#------------------------------------------------------------------------------ #$Date: 2026-06-26 23:56:40 +0100 (Fri, 26 Jun 2026) $ #$Revision: 306666 $ #$URL: svn://www.crystallography.net/cod/cif/1/57/74/1577453.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1577453 loop_ _publ_author_name 'Han, Guopeng' 'Collins, Christopher M.' 'Sonni, Manel' 'Daniels, Luke M.' 'Vasylenko, Andrij' 'Chen, Ruiyong' 'Robertson, Craig' 'Dyer, Matthew Stephen' 'Claridge, John B.' 'Rosseinsky, Matthew J.' _publ_section_title ; Superionic Lithium Mobility in Low Symmetry Li7Si2S7I Polymorph Accessed via Si2S7 Dimer Reorientation ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D5SC09834C _journal_year 2026 _chemical_formula_moiety 'Cl0.119 I0.881 Li7 S7 Si2' _chemical_formula_sum 'Cl0.12 I0.88 Li7 S7 Si2' _chemical_formula_weight 445.11 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_primary dual _audit_creation_date 2025-01-16 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _audit_update_record ; 2025-03-07 deposited with the CCDC. 2026-06-25 downloaded from the CCDC. ; _cell_angle_alpha 90.135(4) _cell_angle_beta 90.937(4) _cell_angle_gamma 90.498(4) _cell_formula_units_Z 2 _cell_length_a 9.0486(5) _cell_length_b 6.0273(3) _cell_length_c 11.9663(6) _cell_measurement_reflns_used 4267 _cell_measurement_temperature 241(3) _cell_measurement_theta_max 30.4160 _cell_measurement_theta_min 2.2460 _cell_volume 652.51(6) _computing_cell_refinement 'CrysAlisPro 1.171.43.107a (Rigaku OD, 2024)' _computing_data_collection 'CrysAlisPro system (CCD 43.107a 64-bit (release 07-02-2024))' _computing_data_reduction 'CrysAlisPro 1.171.43.107a (Rigaku OD, 2024)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 241(3) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_measured_fraction_theta_full 0.980 _diffrn_measured_fraction_theta_max 0.760 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -84.00 42.00 1.00 10.00 -- 5.00 -51.00 -78.00 126 2 \w -47.00 81.00 1.00 10.00 -- -8.80 72.00-120.00 128 3 \w -44.00 81.00 1.00 10.00 -- -8.80 57.00 120.00 125 4 \w -98.00 -54.00 1.00 10.00 -- -8.80 -57.00 30.00 44 5 \w -98.00 27.00 1.00 10.00 -- -8.80 -57.00-180.00 125 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB AFC12 (RCD3): Kappa single' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0730618000 _diffrn_orient_matrix_UB_12 0.0542419000 _diffrn_orient_matrix_UB_13 0.0218196000 _diffrn_orient_matrix_UB_21 0.0068865000 _diffrn_orient_matrix_UB_22 -0.0324563000 _diffrn_orient_matrix_UB_23 0.0534383000 _diffrn_orient_matrix_UB_31 0.0920018000 _diffrn_orient_matrix_UB_32 0.0463814000 _diffrn_orient_matrix_UB_33 0.0135175000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0318 _diffrn_reflns_av_unetI/netI 0.0363 _diffrn_reflns_Laue_measured_fraction_full 0.980 _diffrn_reflns_Laue_measured_fraction_max 0.760 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 10174 _diffrn_reflns_point_group_measured_fraction_full 0.980 _diffrn_reflns_point_group_measured_fraction_max 0.760 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.549 _diffrn_reflns_theta_min 1.702 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 3.446 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.96213 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.43.107a (Rigaku Oxford Diffraction, 2024) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 2.265 _exptl_crystal_description block _exptl_crystal_F_000 419 _exptl_crystal_size_max 0.06 _exptl_crystal_size_mid 0.06 _exptl_crystal_size_min 0.04 _refine_diff_density_max 0.423 _refine_diff_density_min -0.423 _refine_diff_density_rms 0.104 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.043 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 227 _refine_ls_number_reflns 3044 _refine_ls_number_restraints 64 _refine_ls_restrained_S_all 1.041 _refine_ls_R_factor_all 0.0324 _refine_ls_R_factor_gt 0.0230 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0110P)^2^+0.0404P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0391 _refine_ls_wR_factor_ref 0.0410 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2574 _reflns_number_total 3044 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d5sc09834c2.cif _cod_data_source_block lssicl_240k_manual _cod_database_code 1577453 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula Li7Si2S7ICl _chemical_oxdiff_usercomment GH228_500 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.874 _shelx_estimated_absorpt_t_min 0.820 _olex2_refinement_description ; 1. Shared sites {I1, Cl1} 2. Uiso/Uaniso restraints and constraints Uanis(I1) = Uanis(Cl1) 3. Rigid body (RIGU) restrains S6, S7, Li5, Li6, Li13, Li14 with sigma for 1-2 distances of 0.0001 and sigma for 1-3 distances of 0.0001 S1, S2, Li4, Li7, Li12 with sigma for 1-2 distances of 0.0001 and sigma for 1-3 distances of 0.0001 4. Others 1*[Sof(Li11)]+1*[Sof(Li3)]+1*[Sof(Li5)]+1*[Sof(Li1)]+1*[Sof(Li10)]+1* [Sof(Li6)]+1*[Sof(Li12)]+1*[Sof(Li13)]+1*[Sof(Li14)]+1*[Sof(Li9)]+1*[Sof(Li4)]+ 1*[Sof(Li7)]=5.5 with esd of 0.001 1*[Sof(Li14)]+1*[Sof(Li13)]+1*[Sof(Li5)]+1*[Sof(Li6)]=1 with esd of 0.001 1*[Sof(Li9)]+1*[Sof(Li11)]=1 with esd of 0.001 Sof(Cl1)=1-FVAR(1) Sof(I1)=FVAR(1) Fixed Sof: Li8(0.5) ; _shelx_res_file ; TITL lssicl_240k_manual_a.res in P-1 lssicl_240k_manual.res created by SHELXL-2018/3 at 19:53:37 on 10-Jan-2025 REM Old TITL LSSICl_240K_Manual in P-1 REM SHELXT solution in P-1: R1 0.060, Rweak 0.005, Alpha 0.016 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: Li6 Si2 S3 Cl5 I CELL 0.71073 9.0486 6.0273 11.9663 90.135 90.937 90.498 ZERR 2 0.0005 0.0003 0.0006 0.004 0.004 0.004 LATT 1 SFAC Cl I Li S Si UNIT 0.24 1.76 14 14 4 EADP I1 Cl1 RIGU 0.0001 0.0001 S6 S7 Li5 Li6 Li13 Li14 RIGU 0.0001 0.0001 S1 S2 Li4 Li7 Li12 EXYZ I1 Cl1 SUMP 5.5 0.001 1 10 1 3 1 6 1 4 1 11 1 7 1 12 1 13 1 14 1 9 1 5 1 8 SUMP 1 0.001 1 14 1 13 1 6 1 7 SUMP 1 0.001 1 9 1 10 L.S. 20 PLAN 20 SIZE 0.04 0.06 0.06 TEMP -32 CONF CONN 4 Si2 CONN 4 Si1 list 4 MORE -1 fmap 2 53 acta REM REM REM WGHT 0.011000 0.040400 FVAR 0.40618 0.88143 0.94861 0.97042 0.42544 0.24035 0.33075 FVAR 0.52647 0.55173 0.44826 0.54631 0.08263 0.25357 0.17539 PART 1 I1 2 0.989256 0.751606 0.886240 21.00000 0.01796 0.02128 = 0.01918 0.00068 -0.00256 0.00187 PART 2 CL1 1 0.989256 0.751606 0.886240 -21.00000 0.01796 0.02128 = 0.01918 0.00068 -0.00256 0.00187 PART 3 S1 4 0.765597 0.234815 0.407493 11.00000 0.01703 0.02395 = 0.01316 -0.00413 0.00114 -0.00076 S2 4 0.943659 0.223951 0.668453 11.00000 0.01372 0.01727 = 0.01645 -0.00099 -0.00173 0.00280 S3 4 0.771071 0.706606 0.568714 11.00000 0.02051 0.01192 = 0.01829 0.00127 0.00258 0.00138 S4 4 0.560360 0.232575 0.635953 11.00000 0.01326 0.01623 = 0.01352 -0.00224 0.00210 -0.00250 S5 4 0.680529 0.214458 0.915277 11.00000 0.01626 0.01817 = 0.01878 0.00265 -0.00251 0.00139 S6 4 0.305384 0.246833 0.835471 11.00000 0.01378 0.02235 = 0.01642 0.00003 0.00240 -0.00194 S7 4 0.536561 0.702573 0.812082 11.00000 0.02098 0.01295 = 0.01982 -0.00108 0.00249 0.00055 PART 0 SI1 5 0.770259 0.358997 0.571466 11.00000 0.01303 0.01216 = 0.01187 0.00032 0.00150 -0.00037 SI2 5 0.522960 0.355150 0.805991 11.00000 0.01303 0.01289 = 0.01235 -0.00007 0.00161 -0.00005 LI1 3 0.758470 0.929244 0.749811 41.00000 0.03360 0.03358 = 0.02923 -0.00244 0.00255 -0.00970 LI2 3 0.506275 0.773843 0.610959 11.00000 0.01962 0.06426 = 0.03310 -0.00356 -0.00164 0.00042 LI3 3 0.940653 0.293354 0.871935 31.00000 0.03367 0.04899 = 