B4 B3 H3 119.4(15) . . ? B4 B3 B8 107.8(2) . . ? B9 B3 C10 104.1(2) . . ? B9 B3 H3 128.1(15) . . ? B9 B3 B8 60.16(18) . . ? B9 B3 B4 59.58(18) . . ? B2 B3 C10 58.73(16) . . ? B2 B3 H3 119.6(15) . . ? B2 B3 B8 59.31(17) . . ? B2 B3 B4 107.7(2) . . ? B2 B3 B9 107.2(2) . . ? H8a B8 B3 123.2(14) . . ? B11 B8 B3 107.9(2) . . ? B11 B8 H8a 122.1(14) . . ? B9 B8 B3 59.75(18) . . ? B9 B8 H8a 124.9(14) . . ? B9 B8 B11 60.00(19) . . ? B2 B8 B3 60.59(17) . . ? B2 B8 H8a 119.9(14) . . ? B2 B8 B11 107.3(2) . . ? B2 B8 B9 107.9(2) . . ? B7 B8 B3 107.9(2) . . ? B7 B8 H8a 119.1(14) . . ? B7 B8 B11 59.91(17) . . ? B7 B8 B9 107.8(2) . . ? B7 B8 B2 59.18(16) . . ? H11 B11 B8 122.3(15) . . ? B6 B11 B8 108.1(2) . . ? B6 B11 H11 120.7(15) . . ? B10 B11 B8 108.1(2) . . ? B10 B11 H11 121.4(15) . . ? B10 B11 B6 60.45(18) . . ? B9 B11 B8 59.95(19) . . ? B9 B11 H11 122.6(14) . . ? B9 B11 B6 108.2(2) . . ? B9 B11 B10 59.98(19) . . ? B7 B11 B8 60.15(17) . . ? B7 B11 H11 121.4(14) . . ? B7 B11 B6 59.64(17) . . ? B7 B11 B10 108.0(2) . . ? B7 B11 B9 107.9(2) . . ? B11 B6 C9 105.7(2) . . ? H6a B6 C9 120.6(13) . . ? H6a B6 B11 126.0(13) . . ? B10 B6 C9 105.8(2) . . ? B10 B6 B11 59.62(18) . . ? B10 B6 H6a 123.5(14) . . ? B5 B6 C9 59.93(15) . . ? B5 B6 B11 106.8(2) . . ? B5 B6 H6a 119.1(13) . . ? B5 B6 B10 58.88(17) . . ? B7 B6 C9 58.99(15) . . ? B7 B6 B11 60.09(17) . . ? B7 B6 H6a 122.6(14) . . ? B7 B6 B10 107.7(2) . . ? B7 B6 B5 108.0(2) . . ? B3 B4 C10 58.25(16) . . ? H4a B4 C10 114.4(14) . . ? H4a B4 B3 118.7(15) . . ? B10 B4 C10 104.5(2) . . ? B10 B4 B3 108.4(2) . . ? B10 B4 H4a 129.6(14) . . ? B9 B4 C10 104.2(2) . . ? B9 B4 B3 60.05(18) . . ? B9 B4 H4a 131.7(14) . . ? B9 B4 B10 60.39(18) . . ? B5 B4 C10 59.25(16) . . ? B5 B4 B3 108.2(2) . . ? B5 B4 H4a 116.5(14) . . ? B5 B4 B10 59.18(17) . . ? B5 B4 B9 107.6(2) . . ? B6 B10 B11 59.94(18) . . ? B4 B10 B11 107.8(2) . . ? B4 B10 B6 108.1(2) . . ? H10 B10 B11 122.8(15) . . ? H10 B10 B6 122.6(15) . . ? H10 B10 B4 120.6(15) . . ? B9 B10 B11 60.07(19) . . ? B9 B10 B6 107.9(2) . . ? B9 B10 B4 59.54(19) . . ? B9 B10 H10 121.7(15) . . ? B5 B10 B11 107.8(2) . . ? B5 B10 B6 59.82(17) . . ? B5 B10 B4 