#------------------------------------------------------------------------------
#$Date: 2026-07-09 10:10:54 +0100 (Thu, 09 Jul 2026) $
#$Revision: 306694 $
#$URL: svn://www.crystallography.net/cod/hkl/1/57/74/1577466.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_1577466
_space_group_crystal_system      monoclinic
_space_group_IT_number           4
_space_group_name_Hall           ' P 2yb'
_space_group_name_H-M_alt        'P 1 21 1'
_symmetry_Int_Tables_number      4
_symmetry_space_group_name_Hall  ' P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90
_cell_angle_beta                 100.442(2)
_cell_angle_gamma                90
_cell_length_a                   5.1237(2)
_cell_length_b                   6.9197(3)
_cell_length_c                   7.6006(4)
_cell_volume                     265.013(19)
_computing_structure_refinement  'olex2.refine 1.5 (Bourhis et al., 2015)'
_cod_data_source_file            ii4003Ibsup3.hkl
_cod_data_source_block           Ib
_shelx_refln_list_code           4
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 -x,y+1/2,-z
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_f_squared_weight
_refln_observed_status
-7 -1 0 32.522 35.860 1.446 2.366 o
-7 0 1 17.314 14.701 1.519 5.353 o
-7 0 2 0.080 0.138 0.706 57.303 o
-7 0 3 35.744 28.883 1.729 1.976 o
-7 0 4 1.568 1.596 0.998 26.735 o
-7 1 1 3.036 3.468 1.142 19.187 o
-7 1 2 3.464 4.407 0.869 28.979 o
-7 1 3 0.399 1.051 0.937 32.088 o
-7 1 4 5.896 5.472 1.146 15.796 o
-7 2 1 15.961 15.095 1.195 6.995 o
-7 2 2 18.012 19.024 1.285 5.719 o
-7 2 3 72.088 76.109 2.645 0.545 o
-6 -5 0 4.990 5.883 0.870 24.810 o
-6 -4 -2 2.814 2.798 0.754 38.810 o
-6 -4 -1 41.678 45.497 1.465 1.580 o
-6 -4 0 1.306 0.878 0.616 65.197 o
-6 -3 -3 8.701 9.147 0.934 15.703 o
-6 -3 -2 20.108 22.075 1.110 5.353 o
-6 -3 -1 4.496 5.907 0.757 31.216 o
-6 -3 0 16.081 18.447 0.981 7.666 o
-6 -2 -3 39.973 41.345 1.463 1.706 o
-6 -2 -2 19.215 19.308 1.030 5.954 o
-6 -2 -1 3.789 3.966 0.660 41.106 o
-6 -2 0 15.985 15.853 0.998 7.766 o
-6 -1 -4 1.453 2.244 0.844 36.496 o
-6 -1 -3 2.064 1.284 0.718 46.011 o
-6 -1 -2 15.037 14.376 1.005 8.386 o
-6 -1 -1 5.022 5.806 0.753 29.591 o
-6 -1 0 13.311 14.320 0.895 10.333 o
-6 0 1 9.642 9.099 0.597 19.419 o
-6 0 2 3.473 3.392 0.513 58.113 o
-6 0 3 4.757 4.856 0.571 41.433 o
-6 0 4 24.903 24.337 0.994 4.099 o
-6 0 5 11.674 11.386 0.837 12.713 o
-6 0 6 38.116 42.296 1.462 1.829 o
-6 0 7 3.529 3.748 0.796 32.967 o
-6 1 1 41.885 37.896 1.354 1.630 o
-6 1 2 16.437 14.393 1.118 7.094 o
-6 1 3 54.779 48.853 1.879 0.962 o
-6 1 4 2.705 1.619 0.766 38.667 o
-6 1 5 13.485 12.679 1.214 8.294 o
-6 1 6 9.171 8.502 0.768 17.726 o
-6 1 7 0.580 0.608 0.637 66.686 o
-6 2 1 13.114 13.671 0.809 11.158 o
-6 2 2 21.782 19.947 1.294 4.526 o
-6 2 3 7.126 4.848 0.893 19.670 o
-6 2 4 2.986 2.479 0.842 32.226 o
-6 2 5 8.335 7.261 1.046 14.604 o
-6 2 6 7.562 6.916 1.107 14.548 o
-6 2 7 11.961 11.552 1.350 8.338 o
-6 3 1 6.508 6.675 0.714 25.941 o
-6 3 2 48.094 46.840 1.889 1.182 o
-6 3 3 14.620 13.594 1.195 7.727 o
-6 3 4 3.897 2.833 0.886 27.355 o
-6 3 5 6.370 5.336 1.005 18.242 o
-6 3 6 6.516 7.019 1.151 14.926 o
-6 4 1 0.002 0.178 0.574 87.013 o
-6 4 2 4.514 4.687 0.982 22.036 o
-6 4 3 9.718 9.552 1.152 11.635 o
-6 4 4 59.435 62.311 2.288 0.783 o
-6 4 5 6.583 8.967 1.181 14.194 o