0.02345 -0.00853 0.00020 -0.01351 LI4 3 1.001915 0.077668 0.462645 51.00000 0.02379 0.02827 = 0.02136 -0.00435 0.00141 -0.00026 LI5 3 0.293448 0.833573 0.857326 61.00000 0.03929 0.02763 = 0.02699 -0.00141 -0.00047 -0.00085 LI6 3 0.290863 0.643584 0.899580 71.00000 0.03197 0.02751 = 0.02671 -0.00159 0.00094 -0.00006 LI7 3 0.989392 0.365972 0.335438 81.00000 0.02381 0.03410 = 0.02779 0.00178 0.00169 0.00044 LI8 3 0.571666 -0.115665 0.990644 10.50000 0.06006 0.04086 = 0.02867 0.00557 -0.00340 -0.02558 LI9 3 1.195842 0.349087 0.640025 91.00000 0.03521 0.05527 = 0.02702 0.01017 -0.00862 -0.02088 LI10 3 0.291204 0.367160 1.026715 111.00000 0.03917 0.07369 = 0.03484 -0.00743 0.00811 -0.00449 LI11 3 0.757676 0.803370 0.368286 101.00000 0.03092 0.03192 = 0.01446 -0.00230 -0.00225 0.00061 LI12 3 1.000000 0.000000 0.500000 121.00000 0.02513 0.02198 = 0.01463 -0.01086 0.00313 0.00132 LI13 3 0.281461 0.833566 0.811957 131.00000 0.03250 0.02757 = 0.02676 -0.00153 0.00078 -0.00018 LI14 3 0.290346 0.698985 0.873463 141.00000 0.03189 0.02760 = 0.02682 -0.00148 0.00061 -0.00037 HKLF 4 1 0 1 0 1 0 0 0 0 1 REM lssicl_240k_manual_a.res in P-1 REM wR2 = 0.0410, GooF = S = 1.043, Restrained GooF = 1.041 for all data REM R1 = 0.0230 for 2574 Fo > 4sig(Fo) and 0.0324 for all 3044 data REM 227 parameters refined using 64 restraints END WGHT 0.0110 0.0404 REM Highest difference peak 0.423, deepest hole -0.423, 1-sigma level 0.104 Q1 1 0.5891 0.7308 0.8767 11.00000 0.05 0.42 Q2 1 0.5415 0.4984 0.6247 11.00000 0.05 0.42 Q3 1 0.7588 0.1540 0.5815 11.00000 0.05 0.41 Q4 1 0.4420 0.7574 0.7387 11.00000 0.05 0.40 Q5 1 0.3243 0.1012 0.8470 11.00000 0.05 0.39 Q6 1 1.0273 0.9200 0.8995 11.00000 0.05 0.39 Q7 1 0.2574 0.2198 0.8787 11.00000 0.05 0.38 Q8 1 0.8520 0.8662 0.8976 11.00000 0.05 0.38 Q9 1 1.0471 0.7439 0.9608 11.00000 0.05 0.38 Q10 1 0.5082 0.5171 0.7910 11.00000 0.05 0.37 Q11 1 1.0217 0.6444 0.8747 11.00000 0.05 0.37 Q12 1 0.4802 0.6381 0.5916 11.00000 0.05 0.37 Q13 1 0.3100 0.4982 0.8559 11.00000 0.05 0.36 Q14 1 0.6785 0.9141 0.5739 11.00000 0.05 0.36 Q15 1 0.6363 0.4578 0.6022 11.00000 0.05 0.36 Q16 1 0.7969 0.2549 0.4783 11.00000 0.05 0.36 Q17 1 0.8455 0.5257 0.6567 11.00000 0.05 0.35 Q18 1 0.1609 0.7641 0.9797 11.00000 0.05 0.35 Q19 1 1.1204 0.8005 0.8970 11.00000 0.05 0.35 Q20 1 0.5959 0.2074 0.9052 11.00000 0.05 0.35 ; _shelx_res_checksum 52739 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.038 _oxdiff_exptl_absorpt_empirical_full_min 0.953 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group I1 I 0.98926(2) 0.75161(3) 0.88624(2) 0.01949(7) Uani 0.8814(15) 1 d . . P A 1 Cl1 Cl 0.98926(2) 0.75161(3) 0.88624(2) 0.01949(7) Uani 0.1186(15) 1 d . . P A 2 S1 S 0.76560(7) 0.23482(10) 0.40749(5) 0.01805(14) Uani 1 1 d . . . B 3 S2 S 0.94366(7) 0.22395(9) 0.66845(5) 0.01582(14) Uani 1 1 d . . . B 3 S3 S 0.77107(7) 0.70661(9) 0.56871(5) 0.01687(14) Uani 1 1 d . . . A 3 S4 S 0.56036(6) 0.23257(9) 0.63595(5) 0.01434(14) Uani 1 1 d . . . C 3 S5 S 0.68053(7) 0.21446(10) 0.91528(5) 0.01775(14) Uani 1 1 d . . . D 3 S6 S 0.30538(7) 0.24683(10) 0.83547(5) 0.01750(14) Uani 1 1 d . . . A 3 S7 S 0.53656(7) 0.70257(9) 0.81208(5) 0.01789(14) Uani 1 1 d . . . A 3 Si1 Si 0.77026(7) 0.35900(10) 0.57147(5) 0.01234(15) Uani 1 1 d . . . . . Si2 Si 0.52296(7) 0.35515(10) 0.80599(5) 0.01275(15) Uani 1 1 d . . . . . Li1 Li 0.7585(6) 0.9292(8) 0.7498(4) 0.0322(16) Uani 0.970(15) 1 d . . P A . Li2 Li 0.5063(5) 0.7738(9) 0.6110(4) 0.0390(12) Uani 1 1 d . . . . . Li3 Li 0.9407(6) 0.2934(9) 0.8719(4) 0.0355(18) Uani 0.949(15) 1 d . . P . . Li4 Li 1.0019(11) 0.0777(19) 0.4626(10) 0.0245(15) Uani 0.425(12) 1 d . . P . . Li5 Li 0.293(3) 0.834(4) 0.857(3) 0.0313(14) Uani 0.240(16) 1 d . . P . . Li6 Li 0.2909(19) 0.644(3) 0.8996(16) 0.0287(10) Uani 0.331(19) 1 d . . P A . Li7 Li 0.9894(10) 0.3660(14) 0.3354(7) 0.029(2) Uani 0.526(12) 1 d . . P B . Li8 Li 0.5717(13) -0.1157(17) 0.9906(9) 0.043(3) Uani 0.5 1 d . . P . . Li9 Li 1.1958(12) 0.349(2) 0.6400(8) 0.039(4) Uani 0.552(15) 1 d . . P B . Li10 Li 0.2912(11) 0.3672(19) 1.0267(9) 0.049(4) Uani 0.546(15) 1 d . . P A . Li11 Li 0.7577(12) 0.803(2) 0.3683(8) 0.026(3) Uani 0.448(15) 1 d . . P . . Li12 Li 1.000000 0.000000 0.500000 0.0206(16) Uani 0.17(2) 2 d S . P B . Li13 Li 0.281(2) 0.834(3) 0.812(2) 0.0289(11) Uani 0.254(16) 1 d . . P A . Li14 Li 0.290(4) 0.699(7) 0.873(3) 0.0288(13) Uani 0.175(18) 1 d . . P A . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.01796(11) 0.02128(10) 0.01918(10) 0.00068(7) -0.00256(7) 0.00187(7) Cl1 0.01796(11) 0.02128(10) 0.01918(10) 0.00068(7) -0.00256(7) 0.00187(7) S1 0.0170(3) 0.0239(3) 0.0132(3) -0.0041(2) 0.0011(2) -0.0008(2) S2 0.0137(3) 0.0173(3) 0.0164(3) -0.0010(2) -0.0017(2) 0.0028(2) S3 0.0205(3) 0.0119(3) 0.0183(3) 0.0013(2) 0.0026(3) 0.0014(2) S4 0.0133(3) 0.0162(3) 0.0135(3) -0.0022(2) 0.0021(2) -0.0025(2) S5 0.0163(3) 0.0182(3) 0.0188(3) 0.0027(2) -0.0025(3) 0.0014(2) S6 0.0138(3) 0.0223(3) 0.0164(3) 0.0000(2) 0.0024(2) -0.0019(2) S7 0.0210(3) 0.0130(3) 0.0198(3) -0.0011(2) 0.0025(3) 0.0005(2) Si1 0.0130(3) 0.0122(3) 0.0119(3) 0.0003(2) 0.0015(3) -0.0004(2) Si2 0.0130(3) 0.0129(3) 0.0124(3) -0.0001(2) 0.0016(3) 0.0000(2) Li1 0.034(3) 0.034(3) 0.029(3) -0.002(2) 0.003(2) -0.010(2) Li2 0.020(3) 0.064(3) 0.033(3) -0.004(2) -0.002(2) 0.000(2) Li3 0.034(3) 0.049(3) 0.023(3) -0.009(2) 0.000(2) -0.014(2) Li4 0.024(3) 0.0283(17) 0.0214(17) -0.0044(15) 0.0014(13) -0.0003(14) Li5 0.039(4) 0.0276(8) 0.0270(9) -0.0014(6) -0.0005(8) -0.0009(7) Li6 0.032(3) 0.0275(8) 0.0267(8) -0.0016(7) 0.0009(8) -0.0001(6) Li7 0.024(3) 0.034(3) 0.028(3) 0.002(2) 0.0017(18) 0.0004(17) Li8 0.060(7) 0.041(6) 0.029(5) 0.006(4) -0.003(5) -0.026(5) Li9 0.035(6) 0.055(9) 0.027(5) 0.010(5) -0.009(4) -0.021(6) Li10 0.039(6) 0.074(8) 0.035(6) -0.007(5) 0.008(5) -0.004(5) Li11 0.031(6) 0.032(8) 0.014(5) -0.002(4) -0.002(4) 0.001(5) Li12 0.025(3) 0.0220(17) 0.015(2) -0.0109(17) 0.0031(15) 0.0013(15) Li13 0.032(3) 0.0276(8) 0.0268(9) -0.0015(6) 0.0008(8) -0.0002(9) Li14 0.032(4) 0.0276(8) 0.0268(8) -0.0015(6) 0.0006(7) -0.0004(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Li1 I1 Li3 137.66(15) . 2_767 ? Li1 I1 Li3 59.65(13) . 1_565 ? Li3 I1 Li1 103.31(15) . . ? Li3 I1 Li3 89.79(14) . 2_767 ? Li3 I1 Li3 162.2(2) . 1_565 ? Li3 I1 Li3 99.86(13) 2_767 1_565 ? Li3 I1 Li5 108.1(5) . 1_655 ? Li3 I1 Li6 85.3(4) . 1_655 ? Li3 I1 Li10 69.0(3) . 2_667 ? Li3 I1 Li13 106.9(4) . 1_655 ? Li5 I1 Li1 125.0(6) 1_655 . ? Li5 I1 Li3 87.6(5) 1_655 1_565 ? Li5 I1 Li3 86.7(6) 1_655 2_767 ? Li5 I1 Li10 164.6(7) 1_655 2_667 ? Li5 I1 Li13 11.2(5) 1_655 1_655 ? Li6 I1 Li1 145.7(4) 1_655 . ? Li6 I1 Li3 111.6(4) 1_655 1_565 ? Li6 I1 Li3 74.3(4) 1_655 2_767 ? Li6 I1 Li5 25.7(7) 1_655 1_655 ? Li6 I1 Li10 142.2(5) 1_655 2_667 ? Li6 I1 Li13 31.9(6) 1_655 1_655 ? Li7 I1 Li1 66.9(2) 2_766 . ? Li7 I1 Li3 72.7(2) 2_766 . ? Li7 I1 Li3 102.39(19) 2_766 1_565 ? Li7 I1 Li3 153.9(2) 2_766 2_767 ? Li7 I1 Li5 80.8(6) 2_766 1_655 ? Li7 I1 Li6 84.8(4) 2_766 1_655 ? Li7 I1 Li10 111.5(3) 2_766 2_667 ? Li7 I1 Li13 70.2(6) 2_766 1_655 ? Li10 I1 Li1 69.7(2) 2_667 . ? Li10 I1 Li3 78.3(2) 2_667 2_767 ? Li10 I1 Li3 98.2(2) 2_667 1_565 ? Li13 I1 Li1 115.7(5) 1_655 . ? Li13 I1 Li3 86.7(4) 1_655 1_565 ? Li13 I1 Li3 97.8(6) 1_655 2_767 ? Li13 I1 Li10 174.2(5) 1_655 2_667 ? Li14 I1 Li1 137.1(9) 1_655 . ? Li14 I1 Li3 91.7(9) 1_655 . ? Li14 I1 Li3 104.5(9) 1_655 1_565 ? Li14 I1 Li3 81.2(8) 1_655 2_767 ? Li14 I1 Li5 17.2(8) 1_655 1_655 ? Li14 I1 Li6 9.4(8) 1_655 1_655 ? Li14 I1 Li7 80.2(7) 1_655 2_766 ? Li14 I1 Li10 151.6(10) 1_655 2_667 ? Li14 I1 Li13 22.6(11) 1_655 1_655 ? Li1 Cl1 Li3 137.66(15) . 