60.36(17) . . ? B5 B10 H10 121.2(15) . . ? B5 B10 B9 107.8(2) . . ? B8 B9 B3 60.09(18) . . ? B11 B9 B3 108.2(2) . . ? B11 B9 B8 60.05(18) . . ? B4 B9 B3 60.37(18) . . ? B4 B9 B8 108.4(2) . . ? B4 B9 B11 108.1(2) . . ? B10 B9 B3 108.4(2) . . ? B10 B9 B8 108.2(2) . . ? B10 B9 B11 59.95(19) . . ? B10 B9 B4 60.07(18) . . ? H9 B9 B3 120.1(16) . . ? H9 B9 B8 121.3(16) . . ? H9 B9 B11 122.9(16) . . ? H9 B9 B4 120.9(16) . . ? H9 B9 B10 122.6(16) . . ? C10 B5 C9 57.75(14) . . ? B6 B5 C9 58.73(15) . . ? B6 B5 C10 104.5(2) . . ? B4 B5 C9 106.2(2) . . ? B4 B5 C10 58.33(16) . . ? B4 B5 B6 109.3(2) . . ? B10 B5 C9 106.7(2) . . ? B10 B5 C10 104.8(2) . . ? B10 B5 B6 61.30(18) . . ? B10 B5 B4 60.45(17) . . ? H5a B5 C9 119.2(14) . . ? H5a B5 C10 115.6(14) . . ? H5a B5 B6 128.5(14) . . ? H5a B5 B4 118.6(14) . . ? H5a B5 B10 129.9(14) . . ? C10 B2 C9 58.16(15) . . ? B3 B2 C9 106.2(2) . . ? B3 B2 C10 57.93(16) . . ? B8 B2 C9 106.8(2) . . ? B8 B2 C10 104.3(2) . . ? B8 B2 B3 60.10(17) . . ? H2 B2 C9 116.9(13) . . ? H2 B2 C10 117.3(13) . . ? H2 B2 B3 122.3(13) . . ? H2 B2 B8 130.6(13) . . ? B7 B2 C9 59.24(15) . . ? B7 B2 C10 105.0(2) . . ? B7 B2 B3 108.9(2) . . ? B7 B2 B8 61.01(17) . . ? B7 B2 H2 125.2(13) . . ? B8 B7 C9 106.3(2) . . ? B11 B7 C9 105.9(2) . . ? B11 B7 B8 59.94(18) . . ? B6 B7 C9 59.02(15) . . ? B6 B7 B8 108.4(2) . . ? B6 B7 B11 60.27(17) . . ? B2 B7 C9 59.70(15) . . ? B2 B7 B8 59.81(17) . . ? B2 B7 B11 107.8(2) . . ? B2 B7 B6 108.4(2) . . ? H7a B7 C9 116.4(13) . . ? H7a B7 B8 127.6(14) . . ? H7a B7 B11 127.8(13) . . ? H7a B7 B6 118.8(14) . . ? H7a B7 B2 119.0(13) . . ? C1 B12 C2 60.75(14) . . ? H12a B12 C2 118.2(13) . . ? H12a B12 C1 117.7(13) . . ? B16 B12 C2 105.4(2) . . ? B16 B12 C1 106.4(2) . . ? B16 B12 H12a 128.6(13) . . ? B20 B12 C2 58.34(15) . . ? B20 B12 C1 107.58(19) . . ? B20 B12 H12a 123.2(13) . . ? B20 B12 B16 59.73(17) . . ? B13 B12 C2 106.66(19) . . ? B13 B12 C1 58.61(15) . . ? B13 B12 H12a 124.0(13) . . ? B13 B12 B16 59.99(17) . . ? B13 B12 B20 107.8(2) . . ? H16 B16 B12 121.2(13) . . ? B21 B16 B12 108.1(2) . . ? B21 B16 H16 123.1(13) . . ? B20 B16 B12 60.61(17) . . ? B20 B16 H16 123.1(13) . . ? B20 B16 