2_767 ? Li3 Cl1 Li1 103.31(15) . . ? Li3 Cl1 Li3 89.79(14) . 2_767 ? Li3 Cl1 Li5 108.1(5) . 1_655 ? Li3 Cl1 Li6 85.3(4) . 1_655 ? Li3 Cl1 Li10 69.0(3) . 2_667 ? Li3 Cl1 Li13 106.9(4) . 1_655 ? Li5 Cl1 Li1 125.0(6) 1_655 . ? Li5 Cl1 Li3 86.7(6) 1_655 2_767 ? Li5 Cl1 Li10 164.6(7) 1_655 2_667 ? Li5 Cl1 Li13 11.2(5) 1_655 1_655 ? Li6 Cl1 Li1 145.7(4) 1_655 . ? Li6 Cl1 Li3 74.3(4) 1_655 2_767 ? Li6 Cl1 Li5 25.7(7) 1_655 1_655 ? Li6 Cl1 Li10 142.2(5) 1_655 2_667 ? Li6 Cl1 Li13 31.9(6) 1_655 1_655 ? Li7 Cl1 Li1 66.9(2) 2_766 . ? Li7 Cl1 Li3 153.9(2) 2_766 2_767 ? Li7 Cl1 Li3 72.7(2) 2_766 . ? Li7 Cl1 Li5 80.8(6) 2_766 1_655 ? Li7 Cl1 Li6 84.8(4) 2_766 1_655 ? Li7 Cl1 Li10 111.5(3) 2_766 2_667 ? Li7 Cl1 Li13 70.2(6) 2_766 1_655 ? Li10 Cl1 Li1 69.7(2) 2_667 . ? Li10 Cl1 Li3 78.3(2) 2_667 2_767 ? Li13 Cl1 Li1 115.7(5) 1_655 . ? Li13 Cl1 Li3 97.8(6) 1_655 2_767 ? Li13 Cl1 Li10 174.2(5) 1_655 2_667 ? Li14 Cl1 Li1 137.1(9) 1_655 . ? Li14 Cl1 Li3 91.7(9) 1_655 . ? Li14 Cl1 Li3 81.2(8) 1_655 2_767 ? Li14 Cl1 Li5 17.2(8) 1_655 1_655 ? Li14 Cl1 Li6 9.4(8) 1_655 1_655 ? Li14 Cl1 Li7 80.2(7) 1_655 2_766 ? Li14 Cl1 Li10 151.6(10) 1_655 2_667 ? Li14 Cl1 Li13 22.6(11) 1_655 1_655 ? Si1 S1 Li2 95.33(12) . 2_666 ? Si1 S1 Li4 83.3(2) . . ? Si1 S1 Li7 102.9(2) . . ? Si1 S1 Li9 82.1(2) . 2_766 ? Si1 S1 Li11 121.0(2) . 1_545 ? Si1 S1 Li12 78.87(3) . . ? Si1 S1 Li13 165.6(4) . 2_666 ? Li2 S1 Li9 97.5(3) 2_666 2_766 ? Li2 S1 Li11 87.0(3) 2_666 1_545 ? Li2 S1 Li12 141.59(12) 2_666 . ? Li2 S1 Li13 76.6(5) 2_666 2_666 ? Li4 S1 Li2 153.1(3) . 2_666 ? Li4 S1 Li9 108.9(4) . 2_766 ? Li4 S1 Li11 71.2(4) . 1_545 ? Li4 S1 Li12 12.1(3) . . ? Li4 S1 Li13 109.3(5) . 2_666 ? Li7 S1 Li2 146.8(2) . 2_666 ? Li7 S1 Li4 58.0(4) . . ? Li7 S1 Li9 58.7(3) . 2_766 ? Li7 S1 Li11 106.3(3) . 1_545 ? Li7 S1 Li12 70.1(2) . . ? Li7 S1 Li13 79.3(5) . 2_666 ? Li9 S1 Li11 156.2(3) 2_766 1_545 ? Li9 S1 Li12 118.8(2) 2_766 . ? Li9 S1 Li13 87.1(5) 2_766 2_666 ? Li11 S1 Li12 65.2(2) 1_545 . ? Li11 S1 Li13 71.1(5) 1_545 2_666 ? Li13 S1 Li12 114.9(4) 2_666 . ? Si1 S2 Li1 89.71(12) . 1_545 ? Si1 S2 Li3 117.20(13) . . ? Si1 S2 Li4 95.5(3) . 2_756 ? Si1 S2 Li4 77.2(2) . . ? Si1 S2 Li7 77.5(2) . 2_766 ? Si1 S2 Li9 119.8(3) . . ? Si1 S2 Li11 131.6(2) . 2_766 ? Si1 S2 Li12 85.87(3) . . ? Li1 S2 Li4 104.8(3) 1_545 . ? Li1 S2 Li11 130.3(3) 1_545 2_766 ? Li3 S2 Li1 74.33(16) . 1_545 ? Li3 S2 Li4 165.4(3) . . ? Li3 S2 Li7 82.1(2) . 2_766 ? Li3 S2 Li11 101.3(2) . 2_766 ? Li3 S2 Li12 153.62(13) . . ? Li4 S2 Li1 82.8(3) 2_756 1_545 ? Li4 S2 Li3 139.3(3) 2_756 . ? Li4 S2 Li4 28.9(6) 2_756 . ? Li4 S2 Li7 131.0(4) 2_756 2_766 ? Li4 S2 Li11 67.8(3) . 2_766 ? Li4 S2 Li11 68.9(3) 2_756 2_766 ? Li4 S2 Li12 15.1(3) 2_756 . ? Li7 S2 Li1 144.2(2) 2_766 1_545 ? Li7 S2 Li4 104.6(3) 2_766 . ? Li7 S2 Li11 80.1(3) 2_766 2_766 ? Li9 S2 Li1 149.4(3) . 1_545 ? Li9 S2 Li3 96.5(3) . . ? Li9 S2 Li4 76.8(3) . . ? Li9 S2 Li4 86.3(4) . 2_756 ? Li9 S2 Li7 58.5(4) . 2_766 ? Li9 S2 Li11 21.5(3) . 2_766 ? Li9 S2 Li12 81.1(3) . . ? Li12 S2 Li1 94.38(11) . 1_545 ? Li12 S2 Li4 13.8(3) . . ? Li12 S2 Li7 117.4(2) . 2_766 ? Li12 S2 Li11 67.6(2) . 2_766 ? Si1 S3 Li1 120.72(11) . . ? Si1 S3 Li2 99.41(13) . . ? Si1 S3 Li4 121.9(3) . 2_766 ? Si1 S3 Li7 79.1(2) . 2_766 ? Si1 S3 Li9 83.4(3) . 2_766 ? Si1 S3 Li11 104.7(3) . . ? Si1 S3 Li12 128.55(3) . 1_565 ? Li1 S3 Li12 88.02(11) . 1_565 ? Li2 S3 Li1 71.45(17) . . ? Li2 S3 Li9 110.5(3) . 2_766 ? Li2 S3 Li12 131.32(13) . 1_565 ? Li4 S3 Li1 84.5(3) 2_766 . ? Li4 S3 Li2 138.7(3) 2_766 . ? Li4 S3 Li7 56.0(4) 2_766 2_766 ? Li4 S3 Li9 78.8(3) 2_766 2_766 ? Li4 S3 Li11 75.8(4) 2_766 . ? Li4 S3 Li12 11.3(3) 2_766 1_565 ? Li7 S3 Li1 75.8(2) 2_766 . ? Li7 S3 Li2 140.7(2) 2_766 . ? Li7 S3 Li9 108.3(3) 2_766 2_766 ? Li7 S3 Li12 67.20(19) 2_766 1_565 ? Li9 S3 Li1 155.6(3) 2_766 . ? Li9 S3 Li12 72.5(2) 2_766 1_565 ? Li11 S3 Li1 134.2(3) . . ? Li11 S3 Li2 97.1(3) . . ? Li11 S3 Li7 121.5(3) . 2_766 ? Li11 S3 Li9 23.4(3) . 2_766 ? Li11 S3 Li12 66.2(3) . 1_565 ? Si1 S4 Si2 111.05(3) . . ? Si1 S4 Li1 81.38(10) . 1_545 ? Si1 S4 Li2 79.52(10) . 2_666 ? Si1 S4 Li2 116.51(10) . 1_545 ? Si1 S4 Li11 152.4(2) . 2_666 ? Si2 S4 Li1 83.21(10) . 1_545 ? Si2 S4 Li2 113.45(11) . 1_545 ? Si2 S4 Li2 151.94(10) . 2_666 ? Si2 S4 Li11 82.5(2) . 2_666 ? Li1 S4 Li2 124.68(14) 1_545 2_666 ? Li2 S4 Li1 62.01(14) 1_545 1_545 ? Li2 S4 Li2 81.68(16) 1_545 2_666 ? Li2 S4 Li11 76.2(3) 1_545 2_666 ? Li11 S4 Li1 125.1(3) 2_666 1_545 ? Li11 S4 Li2 78.4(2) 2_666 2_666 ? Si2 S5 Li1 89.33(11) . 1_545 ? Si2 S5 Li3 115.69(13) . . ? Si2 S5 Li5 135.0(5) . 2_667 ? Si2 S5 Li6 119.6(4) . 2_667 ? Si2 S5 Li8 76.8(2) . 2_657 ? Si2 S5 Li8 107.2(3) . . ? Si2 S5 Li10 80.4(2) . 2_667 ? Si2 S5 Li14 125.6(8) . 2_667 ? Li1 S5 Li5 129.3(5) 1_545 2_667 ? Li3 S5 Li1 72.79(16) . 1_545 ? Li3 S5 Li5 99.3(5) . 2_667 ? Li3 S5 Li8 166.4(3) . 2_657 ? Li3 S5 Li10 77.8(3) . 2_667 ? Li3 S5 Li14 95.0(8) . 2_667 ? Li6 S5 Li1 151.1(5) 2_667 1_545 ? Li6 S5 Li3 92.3(4) 2_667 . ? Li6 S5 Li5 27.1(7) 2_667 2_667 ? Li6 S5 Li8 76.2(5) 2_667 2_657 ? Li6 S5 Li8 89.1(5) 2_667 . ? Li6 S5 Li10 53.4(5) 2_667 2_667 ? Li6 S5 Li14 9.4(10) 2_667 2_667 ? Li8 S5 Li1 114.2(3) 2_657 1_545 ? Li8 S5 Li1 82.2(3) . 1_545 ? Li8 S5 Li3 129.3(3) . . ? Li8 S5 Li5 64.3(6) . 2_667 ? Li8 S5 Li5 67.2(6) 2_657 2_667 ? Li8 S5 Li8 44.9(5) . 2_657 ? Li8 S5 Li10 137.2(3) . 2_667 ? Li8 S5 Li14 80.4(10) . 2_667 ? Li10 S5 Li1 140.6(2) 2_667 1_545 ? Li10 S5 Li5 80.5(6) 2_667 2_667 ? Li10 S5 Li8 100.3(3) 2_667 2_657 ? Li14 S5 Li1 144.2(9) 2_667 1_545 ? Li14 S5 Li5 17.7(9) 2_667 2_667 ? Li14 S5 Li8 72.6(8) 2_667 2_657 ? Li14 S5 Li10 62.8(11) 2_667 2_667 ? Si2 S6 Li5 111.1(5) . 1_545 ? Si2 S6 Li6 79.5(4) . . ? Si2 S6 Li8 80.3(2) . 2_657 ? Si2 S6 Li9 96.9(2) . 1_455 ? Si2 S6 Li10 97.7(2) . . ? Si2 S6 Li11 94.1(2) . 2_666 ? Si2 S6 Li13 111.1(5) . 1_545 ? Si2 S6 Li14 77.2(7) . . ? Li5 S6 Li6 155.5(8) 1_545 . ? Li5 S6 Li9 108.5(7) 1_545 1_455 ? Li5 S6 Li11 88.6(8) 1_545 2_666 ? Li5 S6 Li13 12.6(6) 1_545 1_545 ? Li5 S6 Li14 163.6(10) 1_545 . ? Li6 S6 Li9 91.3(5) . 1_455 ? Li6 S6 Li14 8.3(7) . . ? Li8 S6 Li5 67.0(7) 2_657 1_545 ? Li8 S6 Li6 94.5(5) 2_657 . ? Li8 S6 Li9 173.0(4) 2_657 1_455 ? Li8 S6 Li11 150.3(4) 2_657 2_666 ? Li8 S6 Li13 79.0(7) 2_657 1_545 ? Li8 S6 Li14 101.8(8) 2_657 . ? Li9 S6 Li14 83.7(8) 1_455 . ? Li10 S6 Li5 101.3(7) . 1_545 ? Li10 S6 Li6 54.6(5) . . ? Li10 S6 Li8 47.8(4) . 2_657 ? Li10 S6 Li9 139.2(4) . 1_455 ? Li10 S6 Li11 160.7(4) . 2_666 ? Li10 S6 Li13 113.4(7) . 1_545 ? Li10 S6 Li14 62.9(8) . . ? Li11 S6 Li6 113.2(6) 2_666 . ? Li11 S6 Li9 22.9(3) 2_666 1_455 ? Li11 S6 Li13 76.0(7) 2_666 1_545 ? Li11 S6 Li14 105.2(8) 2_666 . ? Li13 S6 Li6 166.1(7) 1_545 . ? Li13 S6 Li9 96.2(7) 1_545 1_455 ? Li13 S6 Li14 171.6(9) 1_545 . ? Si2 S7 Li1 124.48(12) . . ? Si2 S7 Li2 97.94(13) . . ? Si2 S7 Li5 106.8(6) . . ? Si2 S7 Li6 80.0(4) . . ? Si2 S7 Li8 119.2(2) . 1_565 ? Si2 S7 Li10 83.5(3) . 2_667 ? Si2 S7 Li13 106.0(5) . . ? Si2 S7 Li14 87.4(11) . . ? Li2 S7 Li1 72.19(16) . . ? Li2 S7 Li6 110.4(5) . . ? Li2 S7 Li10 147.7(3) . 2_667 ? Li5 S7 Li1 128.0(6) . . ? Li5 S7 Li2 94.2(7) . . ? Li5 S7 Li6 29.5(8) . . ? Li5 S7 Li8 76.0(8) . 1_565 ? Li5 S7 Li10 116.4(8) . 2_667 ? Li5 S7 Li13 13.0(6) . . ? Li6 S7 Li1 155.3(4) . . ? Li6 S7 Li10 101.6(5) . 2_667 ? Li8 S7 Li1 85.8(3) 1_565 . ? Li8 S7 Li2 142.9(3) 1_565 . ? Li8 S7 Li6 78.2(5) 1_565 . ? Li8 S7 Li10 47.5(4) 1_565 2_667 ? Li8 S7 Li13 87.8(7) 1_565 . ? Li10 S7 Li1 80.4(3) 2_667 . ? Li13 S7 Li1 125.0(5) . . ? Li13 S7 Li2 81.4(6) . . ? Li13 S7 Li6 36.7(7) . . ? Li13 S7 Li10 129.4(7) . 2_667 ? Li14 S7 Li1 147.9(11) . . ? Li14 S7 Li2 102.4(9) . . ? Li14 S7 Li5 20.1(10) . . ? Li14 S7 Li6 10.3(10) . . ? Li14 S7 Li8 80.6(9) . 1_565 ? Li14 S7 Li10 109.9(10) . 2_667 ? Li14 S7 Li13 26.4(12) . . ? S1 Si1 S2 112.27(4) . . ? S1 Si1 S4 101.77(3) . . ? S2 Si1 S4 108.26(3) . . ? S3 Si1 S1 109.86(4) . . ? S3 Si1 S2 113.58(4) . . ? S3 Si1 S4 110.46(4) . . ? S5 Si2 S4 108.97(4) . . ? S5 Si2 S6 113.45(3) . . ? S6 Si2 S4 102.28(4) . . ? S7 Si2 S4 110.93(3) . . ? S7 Si2 S5 110.43(4) . . ? S7 Si2 S6 110.52(4) . . ? I1 Li1 S4 162.96(18) . 1_565 ? I1 Li1 Li2 139.3(2) . . ? I1 Li1 Li3 67.54(15) . 1_565 ? I1 Li1 Li4 87.2(2) . 2_766 ? I1 Li1 Li7 55.09(19) . 2_766 ? I1 Li1 Li10 55.1(2) . 2_667 ? Cl1 Li1 Li2 139.3(2) . . ? S2 Li1 Li2 119.4(2) 1_565 . ? S3 Li1 Li2 53.36(14) . . ? S4 Li1 Li2 57.65(14) 1_565 . ? S5 Li1 Li2 113.5(2) 1_565 . ? S7 Li1 S3 90.97(15) . . ? S7 Li1 Li2 52.58(14) . . ? Li2 Li1 Li3 152.8(2) . 1_565 ? Li2 Li1 Li4 94.1(2) . 2_766 ? Li2 Li1 Li7 101.7(2) . 2_766 ? Li2 Li1 Li10 100.2(3) . 2_667 ? Li3 Li1 Li4 91.3(2) 1_565 2_766 ? Li3 Li1 Li7 100.1(2) 1_565 2_766 ? Li3 Li1 Li10 94.5(2) 1_565 2_667 ? Li7 Li1 Li4 41.7(3) 2_766 2_766 ? Li7 Li1 Li10 93.7(3) 2_766 2_667 ? Li10 Li1 Li4 135.3(3) 2_667 2_766 ? S1 Li2 S3 160.1(2) 2_666 . ? S1 Li2 Li1 144.7(2) 2_666 . ? S1 Li2 Li13 54.7(5) 2_666 . ? S3 Li2 Li1 55.18(14) . . ? S3 Li2 Li13 142.9(5) . . ? S4 Li2 Li1 60.33(14) 1_565 . ? S4 Li2 Li13 128.4(5) 2_666 . ? S4 Li2 Li13 85.3(4) 1_565 . ? S7 Li2 S3 94.36(17) . . ? S7 Li2 Li1 55.23(14) . . ? S7 Li2 Li13 49.2(5) . . ? Li1 Li2 S4 134.3(2) . 2_666 ? Li1 Li2 Li11 104.7(3) . 2_676 ? Li1 Li2 Li13 92.1(5) . . ? Li13 Li2 Li11 54.6(4) . 2_676 ? I1 Li3 I1 80.14(13) 2_767 1_545 ? I1 Li3 I1 162.2(2) . 1_545 ? I1 Li3 I1 90.21(14) . 2_767 ? I1 Li3 Li1 143.8(2) . 1_545 ? I1 Li3 Li1 119.93(19) 2_767 1_545 ? I1 Li3 Li6 86.4(3) . 2_667 ? I1 Li3 Li6 50.8(3) 2_767 2_667 ? I1 Li3 Li6 98.7(3) 1_545 2_667 ? I1 Li3 Li7 53.05(18) . 2_766 ? I1 Li3 Li7 139.0(2) 2_767 2_766 ? I1 Li3 Li10 56.2(2) . 2_667 ? I1 Li3 Li10 79.8(2) 2_767 2_667 ? S5 Li3 S2 101.70(18) . . ? Li1 Li3 I1 52.81(12) 1_545 1_545 ? Li1 Li3 Li6 97.3(3) 1_545 2_667 ? Li1 Li3 Li7 101.0(2) 1_545 2_766 ? Li1 Li3 Li10 106.6(3) 1_545 2_667 ? Li7 Li3 I1 129.0(2) 2_766 1_545 ? Li7 Li3 Li6 130.2(4) 2_766 2_667 ? Li10 Li3 I1 135.0(3) 2_667 1_545 ? Li10 Li3 Li6 39.2(4) 2_667 2_667 ? Li10 Li3 Li7 91.1(3) 2_667 2_766 ? S1 Li4 S2 86.2(3) . . ? S1 Li4 Si1 43.67(17) . . ? S1 Li4 Li9 117.0(5) . . ? S2 Li4 S2 151.1(6) 2_756 . ? S2 Li4 Si1 147.5(4) 2_756 . ? S2 Li4 Si1 42.91(15) . . ? S2 Li4 Li9 48.1(3) . . ? S2 Li4 Li9 133.6(5) 2_756 . ? S3 Li4 S2 98.4(3) 2_766 . ? S3 Li4 Si1 111.0(4) 2_766 . ? S3 Li4 Li9 51.8(3) 2_766 . ? Si1 Li4 Li9 78.6(3) . . ? Si1 Li4 Li9 102.7(4) . 2_756 ? Si1 Li4 Li11 94.5(4) . 2_766 ? Li4 Li4 S1 116.2(10) 2_756 . ? Li4 Li4 S2 66.1(8) 2_756 . ? Li4 Li4 S2 85.0(9) 2_756 2_756 ? Li4 Li4 S3 121.0(11) 2_756 2_766 ? Li4 Li4 Si1 94.9(9) 2_756 . ? Li4 Li4 Li7 175.0(12) 2_756 . ? Li4 Li4 Li9 71.4(9) 2_756 2_756 ? Li4 Li4 Li9 85.9(9) 2_756 . ? Li4 Li4 Li11 80.6(9) 2_756 1_545 ? Li4 Li4 Li11 74.4(9) 2_756 2_766 ? Li7 Li4 S1 59.2(4) . . ? Li7 Li4 S2 110.4(5) . . ? Li7 Li4 S2 98.4(5) . 2_756 ? Li7 Li4 S3 62.5(4) . 2_766 ? Li7 Li4 Si1 80.2(4) . . ? Li7 Li4 Li9 94.4(5) . . ? Li7 Li4 Li9 108.3(5) . 2_756 ? Li7 Li4 Li11 107.1(5) . 2_766 ? Li7 Li4 Li11 97.8(5) . 1_545 ? Li9 Li4 Li9 157.2(5) . 2_756 ? Li11 Li4 Si1 87.6(4) 1_545 . ? Li11 Li4 Li9 18.7(2) 2_766 . ? Li11 Li4 Li9 17.3(3) 1_545 2_756 ? Li11 Li4 Li9 142.7(5) 2_766 2_756 ? Li11 Li4 Li9 159.7(5) 1_545 . ? Li11 Li4 Li11 155.0(5) 1_545 2_766 ? Li12 Li4 S1 116.2(10) . . ? Li12 Li4 S2 66.1(8) . . ? Li12 Li4 S2 85.0(9) . 2_756 ? Li12 Li4 S3 121.0(11) . 2_766 ? Li12 Li4 Si1 94.9(9) . . ? Li12 Li4 Li4 0.001(3) . 2_756 ? Li12 Li4 Li7 175.0(12) . . ? Li12 Li4 Li9 85.9(9) . . ? Li12 Li4 Li9 71.4(9) . 2_756 ? Li12 Li4 Li11 74.4(9) . 2_766 ? Li12 Li4 Li11 80.6(9) . 1_545 ? I1 Li5 Li8 140.4(11) 1_455 1_565 ? I1 Li5 Li10 77.2(6) 1_455 . ? I1 Li5 Li11 94.7(8) 1_455 2_676 ? S5 Li5 Li10 48.2(5) 2_667 . ? S6 Li5 Li10 150.2(11) 1_565 . ? S7 Li5 Li10 82.7(8) . . ? Li6 Li5 I1 76.9(13) . 1_455 ? Li6 Li5 S5 60.2(14) . 2_667 ? Li6 Li5 S6 162(2) . 1_565 ? Li6 Li5 S7 78.9(14) . . ? Li6 Li5 Li8 107.7(18) . 2_667 ? Li6 Li5 Li8 83.7(15) . 1_565 ? Li6 Li5 Li10 12.0(12) . . ? Li6 Li5 Li11 151.8(19) . 2_676 ? Li8 Li5 I1 116.4(9) 2_667 1_455 ? Li8 Li5 Li8 39.1(6) 2_667 1_565 ? Li8 Li5 Li10 96.8(9) 2_667 . ? Li8 Li5 Li10 77.1(7) 1_565 . ? Li8 Li5 Li11 117.0(8) 1_565 2_676 ? Li8 Li5 Li11 100.2(8) 2_667 2_676 ? Li10 Li5 Li11 163.1(9) . 2_676 ? Li13 Li5 I1 87(4) . 1_455 ? Li13 Li5 S5 171(4) . 2_667 ? Li13 Li5 S6 84(4) . 1_565 ? Li13 Li5 S7 87(4) . . ? Li13 Li5 Li6 113(5) . . ? Li13 Li5 Li8 133(4) . 1_565 ? Li13 Li5 Li8 137(4) . 2_667 ? Li13 Li5 Li10 125(4) . . ? Li13 Li5 Li11 39(4) . 2_676 ? Li13 Li5 Li14 103(5) . . ? Li14 Li5 I1 77(3) . 1_455 ? Li14 Li5 S5 71(3) . 2_667 ? Li14 Li5 S6 173(4) . 1_565 ? Li14 Li5 S7 76(3) . . ? Li14 Li5 Li6 10(3) . . ? Li14 Li5 Li8 90(3) . 1_565 ? Li14 Li5 Li8 117(4) . 2_667 ? Li14 Li5 Li10 22(3) . . ? Li14 Li5 Li11 142(4) . 2_676 ? I1 Li6 Si2 144.3(6) 1_455 . ? I1 Li6 Li3 54.8(3) 1_455 2_667 ? I1 Li6 Li8 100.0(5) 1_455 2_667 ? I1 Li6 Li8 134.4(7) 1_455 1_565 ? S5 Li6 S6 128.1(9) 2_667 . ? S5 Li6 S7 104.9(6) 2_667 . ? S5 Li6 Si2 119.6(7) 2_667 . ? S6 Li6 Si2 44.2(3) . . ? S7 Li6 S6 87.1(5) . . ? S7 Li6 Si2 44.1(3) . . ? Si2 Li6 Li3 143.0(7) . 2_667 ? Si2 Li6 Li8 112.7(6) . 2_667 ? Si2 Li6 Li8 79.8(5) . 1_565 ? Li5 Li6 I1 77.4(13) . 1_455 ? Li5 Li6 S5 92.7(16) . 2_667 ? Li5 Li6 S6 138.2(18) . . ? Li5 Li6 S7 71.6(13) . . ? Li5 Li6 Si2 111.7(15) . . ? Li5 Li6 Li3 103.2(14) . 2_667 ? Li5 Li6 Li8 72.5(14) . 1_565 ? Li5 Li6 Li8 51.4(15) . 2_667 ? Li5 Li6 Li10 161.4(18) . . ? Li5 Li6 Li13 19.0(13) . . ? Li8 Li6 Li3 99.9(5) 1_565 2_667 ? Li8 Li6 Li3 79.7(4) 2_667 2_667 ? Li8 Li6 Li8 34.5(5) 1_565 2_667 ? Li10 Li6 I1 101.9(7) . 1_455 ? Li10 Li6 S5 68.8(6) . 2_667 ? Li10 Li6 S6 60.2(5) . . ? Li10 Li6 S7 113.0(8) . . ? Li10 Li6 Si2 79.9(6) . . ? Li10 Li6 Li3 63.3(5) . 2_667 ? Li10 Li6 Li8 96.4(7) . 1_565 ? Li10 Li6 Li8 111.3(7) . 2_667 ? Li13 Li6 I1 75.1(10) . 1_455 ? Li13 Li6 S5 111.6(12) . 2_667 ? Li13 Li6 S6 119.9(12) . . ? Li13 Li6 S7 69.9(10) . . ? Li13 Li6 Si2 102.3(11) . . ? Li13 Li6 Li3 114.7(11) . 2_667 ? Li13 Li6 Li8 86.1(11) . 1_565 ? Li13 Li6 Li8 69.9(11) . 2_667 ? Li13 Li6 Li10 176.9(14) . . ? I1 Li7 Si1 116.5(3) 2_766 2_766 ? I1 Li7 Li1 57.97(19) 2_766 2_766 ? I1 Li7 Li3 54.26(17) 2_766 2_766 ? I1 Li7 Li11 111.3(3) 2_766 . ? I1 Li7 Li12 116.6(3) 2_766 . ? I1 Li7 Li13 56.2(5) 2_766 2_666 ? S1 Li7 Li11 71.2(3) . . ? S1 Li7 Li12 61.81(19) . . ? S2 Li7 Li11 52.7(2) 2_766 . ? S2 Li7 Li12 137.1(4) 2_766 . ? S3 Li7 Li11 128.7(4) 2_766 . ? S3 Li7 Li12 62.32(19) 2_766 . ? Si1 Li7 Li1 84.4(2) 2_766 2_766 ? Si1 Li7 Li3 77.7(2) 2_766 2_766 ? Si1 Li7 Li11 88.6(3) 2_766 . ? Si1 Li7 Li12 98.5(3) 2_766 . ? Si1 Li7 Li13 165.3(5) 2_766 2_666 ? Li1 Li7 Li3 87.8(3) 2_766 2_766 ? Li1 Li7 Li11 161.7(3) 2_766 . ? Li1 Li7 Li13 99.6(5) 2_766 2_666 ? Li3 Li7 Li11 74.2(3) 2_766 . ? Li4 Li7 I1 115.9(4) . 2_766 ? Li4 Li7 S1 62.8(3) . . ? Li4 Li7 S2 137.2(5) . 2_766 ? Li4 Li7 S3 61.5(3) . 2_766 ? Li4 Li7 Si1 98.2(4) . 2_766 ? Li4 Li7 Li1 75.6(4) . 2_766 ? Li4 Li7 Li3 163.3(5) . 