B21 59.81(18) . . ? B17 B16 B12 107.8(2) . . ? B17 B16 H16 121.3(13) . . ? B17 B16 B21 59.55(18) . . ? B17 B16 B20 107.6(2) . . ? B13 B16 B12 60.02(16) . . ? B13 B16 H16 119.8(13) . . ? B13 B16 B21 107.9(2) . . ? B13 B16 B20 108.6(2) . . ? B13 B16 B17 60.01(17) . . ? B16 B21 B18 108.2(2) . . ? H21 B21 B18 121.9(14) . . ? H21 B21 B16 120.9(14) . . ? B20 B21 B18 107.7(2) . . ? B20 B21 B16 59.98(17) . . ? B20 B21 H21 122.4(15) . . ? B19 B21 B18 59.60(18) . . ? B19 B21 B16 107.7(2) . . ? B19 B21 H21 123.2(14) . . ? B19 B21 B20 59.79(17) . . ? B17 B21 B18 60.22(18) . . ? B17 B21 B16 60.41(17) . . ? B17 B21 H21 120.3(15) . . ? B17 B21 B20 108.4(2) . . ? B17 B21 B19 107.9(2) . . ? B12 B20 C2 59.00(15) . . ? B16 B20 C2 105.9(2) . . ? B16 B20 B12 59.67(16) . . ? B21 B20 C2 106.1(2) . . ? B21 B20 B12 107.7(2) . . ? B21 B20 B16 60.22(17) . . ? H20 B20 C2 116.8(15) . . ? H20 B20 B12 118.5(14) . . ? H20 B20 B16 126.7(14) . . ? H20 B20 B21 128.2(15) . . ? B19 B20 C2 58.93(16) . . ? B19 B20 B12 107.5(2) . . ? B19 B20 B16 108.4(2) . . ? B19 B20 B21 60.39(18) . . ? B19 B20 H20 120.2(14) . . ? B15 B19 C2 58.97(16) . . ? B18 B19 C2 106.3(2) . . ? B18 B19 B15 60.12(18) . . ? B21 B19 C2 105.6(2) . . ? B21 B19 B15 107.9(2) . . ? B21 B19 B18 60.41(18) . . ? B20 B19 C2 58.93(16) . . ? B20 B19 B15 107.5(2) . . ? B20 B19 B18 108.4(2) . . ? B20 B19 B21 59.83(17) . . ? H19 B19 C2 116.5(15) . . ? H19 B19 B15 119.7(15) . . ? H19 B19 B18 127.7(15) . . ? H19 B19 B21 127.7(15) . . ? H19 B19 B20 118.8(15) . . ? B18 B17 B14 60.01(17) . . ? B16 B17 B14 107.5(2) . . ? B16 B17 B18 108.1(2) . . ? B21 B17 B14 108.3(2) . . ? B21 B17 B18 60.43(18) . . ? B21 B17 B16 60.05(17) . . ? H17 B17 B14 119.6(14) . . ? H17 B17 B18 122.2(14) . . ? H17 B17 B16 122.8(14) . . ? H17 B17 B21 124.0(14) . . ? B13 B17 B14 59.81(16) . . ? B13 B17 B18 108.0(2) . . ? B13 B17 B16 59.67(17) . . ? B13 B17 B21 108.1(2) . . ? B13 B17 H17 119.8(14) . . ? B14 B13 C1 58.86(15) . . ? B12 B13 C1 59.93(15) . . ? B12 B13 B14 107.5(2) . . ? B16 B13 C1 107.4(2) . . ? B16 B13 B14 108.2(2) . . ? B16 B13 B12 59.99(17) . . ? B17 B13 C1 106.7(2) . . ? B17 B13 B14 60.02(16) . . ? B17 B13 B12 108.0(2) . . ? B17 B13 B16 60.32(17) . . ? H13a B13 C1 116.8(13) . . ? H13a B13 B14 122.5(13) . . ? H13a B13 B12 117.1(13) . . ? H13a B13 B16 124.5(13) . . ? H13a B13 B17 128.3(13) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag K1 O1 2.861(2) . ? K1 O12 2.8006(18) . ? K1 O7 2.9122(19) . ? K1 O5 2.804(2) . ? K1 O4 2.747(2) . ? K1 O3 2.872(2) . ? K1 O2 2.893(2) . ? K1 O6 2.955(2) . ? K1 C24 3.457(3) . ? K1 C30 3.434(3) . ? O1 C17 1.411(4) . ? O1 C18 1.415(4) . ? O12 C40 1.426(3) . ? O12 C29 1.417(3) . ? O8 C39 1.411(3) 2_565 ? O8 C32 1.420(3) . ? O7 C31 1.417(3) . ? O7 C30 1.419(3) . ? O5 C26 1.410(4) . ? O5 C25 1.432(4) . ? O4 C24 1.422(4) . ? O4 C100 1.432(3) . ? O3 C22 1.409(4) . ? O3 C21 1.437(4) . ? O2 C20 1.409(4) . ? O2 C19 1.440(4) . ? O6 C101 1.422(4) . ? O6 C28 1.418(3) . ? C6 H6 0.9300 . ? C6 C7 1.387(5) . ? C6 C5 1.373(5) . ? C7 H7 0.9300 . ? C7 C8 1.386(4) . ? C8 H8 0.9300 . ? C8 C3 1.384(4) . ? C3 C2 1.506(3) . ? C3 C4 1.393(4) . ? C2 C1 1.750(3) . ? C2 B15 1.720(4) . ? C2 B12 1.721(4) . ? C2 B20 1.709(4) . ? C2 B19 1.709(4) . ? C1 B1 1.634(4) . ? C1 B15 1.735(4) . ? C1 B14 1.712(4) . ? C1 B12 1.741(3) . ? C1 B13 1.717(4) . ? B1 H1 0.9800 . ? B1 C16 1.628(4) . ? B1 C9 1.671(3) . ? C16 C11 1.401(3) . ? C16 C15 1.403(3) . ? C11 C12 1.387(3) . ? C11 C10 1.487(3) . ? C12 H12 0.9300 . ? C12 C13 1.382(4) . ? C13 H13 0.9300 . ? C13 C14 1.385(4) . ? C4 H4 0.9300 . ? C4 C5 1.385(4) . ? C5 H5 0.9300 . ? C9 C10 1.671(3) . ? C9 B6 1.721(4) . ? C9 B5 1.743(4) . ? C9 B2 1.729(4) . ? C9 B7 1.721(4) . ? C15 H15 0.9300 . ? C15 C14 1.388(3) . ? C14 H14 0.9300 . ? C10 B3 1.694(4) . ? C10 B4 1.701(4) . ? C10 B5 1.718(4) . ? C10 B2 1.709(4) . ? C17 H17a 0.9700 . ? C17 H17b 0.9700 . ? C17 C28 1.476(4) . ? C40 H40a 0.9700 . ? C40 H40b 0.9700 . ? C40 C39 1.507(4) . ? C39 H39a 0.9700 . ? C39 H39b 0.9700 . ? C32 H32a 0.9700 . ? C32 H32b 0.9700 . ? C32 C31 1.492(4) . ? C31 H31a 0.9700 . ? C31 H31b 0.9700 . ? C101 H10a 0.9700 . ? C101 H10b 0.9700 . ? C101 C26 1.492(5) . ? C26 H26a 0.9700 . ? C26 H26b 0.9700 . ? C25 H25a 0.9700 . ? C25 H25b 0.9700 . ? C25 C24 1.484(5) . ? C24 H24a 0.9700 . ? C24 H24b 0.9700 . ? C100 H10c 