2_766 ? Li4 Li7 Li9 118.9(5) . 2_766 ? Li4 Li7 Li11 122.3(4) . . ? Li4 Li7 Li12 1.1(3) . . ? Li4 Li7 Li13 96.5(5) . 2_666 ? Li9 Li7 I1 111.0(4) 2_766 2_766 ? Li9 Li7 S2 58.4(3) 2_766 2_766 ? Li9 Li7 S3 132.5(4) 2_766 2_766 ? Li9 Li7 Si1 93.7(4) 2_766 2_766 ? Li9 Li7 Li1 165.5(4) 2_766 2_766 ? Li9 Li7 Li3 77.8(3) 2_766 2_766 ? Li9 Li7 Li11 5.7(3) 2_766 . ? Li9 Li7 Li12 117.8(4) 2_766 . ? Li9 Li7 Li13 78.8(5) 2_766 2_666 ? Li12 Li7 Li1 76.7(2) . 2_766 ? Li12 Li7 Li3 164.3(3) . 2_766 ? Li12 Li7 Li11 121.2(3) . . ? Li12 Li7 Li13 96.2(5) . 2_666 ? Li13 Li7 Li3 88.2(5) 2_666 2_766 ? Li13 Li7 Li11 83.3(5) 2_666 . ? Si2 Li8 Li5 98.1(6) 2_657 1_545 ? Si2 Li8 Li6 79.6(4) 2_657 1_545 ? Si2 Li8 Li13 76.7(5) 2_657 2_667 ? Si2 Li8 Li14 87.4(8) 2_657 1_545 ? Li5 Li8 Si2 83.5(7) 2_667 2_657 ? Li5 Li8 Li5 140.9(6) 2_667 1_545 ? Li5 Li8 Li6 23.7(6) 1_545 1_545 ? Li5 Li8 Li6 150.2(7) 2_667 1_545 ? Li5 Li8 Li13 142.2(8) 1_545 2_667 ? Li5 Li8 Li13 6.9(7) 2_667 2_667 ? Li5 Li8 Li14 150.6(9) 2_667 1_545 ? Li5 Li8 Li14 15.7(7) 1_545 1_545 ? Li6 Li8 Li13 146.9(7) 1_545 2_667 ? Li8 Li8 S5 73.9(5) 2_657 . ? Li8 Li8 S5 61.3(6) 2_657 2_657 ? Li8 Li8 S6 115.7(8) 2_657 2_657 ? Li8 Li8 S7 110.6(8) 2_657 1_545 ? Li8 Li8 Si2 93.2(7) 2_657 2_657 ? Li8 Li8 Li5 76.6(8) 2_657 2_667 ? Li8 Li8 Li5 64.2(8) 2_657 1_545 ? Li8 Li8 Li6 80.0(7) 2_657 1_545 ? Li8 Li8 Li10 176.4(9) 2_657 2_657 ? Li8 Li8 Li13 78.5(7) 2_657 2_667 ? Li8 Li8 Li14 76.1(10) 2_657 1_545 ? Li10 Li8 S5 115.2(5) 2_657 2_657 ? Li10 Li8 S5 109.6(6) 2_657 . ? Li10 Li8 S6 64.2(4) 2_657 2_657 ? Li10 Li8 S7 68.5(5) 2_657 1_545 ? Li10 Li8 Si2 84.3(4) 2_657 2_657 ? Li10 Li8 Li5 105.6(8) 2_657 2_667 ? Li10 Li8 Li5 113.4(7) 2_657 1_545 ? Li10 Li8 Li6 96.9(6) 2_657 1_545 ? Li10 Li8 Li13 103.4(6) 2_657 2_667 ? Li10 Li8 Li14 101.1(9) 2_657 1_545 ? Li14 Li8 Li6 8.5(7) 1_545 1_545 ? Li14 Li8 Li13 149.1(8) 1_545 2_667 ? S1 Li9 Li4 114.8(4) 2_766 . ? S1 Li9 Li12 126.2(3) 2_766 . ? S2 Li9 Li4 55.2(3) . . ? S2 Li9 Li12 50.26(18) . . ? S3 Li9 Li4 49.4(3) 2_766 . ? S3 Li9 Li12 58.2(2) 2_766 . ? S6 Li9 Li4 132.5(5) 1_655 . ? S6 Li9 Li12 120.9(4) 1_655 . ? Si1 Li9 Li4 78.7(3) 2_766 . ? Si1 Li9 Li4 101.2(3) 2_766 2_756 ? Si1 Li9 Li12 90.2(2) 2_766 . ? Li4 Li9 Li4 22.8(5) . 2_756 ? Li4 Li9 Li12 11.7(2) . . ? Li7 Li9 S1 55.5(4) 2_766 2_766 ? Li7 Li9 S3 107.7(4) 2_766 2_766 ? Li7 Li9 S6 108.5(5) 2_766 1_655 ? Li7 Li9 Si1 76.8(4) 2_766 2_766 ? Li7 Li9 Li4 102.9(4) 2_766 2_756 ? Li7 Li9 Li4 93.9(4) 2_766 . ? Li7 Li9 Li12 98.7(4) 2_766 . ? Li11 Li9 S1 142.7(10) 2_766 2_766 ? Li11 Li9 S2 97.5(9) 2_766 . ? Li11 Li9 S3 74.4(8) 2_766 2_766 ? Li11 Li9 S6 73.5(8) 2_766 1_655 ? Li11 Li9 Si1 112.8(9) 2_766 2_766 ? Li11 Li9 Li4 59.5(8) 2_766 2_756 ? Li11 Li9 Li4 72.5(8) 2_766 . ? Li11 Li9 Li7 160.5(10) 2_766 2_766 ? Li11 Li9 Li12 65.4(8) 2_766 . ? Li12 Li9 Li4 11.1(2) . 2_756 ? I1 Li10 Si2 112.0(3) 2_667 2_667 ? I1 Li10 Li1 55.2(2) 2_667 2_667 ? I1 Li10 Li3 54.8(2) 2_667 2_667 ? I1 Li10 Li5 115.2(5) 2_667 . ? S5 Li10 Li5 51.3(5) 2_667 . ? S5 Li10 Li14 58.0(8) 2_667 . ? S6 Li10 Li5 71.7(5) . . ? S6 Li10 Li14 65.1(8) . . ? S7 Li10 Li5 125.7(6) 2_667 . ? S7 Li10 Li14 130.2(8) 2_667 . ? Si2 Li10 Li1 80.9(3) 2_667 2_667 ? Si2 Li10 Li3 76.2(3) 2_667 2_667 ? Si2 Li10 Li5 86.3(5) 2_667 . ? Li1 Li10 Li5 158.2(6) 2_667 . ? Li3 Li10 Li1 86.7(3) 2_667 2_667 ? Li3 Li10 Li5 73.0(5) 2_667 . ? Li6 Li10 I1 115.9(6) . 2_667 ? Li6 Li10 S5 57.8(5) . 2_667 ? Li6 Li10 S6 65.2(5) . . ? Li6 Li10 S7 130.1(7) . 2_667 ? Li6 Li10 Si2 92.0(6) . 2_667 ? Li6 Li10 Li1 163.9(6) . 2_667 ? Li6 Li10 Li3 77.6(5) . 2_667 ? Li6 Li10 Li5 6.6(6) . . ? Li6 Li10 Li14 0.1(11) . . ? Li8 Li10 I1 114.5(5) 2_657 2_667 ? Li8 Li10 S5 135.2(6) 2_657 2_667 ? Li8 Li10 S6 68.0(4) 2_657 . ? Li8 Li10 S7 64.0(4) 2_657 2_667 ? Li8 Li10 Si2 98.4(5) 2_657 2_667 ? Li8 Li10 Li1 76.0(4) 2_657 2_667 ? Li8 Li10 Li3 162.5(6) 2_657 2_667 ? Li8 Li10 Li5 123.7(6) 2_657 . ? Li8 Li10 Li6 119.5(7) 2_657 . ? Li8 Li10 Li14 119.5(9) 2_657 . ? Li14 Li10 I1 115.8(8) . 2_667 ? Li14 Li10 Si2 92.2(8) . 2_667 ? Li14 Li10 Li1 164.0(8) . 2_667 ? Li14 Li10 Li3 77.6(8) . 2_667 ? Li14 Li10 Li5 6.7(9) . . ? S1 Li11 Li7 140.5(4) 1_565 . ? S2 Li11 Li7 47.2(3) 2_766 . ? S3 Li11 Li7 84.6(4) . . ? S4 Li11 Li7 124.2(4) 2_666 . ? S6 Li11 Li7 85.9(4) 2_666 . ? Li4 Li11 Li4 25.0(5) 1_565 2_766 ? Li4 Li11 Li5 117.1(6) 2_766 2_676 ? Li4 Li11 Li5 92.1(6) 1_565 2_676 ? Li4 Li11 Li7 90.9(4) 1_565 . ? Li4 Li11 Li7 79.6(4) 2_766 . ? Li4 Li11 Li13 87.2(6) 1_565 2_676 ? Li4 Li11 Li13 112.1(6) 2_766 2_676 ? Li7 Li11 Li5 118.2(5) . 2_676 ? Li9 Li11 S1 153.8(10) 2_766 1_565 ? Li9 Li11 S2 61.0(8) 2_766 2_766 ? Li9 Li11 S3 82.2(8) 2_766 . ? Li9 Li11 S4 110.6(9) 2_766 2_666 ? Li9 Li11 S6 83.5(8) 2_766 2_666 ? Li9 Li11 Li4 103.3(9) 2_766 1_565 ? Li9 Li11 Li4 88.8(9) 2_766 2_766 ? Li9 Li11 Li5 122.8(10) 2_766 2_676 ? Li9 Li11 Li7 13.8(7) 2_766 . ? Li9 Li11 Li12 96.1(9) 2_766 1_565 ? Li9 Li11 Li13 128.1(10) 2_766 2_676 ? Li12 Li11 Li4 12.6(3) 1_565 1_565 ? Li12 Li11 Li4 12.3(2) 1_565 2_766 ? Li12 Li11 Li5 104.7(5) 1_565 2_676 ? Li12 Li11 Li7 85.1(3) 1_565 . ? Li12 Li11 Li13 99.8(6) 1_565 2_676 ? Li13 Li11 Li5 6.4(6) 2_676 2_676 ? Li13 Li11 Li7 122.4(5) 2_676 . ? S1 Li12 Li7 48.12(17) . . ? S1 Li12 Li7 131.88(17) 2_756 . ? S2 Li12 S1 82.934(18) . . ? S2 Li12 S1 97.067(18) 2_756 . ? S2 Li12 Li7 82.59(17) 2_756 . ? S2 Li12 Li7 97.41(17) . . ? S3 Li12 Li7 50.48(17) 2_766 . ? S3 Li12 Li7 129.52(17) 1_545 . ? Li4 Li12 S1 128.3(9) 2_756 . ? Li4 Li12 S1 51.7(9) 2_756 2_756 ? Li4 Li12 S1 128.3(9) . 2_756 ? Li4 Li12 S1 51.7(9) . . ? Li4 Li12 S2 100.1(9) 2_756 2_756 ? Li4 Li12 S2 100.0(9) . . ? Li4 Li12 S2 80.0(9) . 2_756 ? Li4 Li12 S2 79.9(9) 2_756 . ? Li4 Li12 S3 47.7(9) 2_756 1_545 ? Li4 Li12 S3 132.3(9) . 1_545 ? Li4 Li12 S3 47.7(9) . 2_766 ? Li4 Li12 S3 132.3(9) 2_756 2_766 ? Li4 Li12 Li4 180.0 2_756 . ? Li4 Li12 Li7 3.9(9) 2_756 2_756 ? Li4 Li12 Li7 3.9(9) . . ? Li4 Li12 Li7 176.1(9) 2_756 . ? Li4 Li12 Li7 176.1(9) . 2_756 ? Li4 Li12 Li11 93.2(9) 2_756 1_545 ? Li4 Li12 Li11 86.8(9) 2_756 2_766 ? Li4 Li12 Li11 86.8(9) . 1_545 ? Li4 Li12 Li11 93.2(9) . 2_766 ? Li7 Li12 Li7 180.0 2_756 . ? Li11 Li12 Li7 94.4(3) 2_766 . ? Li11 Li12 Li7 85.6(3) 2_766 2_756 ? Li11 Li12 Li7 94.4(3) 1_545 2_756 ? Li11 Li12 Li7 85.6(3) 1_545 . ? Li11 Li12 Li11 180.0 2_766 1_545 ? I1 Li13 Li2 145.3(10) 1_455 . ? I1 Li13 Li7 53.6(4) 1_455 2_666 ? I1 Li13 Li8 103.6(8) 1_455 2_667 ? I1 Li13 Li8 122.3(9) 1_455 1_565 ? I1 Li13 Li11 103.9(7) 1_455 2_676 ? S1 Li13 Li2 48.6(4) 2_666 . ? S6 Li13 Li2 98.3(7) 1_565 . ? S7 Li13 Li2 49.5(4) . . ? Li2 Li13 Li7 91.9(7) . 2_666 ? Li2 Li13 Li8 89.3(6) . 1_565 ? Li5 Li13 I1 82(4) . 1_455 ? Li5 Li13 S1 171(4) . 2_666 ? Li5 Li13 S6 83(4) . 1_565 ? Li5 Li13 S7 80(4) . . ? Li5 Li13 Li2 128(4) . . ? Li5 Li13 Li6 48(4) . . ? Li5 Li13 Li7 132(4) . 2_666 ? Li5 Li13 Li8 40(4) . 1_565 ? Li5 Li13 Li8 37(4) . 2_667 ? Li5 Li13 Li11 135(4) . 2_676 ? Li5 Li13 Li14 48(3) . . ? Li6 Li13 I1 73.0(10) . 1_455 ? Li6 Li13 S1 123.7(12) . 2_666 ? Li6 Li13 S6 130.6(16) . 1_565 ? Li6 Li13 S7 73.4(10) . . ? Li6 Li13 Li2 113.1(11) . . ? Li6 Li13 Li7 97.6(11) . 2_666 ? Li6 Li13 Li8 82.7(12) . 2_667 ? Li6 Li13 Li8 66.4(11) . 1_565 ? Li6 Li13 Li11 176.0(14) . 2_676 ? Li7 Li13 Li8 162.9(7) 2_666 1_565 ? Li8 Li13 Li2 111.0(7) 2_667 . ? Li8 Li13 Li7 155.1(8) 2_667 2_666 ? Li8 Li13 Li8 34.1(5) 2_667 1_565 ? Li11 Li13 Li2 68.0(6) 2_676 . ? Li11 Li13 Li7 78.5(7) 2_676 2_666 ? Li11 Li13 Li8 100.6(6) 2_676 2_667 ? Li11 Li13 Li8 117.6(7) 2_676 1_565 ? Li14 Li13 I1 74(2) . 1_455 ? Li14 Li13 S1 124(3) . 