0.9700 . ? C100 H10d 0.9700 . ? C100 C22 1.497(5) . ? C22 H22a 0.9700 . ? C22 H22b 0.9700 . ? C21 H21a 0.9700 . ? C21 H21b 0.9700 . ? C21 C20 1.486(5) . ? C20 H20a 0.9700 . ? C20 H20b 0.9700 . ? C19 H19a 0.9700 . ? C19 H19b 0.9700 . ? C19 C18 1.466(5) . ? C18 H18a 0.9700 . ? C18 H18b 0.9700 . ? C29 H29a 0.9700 . ? C29 H29b 0.9700 . ? C29 C30 1.484(4) . ? C30 H30a 0.9700 . ? C30 H30b 0.9700 . ? C28 H28a 0.9700 . ? C28 H28b 0.9700 . ? B15 H15a 1.03(3) . ? B15 B14 1.765(4) . ? B15 B18 1.778(4) . ? B15 B19 1.783(4) . ? B14 H14a 1.08(3) . ? B14 B18 1.774(4) . ? B14 B17 1.770(4) . ? B14 B13 1.766(4) . ? B18 H18 1.10(3) . ? B18 B21 1.782(4) . ? B18 B19 1.767(5) . ? B18 B17 1.778(4) . ? B3 H3 1.05(3) . ? B3 B8 1.778(5) . ? B3 B4 1.778(5) . ? B3 B9 1.772(4) . ? B3 B2 1.787(4) . ? B8 H8a 1.13(3) . ? B8 B11 1.781(5) . ? B8 B9 1.779(5) . ? B8 B2 1.764(4) . ? B8 B7 1.785(5) . ? B11 H11 1.09(3) . ? B11 B6 1.784(4) . ? B11 B10 1.778(5) . ? B11 B9 1.780(5) . ? B11 B7 1.781(4) . ? B6 H6a 1.11(3) . ? B6 B10 1.793(4) . ? B6 B5 1.767(4) . ? B6 B7 1.773(4) . ? B4 H4a 1.10(3) . ? B4 B10 1.773(4) . ? B4 B9 1.764(5) . ? B4 B5 1.771(4) . ? B10 H10 1.06(3) . ? B10 B9 1.779(5) . ? B10 B5 1.750(4) . ? B9 H9 1.01(3) . ? B5 H5a 1.06(3) . ? B2 H2 1.11(3) . ? B2 B7 1.753(4) . ? B7 H7a 1.13(3) . ? B12 H12a 1.09(2) . ? B12 B16 1.766(4) . ? B12 B20 1.783(4) . ? B12 B13 1.767(4) . ? B16 H16 1.12(3) . ? B16 B21 1.772(4) . ? B16 B20 1.767(4) . ? B16 B17 1.778(4) . ? B16 B13 1.766(4) . ? B21 H21 1.08(3) . ? B21 B20 1.764(5) . ? B21 B19 1.774(5) . ? B21 B17 1.763(5) . ? B20 H20 1.05(3) . ? B20 B19 1.764(4) . ? B19 H19 1.03(3) . ? B17 H17 1.08(3) . ? B17 B13 1.772(4) . ? B13 H13a 1.10(3) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag K1 O1 C17 C28 34.24(18) . . . . ? K1 O1 C18 C19 -28.1(2) . . . . ? K1 O12 C40 C39 123.7(2) . . . . ? K1 O12 C29 C30 16.22(17) . . . . ? K1 O7 C31 C32 -76.01(17) . . . . ? K1 O7 C30 C29 72.64(16) . . . . ? K1 O5 C26 C101 -34.43(18) . . . . ? K1 O5 C25 C24 21.24(17) . . . . ? K1 O4 C24 C25 61.97(18) . . . . ? K1 O4 C100 C22 63.34(18) . . . . ? K1 O3 C22 C100 34.21(16) . . . . ? K1 O3 C21 C20 -38.30(17) . . . . ? K1 O2 C20 C21 -54.52(18) . . . . ? K1 O2 C19 C18 -57.61(19) . . . . ? K1 O6 C101 C26 -58.06(17) . . . . ? K1 O6 C28 C17 59.17(17) . . . . ? K1 C24 O4 C100 -126.75(18) . . . . ? K1 C24 C25 O5 -15.12(16) . . . . ? K1 C30 O7 C31 126.40(15) . . . . ? K1 C30 C29 O12 -11.72(15) . . . . ? O1 C17 C28 O6 -63.1(3) . . . . ? O1 C18 C19 O2 57.8(3) . . . . ? O12 C40 C39 O8 -59.6(3) . . . 2_565 ? O12 C29 C30 O7 -64.9(2) . . . . ? O8 C32 C31 O7 -71.7(2) . . . . ? O5 C26 C101 O6 62.3(3) . . . . ? O5 C25 C24 O4 -57.1(3) . . . . ? O4 C100 C22 O3 -63.6(2) . . . . ? O3 C21 C20 O2 60.9(2) . . . . ? C6 C7 C8 C3 1.2(4) . . . . ? C6 C5 C4 C3 0.7(4) . . . . ? C7 C8 C3 C2 178.2(3) . . . . ? C7 C8 C3 C4 -2.4(4) . . . . ? C8 C3 C2 C1 -83.1(3) . . . . ? C8 C3 C2 B15 -13.5(3) . . . . ? C8 C3 C2 B12 -152.6(2) . . . . ? C8 C3 C2 B20 134.3(2) . . . . ? C8 C3 C2 B19 60.2(3) . . . . ? C8 C3 C4 C5 1.5(3) . . . . ? C2 C1 B1 C16 -128.79(18) . . . . ? C2 C1 B1 C9 111.17(19) . . . . ? C1 B1 C16 C11 -137.5(2) . . . . ? C1 B1 C16 C15 49.7(3) . . . . ? C1 B1 C9 C10 136.3(2) . . . . ? C1 B1 C9 B6 -93.5(2) . . . . ? C1 B1 C9 B5 -160.6(2) . . . . ? C1 B1 C9 B2 72.5(2) . . . . ? C1 B1 C9 B7 -3.4(3) . . . . ? B1 C16 C11 C12 -174.5(2) . . . . ? B1 C16 C11 C10 5.7(2) . . . . ? B1 C16 C15 C14 174.0(3) . . . . ? B1 C9 C10 C11 -6.0(2) . . . . ? B1 C9 C10 B3 -151.03(19) . . . . ? B1 C9 C10 B4 139.55(19) . . . . ? B1 C9 C10 B5 102.3(2) . . . . ? B1 C9 C10 B2 -113.3(2) . . . . ? C16 C11 C12 C13 -0.3(3) . . . . ? C16 C11 C10 C9 0.5(2) . . . . ? C16 C11 C10 B3 139.1(2) . . . . ? C16 C11 C10 B4 -138.2(2) . . . . ? C16 C11 C10 B5 -65.6(2) . . . . ? C16 C11 C10 B2 66.1(2) . . . . ? C16 C15 C14 C13 -1.1(3) . . . . ? C11 C12 C13 C14 0.5(3) . . . . ? C11 C10 C9 B6 -147.51(19) . . . . ? C11 C10 C9 B5 -108.3(3) . . . . ? C11 C10 C9 B2 107.3(2) . . . . ? C11 C10 C9 B7 146.75(19) . . . . ? C11 C10 B3 B8 -139.0(3) . . . . ? C11 C10 B3 B4 118.6(4) . . . . ? C11 C10 B3 B9 158.7(3) . . . . ? C11 C10 B3 B2 -99.5(3) . . . . ? C12 C13 C14 C15 0.1(3) . . . . ? C9 C10 B3 B8 -2.5(2) . . . . ? C9 C10 B3 B4 -104.9(3) . . . . ? C9 C10 B3 B9 -64.8(2) . . . . ? C9 C10 B3 B2 37.0(2) . . . . ?