2_666 ? Li14 Li13 S6 131(3) . 1_565 ? Li14 Li13 S7 72(2) . . ? Li14 Li13 Li2 112(2) . . ? Li14 Li13 Li6 1(2) . . ? Li14 Li13 Li7 98(2) . 2_666 ? Li14 Li13 Li8 82(2) . 2_667 ? Li14 Li13 Li8 66(2) . 1_565 ? Li14 Li13 Li11 177(3) . 2_676 ? I1 Li14 Si2 141.2(15) 1_455 . ? I1 Li14 Li8 137.8(13) 1_455 1_565 ? I1 Li14 Li8 104.6(11) 1_455 2_667 ? S5 Li14 S6 110.6(16) 2_667 . ? S5 Li14 Si2 109.3(13) 2_667 . ? S5 Li14 Li10 59.2(9) 2_667 . ? S6 Li14 Si2 41.7(5) . . ? S7 Li14 S6 84.3(11) . . ? S7 Li14 Si2 42.8(6) . . ? S7 Li14 Li10 102.7(14) . . ? Si2 Li14 Li8 113.4(10) . 2_667 ? Si2 Li14 Li8 78.3(8) . 1_565 ? Li5 Li14 I1 86(3) . 1_455 ? Li5 Li14 S5 92(3) . 2_667 ? Li5 Li14 S6 157(4) . . ? Li5 Li14 S7 84(3) . . ? Li5 Li14 Si2 125(3) . . ? Li5 Li14 Li8 49(3) . 2_667 ? Li5 Li14 Li8 74(3) . 1_565 ? Li5 Li14 Li10 151(4) . . ? Li5 Li14 Li13 29(2) . . ? Li8 Li14 Li8 35.5(6) 1_565 2_667 ? Li10 Li14 I1 92.6(12) . 1_455 ? Li10 Li14 S6 52.0(9) . . ? Li10 Li14 Si2 71.5(10) . . ? Li10 Li14 Li8 103.6(11) . 2_667 ? Li10 Li14 Li8 87.8(11) . 1_565 ? Li13 Li14 I1 83(2) . 1_455 ? Li13 Li14 S5 121(3) . 2_667 ? Li13 Li14 S6 128(3) . . ? Li13 Li14 S7 81(2) . . ? Li13 Li14 Si2 112(2) . . ? Li13 Li14 Li8 78(3) . 2_667 ? Li13 Li14 Li8 95(3) . 1_565 ? Li13 Li14 Li10 176(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag I1 Li1 2.847(5) . ? I1 Li3 2.797(5) . ? I1 Li3 2.966(5) 2_767 ? I1 Li3 3.303(5) 1_565 ? I1 Li5 2.82(2) 1_655 ? I1 Li6 2.813(17) 1_655 ? I1 Li7 2.754(9) 2_766 ? I1 Li10 2.845(10) 2_667 ? I1 Li13 2.84(2) 1_655 ? I1 Li14 2.75(3) 1_655 ? Cl1 Li1 2.847(5) . ? Cl1 Li3 2.966(5) 2_767 ? Cl1 Li3 2.797(5) . ? Cl1 Li5 2.82(2) 1_655 ? Cl1 Li6 2.813(17) 1_655 ? Cl1 Li7 2.754(9) 2_766 ? Cl1 Li10 2.845(10) 2_667 ? Cl1 Li13 2.84(2) 1_655 ? Cl1 Li14 2.75(3) 1_655 ? S1 Si1 2.0981(9) . ? S1 Li2 2.466(5) 2_666 ? S1 Li4 2.428(11) . ? S1 Li7 2.346(9) . ? S1 Li9 2.595(12) 2_766 ? S1 Li11 2.642(14) 1_545 ? S1 Li12 2.7767(6) . ? S1 Li13 2.68(3) 2_666 ? S2 Si1 2.1067(8) . ? S2 Li1 2.631(5) 1_545 ? S2 Li3 2.470(5) . ? S2 Li4 2.676(11) . ? S2 Li4 2.457(10) 2_756 ? S2 Li7 2.540(9) 2_766 ? S2 Li9 2.427(9) . ? S2 Li11 2.751(11) 2_766 ? S2 Li12 2.4855(6) . ? S3 Si1 2.0954(8) . ? S3 Li1 2.551(5) . ? S3 Li2 2.493(5) . ? S3 Li4 2.456(11) 2_766 ? S3 Li7 2.478(9) 2_766 ? S3 Li9 2.542(10) 2_766 ? S3 Li11 2.471(10) . ? S3 Li12 2.8449(6) 1_565 ? S4 Si1 2.1929(8) . ? S4 Si2 2.1955(9) . ? S4 Li1 2.898(5) 1_545 ? S4 Li2 2.818(6) 1_545 ? S4 Li2 3.006(5) 2_666 ? S4 Li11 2.884(11) 2_666 ? S5 Si2 2.1041(8) . ? S5 Li1 2.725(5) 1_545 ? S5 Li3 2.461(5) . ? S5 Li5 2.74(3) 2_667 ? S5 Li6 2.382(18) 2_667 ? S5 Li8 2.625(11) 2_657 ? S5 Li8 2.397(9) . ? S5 Li10 2.623(11) 2_667 ? S5 Li14 2.59(3) 2_667 ? S6 Si2 2.1043(9) . ? S6 Li5 2.51(3) 1_545 ? S6 Li6 2.515(18) . ? S6 Li8 2.478(10) 2_657 ? S6 Li9 2.603(9) 1_455 ? S6 Li10 2.405(10) . ? S6 Li11 2.512(10) 2_666 ? S6 Li13 2.51(2) 1_545 ? S6 Li14 2.77(4) . ? S7 Si2 2.0976(8) . ? S7 Li1 2.542(5) . ? S7 Li2 2.457(5) . ? S7 Li5 2.41(2) . ? S7 Li6 2.496(18) . ? S7 Li8 2.414(11) 1_565 ? S7 Li10 2.499(11) 2_667 ? S7 Li13 2.45(2) . ? S7 Li14 2.36(3) . ? Li1 Li2 2.946(7) . ? Li1 Li3 3.084(7) 1_565 ? Li1 Li4 3.369(12) 2_766 ? Li1 Li7 3.090(10) 2_766 ? Li1 Li10 3.255(12) 2_667 ? Li2 Li11 3.519(15) 2_676 ? Li2 Li13 3.20(2) . ? Li3 Li6 3.494(19) 2_667 ? Li3 Li7 3.291(10) 2_766 ? Li3 Li10 3.195(12) 2_667 ? Li4 Li4 1.30(3) 2_756 ? Li4 Li7 2.315(16) . ? Li4 Li9 3.341(15) 2_756 ? Li4 Li9 3.174(14) . ? Li4 Li11 3.027(15) 2_766 ? Li4 Li11 2.956(15) 1_545 ? Li4 Li12 0.648(13) . ? Li5 Li6 1.25(3) . ? Li5 Li8 2.75(3) 2_667 ? Li5 Li8 2.97(3) 1_565 ? Li5 Li10 3.47(3) . ? Li5 Li11 3.51(3) 2_676 ? Li5 Li13 0.55(2) . ? Li5 Li14 0.83(4) . ? Li6 Li8 3.35(2) 2_667 ? Li6 Li8 3.10(2) 1_565 ? Li6 Li10 2.26(2) . ? Li6 Li13 1.56(3) . ? Li7 Li9 2.431(17) 2_766 ? Li7 Li11 3.409(16) . ? Li7 Li12 2.962(8) . ? Li7 Li13 3.22(3) 2_666 ? Li8 Li8 1.93(2) 2_657 ? Li8 Li10 1.980(17) 2_657 ? Li8 Li13 3.17(3) 2_667 ? Li8 Li14 3.09(4) 1_545 ? Li9 Li11 1.019(13) 2_766 ? Li9 Li12 3.193(10) . ? Li10 Li14 2.72(5) . ? Li11 Li12 2.921(10) 1_565 ? Li11 Li13 3.09(3) 2_676 ? Li13 Li14 1.10(5) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag I1 Li5 Li6 Si2 143.7(9) 1_455 . . . ? I1 Li5 Li6 Li3 -48.8(7) 1_455 . . 2_667 ? I1 Li5 Li6 Li8 -145.2(7) 1_455 . . 1_565 ? I1 Li5 Li6 Li8 -113.9(11) 1_455 . . 2_667 ? I1 Li5 Li6 Li10 -90(5) 1_455 . . . ? I1 Li5 Li6 Li13 81(5) 1_455 . . . ? I1 Li5 Li13 Li2 -162(3) 1_455 . . . ? I1 Li5 Li13 Li6 -74(3) 1_455 . . . ? I1 Li5 Li13 Li7 -20(4) 1_455 . . 2_666 ? I1 Li5 Li13 Li8 -178(5) 1_455 . . 1_565 ? I1 Li5 Li13 Li8 126(5) 1_455 . . 2_667 ? I1 Li5 Li13 Li11 102(4) 1_455 . . 2_676 ? I1 Li5 Li13 Li14 -76(4) 1_455 . . . ? I1 Li5 Li14 Si2 155(3) 1_455 . . . ? I1 Li5 Li14 Li8 -142.3(8) 1_455 . . 1_565 ? I1 Li5 Li14 Li8 -113.2(19) 1_455 . . 2_667 ? I1 Li5 Li14 Li10 -88(6) 1_455 . . . ? I1 Li5 Li14 Li13 84(5) 1_455 . . . ? I1 Li6 Li13 Li2 -143.6(11) 1_455 . . . ? I1 Li6 Li13 Li5 95(5) 1_455 . . . ? I1 Li6 Li13 Li7 -48.2(5) 1_455 . . 2_666 ? I1 Li6 Li13 Li8 138.0(6) 1_455 . . 1_565 ? I1 Li6 Li13 Li8 106.7(5) 1_455 . . 2_667 ? I1 Li6 Li13 Li14 -173(100) 1_455 . . . ? I1 Li13 Li14 Si2 142.9(19) 1_455 . . . ? I1 Li13 Li14 Li5 -94(5) 1_455 . . . ? I1 Li13 Li14 Li8 -106.6(7) 1_455 . . 2_667 ? I1 Li13 Li14 Li8 -137.6(12) 1_455 . . 1_565 ? S1 Li4 Li12 S1 180.001(1) . . . 2_756 ? S1 Li4 Li12 S2 107.4(8) . . . 2_756 ? S1 Li4 Li12 S2 -72.6(8) . . . . ? S1 Li4 Li12 S3 21.9(15) . . . 1_545 ? S1 Li4 Li12 S3 -158.1(15) . . . 2_766 ? S1 Li4 Li12 Li7 -25(13) . . . . ? S1 Li4 Li12 Li11 -133.2(7) . . . 2_766 ? S1 Li4 Li12 Li11 46.8(7) . . . 1_545 ? S1 Li13 Li14 S5 -176.1(10) 2_666 . . 2_667 ? S1 Li13 Li14 S6 8(4) 2_666 . . . ? S1 Li13 Li14 S7 84.0(18) 2_666 . . . ? S1 Li13 Li14 Si2 53(3) 2_666 . . . ? S1 Li13 Li14 Li5 177(6) 2_666 . . . ? S1 Li13 Li14 Li8 132.7(15) 2_666 . . 1_565 ? S1 Li13 Li14 Li8 163.7(17) 2_666 . . 2_667 ? S2 Li4 Li12 S1 72.6(8) 2_756 . . 2_756 ? S2 Li4 Li12 S1 -107.4(8) 2_756 . . . ? S2 Li4 Li12 S1 72.6(8) . . . . ? S2 Li4 Li12 S1 -107.4(8) . . . 2_756 ? S2 Li4 Li12 S2 179.999(1) 2_756 . . . ? S2 Li4 Li12 S2 180.001(2) . . . 2_756 ? S2 Li4 Li12 S3 -85.5(8) 2_756 . . 1_545 ? S2 Li4 Li12 S3 94.5(8) . . . 1_545 ? S2 Li4 Li12 S3 -85.5(8) . . . 2_766 ? S2 Li4 Li12 S3 94.5(8) 2_756 . . 2_766 ? S2 Li4 Li12 Li7 48(14) . . . . ? S2 Li4 Li12 Li7 -132(14) 2_756 . . . ? S2 Li4 Li12 Li11 -60.6(3) . . . 2_766 ? S2 Li4 Li12 Li11 119.4(3) 2_756 . . 2_766 ? S2 Li4 Li12 Li11 119.4(3) . . . 1_545 ? S2 Li4 Li12 Li11 -60.6(3) 2_756 . . 1_545 ? S3 Li4 Li12 S1 158.1(15) 2_766 . . . ? S3 Li4 Li12 S1 -21.9(15) 2_766 . . 2_756 ? S3 Li4 Li12 S2 85.5(8) 2_766 . . . ? S3 Li4 Li12 S2 -94.5(8) 2_766 . . 2_756 ? S3 Li4 Li12 S3 180.000(1) 2_766 . . 1_545 ? S3 Li4 Li12 Li7 133(14) 2_766 . . . ? S3 Li4 Li12 Li11 24.8(9) 2_766 . . 2_766 ? S3 Li4 Li12 Li11 -155.2(9) 2_766 . . 1_545 ? S5 Li5 Li6 S6 -168(2) 2_667 . . . ? S5 Li5 Li6 S7 -104.9(7) 2_667 . . . ? S5 Li5 Li6 Si2 -123.5(11) 2_667 . . . ? S5 Li5 Li6 Li3 44.0(5) 2_667 . . 2_667 ? S5 Li5 Li6 Li8 -21.1(11) 2_667 . . 2_667 ? S5 Li5 Li6 Li8 -52.4(6) 2_667 . . 1_565 ? S5 Li5 Li6 Li10 3(4) 2_667 . . . ? S5 Li5 Li6 Li13 173(5) 2_667 . . . ? S5 Li5 Li14 S6 -162(9) 2_667 . . . ? S5 Li5 Li14 S7 -102.7(11) 2_667 . . . ? S5 Li5 Li14 Si2 -115(3) 2_667 . . . ? S5 Li5 Li14 Li8 -23(3) 2_667 . . 2_667 ? S5 Li5 Li14 Li8 -52.0(10) 2_667 . . 1_565 ? S5 Li5 Li14 Li10 2(6) 2_667 . . . ? S5 Li5 Li14 Li13 174(4) 2_667 . . . ? S5 Li6 Li13 S1 -176.6(8) 2_667 . . 2_666 ? S5 Li6 Li13 S6 4(2) 2_667 . . 1_565 ? S5 Li6 Li13 S7 98.7(9) 2_667 . . . ? S5 Li6 Li13 Li2 128.8(9) 2_667 . . . ? S5 Li6 Li13 Li5 7(5) 2_667 . . . ? S5 Li6 Li13 Li7 -135.8(8) 2_667 . . 2_666 ? S5 Li6 Li13 Li8 50.3(7) 2_667 . . 1_565 ? S5 Li6 Li13 Li8 19.1(9) 2_667 . . 2_667 ? S5 Li6 Li13 Li14 99(100) 2_667 . . . ? S6 Li5 Li6 S5 -2(6) 1_565 . . 2_667 ? S6 Li5 Li6 S6 -170(4) 1_565 . . . ? S6 Li5 Li6 S7 -106(6) 1_565 . . . ? S6 Li5 Li6 Si2 -125(5) 1_565 . . . ? S6 Li5 Li6 Li3 42(6) 1_565 . . 2_667 ? S6 Li5 Li6 Li8 -23(5) 1_565 . . 2_667 ? S6 Li5 Li6 Li8 -54(5) 1_565 . . 1_565 ? S6 Li5 Li6 Li10 1(10) 1_565 . . . ? S6 Li5 Li6 Li13 172(10) 1_565 . . . ? S6 Li5 Li13 S7 106.0(6) 1_565 . . . ? S6 Li5 Li13 Li2 95(4) 1_565 . . . ? S6 Li5 Li13 Li6 -178(3) 1_565 . . . ? S6 Li5 Li13 Li7 -124(4) 1_565 . . 2_666 ? S6 Li5 Li13 Li8 23(5) 1_565 . . 2_667 ? S6 Li5 Li13 Li8 79(4) 1_565 . . 1_565 ? S6 Li5 Li13 Li11 -2(5) 1_565 . . 2_676 ? S6 Li5 Li13 Li14 -179(4) 1_565 . . . ? S6 Li6 Li13 S1 11(2) . . . 2_666 ? S6 Li6 Li13 S6 -169.1(9) . . . 1_565 ? S6 Li6 Li13 S7 -74.2(10) . . . . ? S6 Li6 Li13 Li2 -44.1(16) . . . . ? S6 Li6 Li13 Li5 -166(5) . . . . ? S6 Li6 Li13 Li7 51.3(12) . . . 2_666 ? S6 Li6 Li13 Li8 -153.8(9) . . . 2_667 ? S6 Li6 Li13 Li8 -122.5(11) . . . 1_565 ? S6 Li6 Li13 Li14 -74(100) . . . . ? S6 Li13 Li14 S5 6(4) 1_565 . . 2_667 ? S6 Li13 Li14 S6 -169.5(12) 1_565 . . . ? S6 Li13 Li14 S7 -94(2) 1_565 . . . ? S6 Li13 Li14 Si2 -124.8(19) 1_565 . . . ? S6 Li13 Li14 Li5 -1(5) 1_565 . . . ? S6 Li13 Li14 Li8 -14(2) 1_565 . . 2_667 ? S6 Li13 Li14 Li8 -45(3) 1_565 . . 1_565 ? S7 Li5 Li6 S5 104.9(7) . . . 2_667 ? S7 Li5 Li6 S6 -63(2) . . . . ? S7 Li5 Li6 Si2 -18.6(11) . . . . ? S7 Li5 Li6 Li3 148.9(7) . . . 2_667 ? S7 Li5 Li6 Li8 52.5(4) . . . 1_565 ? S7 Li5 Li6 Li8 83.8(10) . . . 2_667 ? S7 Li5 Li6 Li10 108(5) . . . . ? S7 Li5 Li6 Li13 -82(5) . . . . ? S7 Li5 Li13 S6 -106.0(6) . . . 1_565 ? S7 Li5 Li13 Li2 -11(4) . . . . ? S7 Li5 Li13 Li6 77(3) . . . . ? S7 Li5 Li13 Li7 131(4) . . . 2_666 ? S7 Li5 Li13 Li8 -27(4) . . . 1_565 ? S7 Li5 Li13 Li8 -83(5) . . . 2_667 ? S7 Li5 Li13 Li11 -108(4) . . . 2_676 ? S7 Li5 Li13 Li14 75(4) . . . . ? S7 Li5 Li14 S5 102.7(11) . . . 2_667 ? S7 Li5 Li14 S6 -60(8) . . . . ? S7 Li5 Li14 Si2 -12(3) . . . . ? S7 Li5 Li14 Li8 50.7(7) . . . 1_565 ? S7 Li5 Li14 Li8 80(2) . . . 2_667 ? S7 Li5 Li14 Li10 105(7) . . . . ? S7 Li5 Li14 Li13 -83(5) . . . . ? S7 Li6 Li13 S1 84.8(12) . . . 2_666 ? S7 Li6 Li13 S6 -94.9(15) . . . 1_565 ? S7 Li6 Li13 Li2 30.1(7) . . . . ? S7 Li6 Li13 Li5 -92(5) . . . . ? S7 Li6 Li13 Li7 125.5(8) . . . 2_666 ? S7 Li6 Li13 Li8 -48.3(4) . . . 1_565 ? S7 Li6 Li13 Li8 -79.6(5) . . . 2_667 ? S7 Li6 Li13 Li14 1(100) . . . . ? S7 Li13 Li14 S5 100(2) . . . 2_667 ? S7 Li13 Li14 S6 -76(2) . . . . ? S7 Li13 Li14 Si2 -30.8(12) . . . . ? S7 Li13 Li14 Li5 93(5) . . . . ? S7 Li13 Li14 Li8 79.7(7) . . . 2_667 ? S7 Li13 Li14 Li8 48.7(7) . . . 1_565 ? Si1 Li4 Li12 S1 -140.1(5) . . . 2_756 ? Si1 Li4 Li12 S1 39.9(5) . . . . ? Si1 Li4 Li12 S2 147.3(4) . . . 2_756 ? Si1 Li4 Li12 S2 -32.7(4) . . . . ? Si1 Li4 Li12 S3 -118.1(10) . . . 2_766 ? Si1 Li4 Li12 S3 61.9(10) . . . 1_545 ? Si1 Li4 Li12 Li7 15(13) . . . . ? Si1 Li4 Li12 Li11 86.7(4) . . . 1_545 ? Si1 Li4 Li12 Li11 -93.3(4) . . . 2_766 ? Si2 Li6 Li13 I1 143.3(7) . . . 1_455 ? Si2 Li6 Li13 S1 54.4(14) . . . 2_666 ? Si2 Li6 Li13 S6 -125.3(13) . . . 1_565 ? Si2 Li6 Li13 S7 -30.4(6) . . . . ? Si2 Li6 Li13 Li2 -0.3(13) . . . . ? Si2 Li6 Li13 Li5 -122(5) . . . . ? Si2 Li6 Li13 Li7 95.1(7) . . . 2_666 ? Si2 Li6 Li13 Li8 -78.7(6) . . . 1_565 ? Si2 Li6 Li13 Li8 -110.0(6) . . . 2_667 ? Si2 Li6 Li13 Li14 -30(100) . . . . ? Li2 Li13 Li14 I1 -143.8(12) . . . 1_455 ? Li2 Li13 Li14 S5 129.8(17) . . . 2_667 ? Li2 Li13 Li14 S6 -46(3) . . . . ? Li2 Li13 Li14 S7 29.9(16) . . . . ? Li2 Li13 Li14 Si2 -1(3) . . . . ? Li2 Li13 Li14 Li5 123(5) . . . . ? Li2 Li13 Li14 Li8 78.6(17) . . . 1_565 ? Li2 Li13 Li14 Li8 109.6(14) . . . 2_667 ? Li3 Li6 Li13 I1 -38.9(8) 2_667 . . 1_455 ? Li3 Li6 Li13 S1 -127.8(10) 2_667 . . 2_666 ? Li3 Li6 Li13 S6 52.6(19) 2_667 . . 1_565 ? Li3 Li6 Li13 S7 147.4(8) 2_667 . . . ? Li3 Li6 Li13 Li2 177.6(6) 2_667 . . . ? Li3 Li6 Li13 Li5 56(5) 2_667 . . . ? Li3 Li6 Li13 Li7 -87.1(9) 2_667 . . 2_666 ? Li3 Li6 Li13 Li8 99.1(8) 2_667 . . 1_565 ? Li3 Li6 Li13 Li8 67.9(8) 2_667 . . 2_667 ? Li3 Li6 Li13 Li14 148(100) 2_667 . . . ? Li4 Li4 Li12 S1 137(29) 2_756 . . . ? Li4 Li4 Li12 S1 -43(29) 2_756 . . 2_756 ? Li4 Li4 Li12 S2 -116(29) 2_756 . . 2_756 ? Li4 Li4 Li12 S2 64(29) 2_756 . . . ? Li4 Li4 Li12 S3 159(29) 2_756 . . 1_545 ? Li4 Li4 Li12 S3 -21(29) 2_756 . . 2_766 ? Li4 Li4 Li12 Li7 112(31) 2_756 . . . ? Li4 Li4 Li12 Li11 -177(29) 2_756 . . 1_545 ? Li4 Li4 Li12 Li11 3(29) 2_756 . . 2_766 ? Li5 Li6 Li13 I1 -95(5) . . . 1_455 ? Li5 Li6 Li13 S1 176(6) . . . 2_666 ? Li5 Li6 Li13 S6 -3(4) . . . 1_565 ? Li5 Li6 Li13 S7 92(5) . . . . ? Li5 Li6 Li13 Li2 122(5) . . . . ? Li5 Li6 Li13 Li7 -143(5) . . . 2_666 ? Li5 Li6 Li13 Li8 12(5) . . . 2_667 ? Li5 Li6 Li13 Li8 43(5) . . . 1_565 ? Li5 Li6 Li13 Li14 92(100) . . . . ? Li5 Li13 Li14 I1 94(5) . . . 1_455 ? Li5 Li13 Li14 S5 7(5) . . . 2_667 ? Li5 Li13 Li14 S6 -168(6) . . . . ? Li5 Li13 Li14 S7 -93(5) . . . . ? Li5 Li13 Li14 Si2 -123(5) . . . . ? Li5 Li13 Li14 Li8 -13(5) . . . 2_667 ? Li5 Li13 Li14 Li8 -44(5) . . . 1_565 ? Li6 Li5 Li13 I1 74(3) . . . 1_455 ? Li6 Li5 Li13 S6 178(3) . . . 1_565 ? Li6 Li5 Li13 S7 -77(3) . . . . ? Li6 Li5 Li13 Li2 -87(5) . . . . ? Li6 Li5 Li13 Li7 54(6) . . . 2_666 ? Li6 Li5 Li13 Li8 -104(6) . . . 1_565 ? Li6 Li5 Li13 Li8 -160(8) . . . 2_667 ? Li6 Li5 Li13 Li11 176(2) . . . 2_676 ? Li6 Li5 Li13 Li14 -1(3) . . . . ? Li6 Li5 Li14 I1 89(15) . . . 1_455 ? Li6 Li5 Li14 S5 -1(15) . . . 2_667 ? Li6 Li5 Li14 S6 -164(23) . . . . ? Li6 Li5 Li14 S7 -104(16) . . . . ? Li6 Li5 Li14 Si2 -116(17) . . . . ? Li6 Li5 Li14 Li8 -24(17) . . . 2_667 ? Li6 Li5 Li14 Li8 -53(15) . . . 1_565 ? Li6 Li5 Li14 Li10 1(10) . . . . ? Li6 Li5 Li14 Li13 172(14) . . . . ? Li6 Li13 Li14 I1 7(100) . . . 1_455 ? Li6 Li13 Li14 S5 -80(100) . . . 2_667 ? Li6 Li13 Li14 S6 105(100) . . . . ? Li6 Li13 Li14 S7 -179(100) . . . . ? Li6 Li13 Li14 Si2 150(100) . . . . ? Li6 Li13 Li14 Li5 -87(100) . . . . ? Li6 Li13 Li14 Li8 -100(100) . . . 2_667 ? Li6 Li13 Li14 Li8 -131(100) . . . 1_565 ? Li7 Li13 Li14 I1 -48.4(9) 2_666 . . 1_455 ? Li7 Li13 Li14 S5 -134.8(18) 2_666 . . 2_667 ? Li7 Li13 Li14 S6 50(3) 2_666 . . . ? Li7 Li13 Li14 S7 125.4(8) 2_666 . . . ? Li7 Li13 Li14 Si2 94.5(15) 2_666 . . . ? Li7 Li13 Li14 Li5 -142(5) 2_666 . . . ? Li7 Li13 Li14 Li8 174.1(7) 2_666 . . 1_565 ? Li7 Li13 Li14 Li8 -154.9(9) 2_666 . . 2_667 ? Li8 Li5 Li6 I1 113.9(11) 2_667 . . 1_455 ? Li8 Li5 Li6 I1 145.2(7) 1_565 . . 1_455 ? Li8 Li5 Li6 S5 52.4(6) 1_565 . . 2_667 ? Li8 Li5 Li6 S5 21.1(11) 2_667 . . 2_667 ? Li8 Li5 Li6 S6 -115.6(19) 1_565 . . . ? Li8 Li5 Li6 S6 -146.9(15) 2_667 . . . ? Li8 Li5 Li6 S7 -52.5(4) 1_565 . . . ? Li8 Li5 Li6 S7 -83.8(10) 2_667 . . . ? Li8 Li5 Li6 Si2 -71.1(10) 1_565 . . . ? Li8 Li5 Li6 Si2 -102.4(12) 2_667 . . . ? Li8 Li5 Li6 Li3 96.4(7) 1_565 . . 2_667 ? Li8 Li5 Li6 Li3 65.1(12) 2_667 . . 2_667 ? Li8 Li5 Li6 Li8 31.3(8) 1_565 . . 2_667 ? Li8 Li5 Li6 Li8 -31.3(8) 2_667 . . 1_565 ? Li8 Li5 Li6 Li10 24(6) 2_667 . . . ? Li8 Li5 Li6 Li10 55(5) 1_565 . . . ? Li8 Li5 Li6 Li13 -165(6) 2_667 . . . ? Li8 Li5 Li6 Li13 -134(5) 1_565 . . . ? Li8 Li5 Li13 I1 178(5) 1_565 . . 1_455 ? Li8 Li5 Li13 I1 -126(5) 2_667 . . 1_455 ? Li8 Li5 Li13 S6 -79(4) 1_565 . . 1_565 ? Li8 Li5 Li13 S6 -23(5) 2_667 . . 1_565 ? Li8 Li5 Li13 S7 27(4) 1_565 . . . ? Li8 Li5 Li13 S7 83(5) 2_667 . . . ? Li8 Li5 Li13 Li2 72(7) 2_667 . . . ? Li8 Li5 Li13 Li2 16(8) 1_565 . . . ? Li8 Li5 Li13 Li6 160(8) 2_667 . . . ? Li8 Li5 Li13 Li6 104(6) 1_565 . . . ? Li8 Li5 Li13 Li7 -146(3) 2_667 . . 2_666 ? Li8 Li5 Li13 Li7 157.7(18) 1_565 . . 2_666 ? Li8 Li5 Li13 Li8 56(4) 2_667 . . 1_565 ? Li8 Li5 Li13 Li8 -56(4) 1_565 . . 2_667 ? Li8 Li5 Li13 Li11 -24(9) 2_667 . . 2_676 ? Li8 Li5 Li13 Li11 -80(7) 1_565 . . 2_676 ? Li8 Li5 Li13 Li14 158(8) 2_667 . . . ? Li8 Li5 Li13 Li14 102(6) 1_565 . . . ? Li8 Li5 Li14 I1 113.2(19) 2_667 . . 1_455 ? Li8 Li5 Li14 I1 142.3(8) 1_565 . . 1_455 ? Li8 Li5 Li14 S5 52.0(10) 1_565 . . 2_667 ? Li8 Li5 Li14 S5 23(3) 2_667 . . 2_667 ? Li8 Li5 Li14 S6 -110(8) 1_565 . . . ? Li8 Li5 Li14 S6 -140(7) 2_667 . . . ? Li8 Li5 Li14 S7 -50.7(7) 1_565 . . . ? Li8 Li5 Li14 S7 -80(2) 2_667 . . . ? Li8 Li5 Li14 Si2 -63(3) 1_565 . . . ? Li8 Li5 Li14 Si2 -92(4) 2_667 . . . ? Li8 Li5 Li14 Li8 -29.1(17) 2_667 . . 1_565 ? Li8 Li5 Li14 Li8 29.1(17) 1_565 . . 2_667 ? Li8 Li5 Li14 Li10 54(7) 1_565 . . . ? Li8 Li5 Li14 Li10 25(8) 2_667 . . . ? Li8 Li5 Li14 Li13 -163(6) 2_667 . . . ? Li8 Li5 Li14 Li13 -134(5) 1_565 . . . ? Li8 Li6 Li13 I1 -138.0(6) 1_565 . . 1_455 ? Li8 Li6 Li13 I1 -106.7(5) 2_667 . . 1_455 ? Li8 Li6 Li13 S1 164.3(14) 2_667 . . 2_666 ? Li8 Li6 Li13 S1 133.1(12) 1_565 . . 2_666 ? Li8 Li6 Li13 S6 -46.6(15) 1_565 . . 1_565 ? Li8 Li6 Li13 S6 -15.3(12) 2_667 . . 1_565 ? Li8 Li6 Li13 S7 48.3(4) 1_565 . . . ? Li8 Li6 Li13 S7 79.6(5) 2_667 . . . ? Li8 Li6 Li13 Li2 78.4(9) 1_565 . . . ? Li8 Li6 Li13 Li2 109.7(10) 2_667 . . . ? Li8 Li6 Li13 Li5 -12(5) 2_667 . . . ? Li8 Li6 Li13 Li5 -43(5) 1_565 . . . ? Li8 Li6 Li13 Li7 -154.9(8) 2_667 . . 2_666 ? Li8 Li6 Li13 Li7 173.8(7) 1_565 . . 2_666 ? Li8 Li6 Li13 Li8 -31.3(5) 1_565 . . 2_667 ? Li8 Li6 Li13 Li8 31.3(5) 2_667 . . 1_565 ? Li8 Li6 Li13 Li14 80(100) 2_667 . . . ? Li8 Li6 Li13 Li14 49(100) 1_565 . . . ? Li8 Li13 Li14 I1 137.6(12) 1_565 . . 1_455 ? Li8 Li13 Li14 I1 106.6(7) 2_667 . . 1_455 ? Li8 Li13 Li14 S5 51.2(17) 1_565 . . 2_667 ? Li8 Li13 Li14 S5 20.1(18) 2_667 . . 2_667 ? Li8 Li13 Li14 S6 -124(3) 1_565 . . . ? Li8 Li13 Li14 S6 -155(2) 2_667 . . . ? Li8 Li13 Li14 S7 -48.7(7) 1_565 . . . ? Li8 Li13 Li14 S7 -79.7(7) 2_667 . . . ? Li8 Li13 Li14 Si2 -79.5(15) 1_565 . . . ? Li8 Li13 Li14 Si2 -110.5(16) 2_667 . . . ? Li8 Li13 Li14 Li5 44(5) 1_565 . . . ? Li8 Li13 Li14 Li5 13(5) 2_667 . . . ? Li8 Li13 Li14 Li8 -31.0(8) 2_667 . . 1_565 ? Li8 Li13 Li14 Li8 31.0(8) 1_565 . . 2_667 ? Li9 Li4 Li12 S1 -61.9(8) 2_756 . . . ? Li9 Li4 Li12 S1 -61.9(8) . . . 2_756 ? Li9 Li4 Li12 S1 118.1(8) . . . . ? Li9 Li4 Li12 S1 118.1(8) 2_756 . . 2_756 ? Li9 Li4 Li12 S2 45.6(4) 2_756 . . 2_756 ? Li9 Li4 Li12 S2 45.6(4) . . . . ? Li9 Li4 Li12 S2 -134.4(4) . . . 2_756 ? Li9 Li4 Li12 S2 -134.4(4) 2_756 . . . ? Li9 Li4 Li12 S3 -39.9(7) . . . 2_766 ? Li9 Li4 Li12 S3 140.1(7) . . . 1_545 ? Li9 Li4 Li12 S3 -39.9(7) 2_756 . . 1_545 ? Li9 Li4 Li12 S3 140.1(7) 2_756 . . 2_766 ? Li9 Li4 Li12 Li7 94(14) . . . . ? Li9 Li4 Li12 Li7 -86(14) 2_756 . . . ? Li9 Li4 Li12 Li11 -15.1(3) 2_756 . . 1_545 ? Li9 Li4 Li12 Li11 -15.1(3) . . . 2_766 ? Li9 Li4 Li12 Li11 164.9(3) 2_756 . . 2_766 ? Li9 Li4 Li12 Li11 164.9(3) . . . 1_545 ? Li10 Li5 Li6 I1 90(5) . . . 1_455 ? Li10 Li5 Li6 S5 -3(4) . . . 2_667 ? Li10 Li5 Li6 S6 -171(7) . . . . ? Li10 Li5 Li6 S7 -108(5) . . . . ? Li10 Li5 Li6 Si2 -126(5) . . . . ? Li10 Li5 Li6 Li3 41(4) . . . 2_667 ? Li10 Li5 Li6 Li8 -55(5) . . . 1_565 ? Li10 Li5 Li6 Li8 -24(6) . . . 2_667 ? Li10 Li5 Li6 Li13 171(4) . . . . ? Li10 Li5 Li13 I1 72(3) . . . 1_455 ? Li10 Li5 Li13 S6 175(3) . . . 1_565 ? Li10 Li5 Li13 S7 -79(3) . . . . ? Li10 Li5 Li13 Li2 -90(5) . . . . ? Li10 Li5 Li13 Li6 -2.4(11) . . . . ? Li10 Li5 Li13 Li7 52(7) . . . 2_666 ? Li10 Li5 Li13 Li8 -162(8) . . . 2_667 ? Li10 Li5 Li13 Li8 -106(6) . . . 1_565 ? Li10 Li5 Li13 Li11 173.5(15) . . . 2_676 ? Li10 Li5 Li13 Li14 -4(2) . . . . ? Li10 Li5 Li14 I1 88(6) . . . 1_455 ? Li10 Li5 Li14 S5 -2(6) . . . 2_667 ? Li10 Li5 Li14 S6 -165(15) . . . . ? Li10 Li5 Li14 S7 -105(7) . . . . ? Li10 Li5 Li14 Si2 -117(8) . . . . ? Li10 Li5 Li14 Li8 -25(8) . . . 2_667 ? Li10 Li5 Li14 Li8 -54(7) . . . 1_565 ? Li10 Li5 Li14 Li13 172(5) . . . . ? Li11 Li4 Li12 S1 133.2(7) 1_545 . . 2_756 ? Li11 Li4 Li12 S1 133.2(7) 2_766 . . . ? Li11 Li4 Li12 S1 -46.8(7) 2_766 . . 2_756 ? Li11 Li4 Li12 S1 -46.8(7) 1_545 . . . ? Li11 Li4 Li12 S2 -119.4(3) 2_766 . . 2_756 ? Li11 Li4 Li12 S2 60.6(3) 1_545 . . 2_756 ? Li11 Li4 Li12 S2 -119.4(3) 1_545 . . . ? Li11 Li4 Li12 S2 60.6(3) 2_766 . . . ? Li11 Li4 Li12 S3 -24.8(9) 2_766 . . 2_766 ? Li11 Li4 Li12 S3 155.2(9) 2_766 . . 1_545 ? Li11 Li4 Li12 S3 -24.8(9) 1_545 . . 1_545 ? Li11 Li4 Li12 S3 155.2(9) 1_545 . . 2_766 ? Li11 Li4 Li12 Li7 -71(14) 1_545 . . . ? Li11 Li4 Li12 Li7 109(14) 2_766 . . . ? Li11 Li4 Li12 Li11 180.000(0) 2_766 . . 1_545 ? Li11 Li4 Li12 Li11 180.000(1) 1_545 . . 2_766 ? Li11 Li5 Li6 I1 -75(3) 2_676 . . 1_455 ? Li11 Li5 Li6 S5 -168(3) 2_676 . . 2_667 ? Li11 Li5 Li6 S6 24(5) 2_676 . . . ? Li11 Li5 Li6 S7 87(3) 2_676 . . . ? Li11 Li5 Li6 Si2 69(3) 2_676 . . . ? Li11 Li5 Li6 Li3 -124(3) 2_676 . . 2_667 ? Li11 Li5 Li6 Li8 140(3) 2_676 . . 1_565 ? Li11 Li5 Li6 Li8 171(4) 2_676 . . 2_667 ? Li11 Li5 Li6 Li10 -165(3) 2_676 . . . ? Li11 Li5 Li6 Li13 5(3) 2_676 . . . ? Li11 Li5 Li13 I1 -102(4) 2_676 . . 1_455 ? Li11 Li5 Li13 S6 2(5) 2_676 . . 1_565 ? Li11 Li5 Li13 S7 108(4) 2_676 . . . ? Li11 Li5 Li13 Li2 97(6) 2_676 . . . ? Li11 Li5 Li13 Li6 -176(2) 2_676 . . . ? Li11 Li5 Li13 Li7 -122(7) 2_676 . . 2_666 ? Li11 Li5 Li13 Li8 24(9) 2_676 . . 2_667 ? Li11 Li5 Li13 Li8 80(7) 2_676 . . 1_565 ? Li11 Li5 Li13 Li14 -177(3) 2_676 . . . ? Li11 Li5 Li14 I1 -81(4) 2_676 . . 1_455 ? Li11 Li5 Li14 S5 -171(3) 2_676 . . 2_667 ? Li11 Li5 Li14 S6 26(12) 2_676 . . . ? Li11 Li5 Li14 S7 86(4) 2_676 . . . ? Li11 Li5 Li14 Si2 74(6) 2_676 . . . ? Li11 Li5 Li14 Li8 137(4) 2_676 . . 1_565 ? Li11 Li5 Li14 Li8 166(6) 2_676 . . 2_667 ? Li11 Li5 Li14 Li10 -169(3) 2_676 . . . ? Li11 Li5 Li14 Li13 3(3) 2_676 . . . ? Li13 Li5 Li6 I1 -81(5) . . . 1_455 ? Li13 Li5 Li6 S5 -173(5) . . . 2_667 ? Li13 Li5 Li6 S6 19(6) . . . . ? Li13 Li5 Li6 S7 82(5) . . . . ? Li13 Li5 Li6 Si2 63(5) . . . . ? Li13 Li5 Li6 Li3 -129(5) . . . 2_667 ? Li13 Li5 Li6 Li8 165(6) . . . 2_667 ? Li13 Li5 Li6 Li8 134(5) . . . 1_565 ? Li13 Li5 Li6 Li10 -171(4) . . . . ? Li13 Li5 Li14 I1 -84(5) . . . 1_455 ? Li13 Li5 Li14 S5 -174(4) . . . 2_667 ? Li13 Li5 Li14 S6 24(11) . . . . ? Li13 Li5 Li14 S7 83(5) . . . . ? Li13 Li5 Li14 Si2 71(6) . . . . ? Li13 Li5 Li14 Li8 134(5) . . . 1_565 ? Li13 Li5 Li14 Li8 163(6) . . . 2_667 ? Li13 Li5 Li14 Li10 -172(5) . . . . ? Li14 Li5 Li6 I1 -89(16) . . . 1_455 ? Li14 Li5 Li6 S5 179(16) . . . 2_667 ? Li14 Li5 Li6 S6 11(15) . . . . ? Li14 Li5 Li6 S7 74(16) . . . . ? Li14 Li5 Li6 Si2 55(15) . . . . ? Li14 Li5 Li6 Li3 -137(16) . . . 2_667 ? Li14 Li5 Li6 Li8 157(16) . . . 2_667 ? Li14 Li5 Li6 Li8 126(16) . . . 1_565 ? Li14 Li5 Li6 Li10 -179(18) . . . . ? Li14 Li5 Li6 Li13 -8(15) . . . . ? Li14 Li5 Li13 I1 76(4) . . . 1_455 ? Li14 Li5 Li13 S6 179(4) . . . 1_565 ? Li14 Li5 Li13 S7 -75(4) . . . . ? Li14 Li5 Li13 Li2 -86(5) . . . . ? Li14 Li5 Li13 Li6 1(3) . . . . ? Li14 Li5 Li13 Li7 55(6) . . . 2_666 ? Li14 Li5 Li13 Li8 -158(8) . . . 2_667 ? Li14 Li5 Li13 Li8 -102(6) . . . 1_565 ? Li14 Li5 Li13 Li11 177(3) . . . 2_676 ?