-6 5 1 14.063 11.818 1.101 8.632 o
-6 5 2 12.638 14.364 1.192 8.860 o
-6 5 3 3.770 3.414 1.010 22.512 o
-5 -6 -2 16.393 19.384 1.766 4.779 o
-5 -6 -1 27.768 23.506 1.774 2.766 o
-5 -6 0 3.886 2.432 0.806 31.562 o
-5 -5 -3 27.601 30.560 1.509 2.967 o
-5 -5 -2 23.067 20.920 1.259 4.245 o
-5 -5 -1 14.248 13.864 0.861 9.763 o
-5 -5 0 8.271 6.158 0.673 22.040 o
-5 -4 -4 8.508 9.361 1.072 13.834 o
-5 -4 -3 4.549 5.892 0.892 25.020 o
-5 -4 -2 2.592 2.360 0.578 59.049 o
-5 -4 -1 3.754 5.148 0.624 43.728 o
-5 -4 0 4.453 5.251 0.603 40.909 o
-5 -3 -5 1.841 2.821 0.944 28.931 o
-5 -3 -4 4.444 5.028 0.880 25.874 o
-5 -3 -3 14.951 16.223 0.913 8.803 o
-5 -3 -2 38.781 38.314 1.203 1.884 o
-5 -3 -1 92.158 87.352 1.765 0.379 o
-5 -3 0 39.389 34.776 0.902 1.937 o
-5 -2 -5 0.632 0.713 0.755 48.089 o
-5 -2 -4 12.233 12.542 1.027 10.435 o
-5 -2 -3 9.381 9.016 0.731 17.860 o
-5 -2 -2 17.604 16.166 0.828 7.428 o
-5 -2 -1 87.999 87.310 1.952 0.407 o
-5 -2 0 7.032 5.437 0.490 32.013 o
-5 -1 -6 0.961 0.422 0.850 37.612 o
-5 -1 -5 15.675 16.337 1.178 7.155 o
-5 -1 -4 1.236 1.456 0.651 59.348 o
-5 -1 -3 12.546 11.543 0.758 12.341 o
-5 -1 -2 74.172 71.290 1.761 0.565 o
-5 -1 -1 27.862 23.997 0.781 3.632 o
-5 -1 0 43.404 39.208 0.988 1.607 o
-5 0 1 227.749 227.879 3.495 0.064 o
-5 0 2 4.113 4.720 0.465 55.617 o
-5 0 3 38.284 38.206 1.094 1.957 o
-5 0 4 21.627 20.899 0.874 5.313 o
-5 0 5 35.975 33.425 1.144 2.178 o
-5 0 6 0.727 0.988 0.523 93.906 o
-5 0 7 1.369 1.897 0.619 63.540 o
-5 0 8 40.205 37.830 1.453 1.711 o
-5 1 1 85.518 77.073 1.636 0.441 o
-5 1 2 32.312 26.618 1.230 2.591 o
-5 1 3 80.820 75.280 2.110 0.474 o
-5 1 4 22.140 18.335 0.754 5.391 o
-5 1 5 9.348 7.099 0.617 20.179 o
-5 1 6 14.052 10.762 0.775 10.661 o
-5 1 7 20.885 18.878 1.009 5.379 o
-5 1 8 157.605 168.068 3.171 0.130 o
-5 2 1 12.374 11.788 0.733 12.734 o
-5 2 2 95.026 90.420 2.309 0.348 o
-5 2 3 43.430 39.775 1.498 1.497 o
-5 2 4 30.039 29.009 1.338 2.789 o
-5 2 5 35.009 33.853 1.476 2.125 o
-5 2 6 4.989 4.187 0.578 39.841 o
-5 2 7 58.862 60.510 1.606 0.861 o
-5 2 8 6.604 5.362 0.779 23.860 o
-5 3 1 62.195 54.554 1.483 0.804 o
-5 3 2 7.985 6.335 0.656 23.190 o
-5 3 3 46.359 41.181 1.590 1.327 o
-5 3 4 8.270 7.437 0.870 17.705 o
-5 3 5 16.814 16.028 1.139 6.777 o
-5 3 6 12.808 12.623 1.098 9.463 o
-5 3 7 14.238 13.187 0.838 9.947 o
-5 3 8 10.498 10.202 1.064 11.812 o
-5 4 1 17.882 20.477 1.011 6.547 o
-5 4 2 52.555 53.413 1.550 1.059 o
-5 4 3 11.361 10.626 0.977 11.800 o
-5 4 4 15.498 16.574 1.145 7.376 o
-5 4 5 9.522 7.524 0.911 15.050 o
-5 4 6 19.110 17.173 2.033 3.680 o
-5 4 7 29.688 29.599 2.573 1.918 o
-5 5 1 34.406 35.427 1.386 2.212 o
-5 5 2 27.608 28.761 1.579 2.921 o
-5 5 3 36.167 37.468 1.643 1.932 o
-5 5 4 13.352 11.966 1.100 9.099 o
-5 5 5 7.977 7.973 1.644 8.145 o
-5 5 6 10.678 11.958 1.931 5.649 o
-5 6 1 8.729 7.948 0.921 15.995 o
-5 6 2 0.926 1.171 0.916 32.575 o
-5 6 3 6.331 6.200 1.565 9.530 o
-5 6 4 29.438 27.917 2.466 2.016 o
-5 6 5 7.018 6.749 1.733 7.827 o
-5 7 1 45.114 46.293 2.256 1.219 o
-4 -8 0 36.707 37.085 2.283 1.625 o
-4 -7 -3 21.172 22.565 1.858 3.604 o
-4 -7 -2 44.811 46.581 2.358 1.205 o
-4 -7 -1 11.101 12.298 1.398 8.436 o
-4 -7 0 11.765 10.868 1.064 10.634 o
-4 -6 -4 17.515 17.936 1.692 4.744 o
-4 -6 -3 43.044 47.474 2.318 1.280 o
-4 -6 -2 8.822 7.593 1.188 12.126 o
-4 -6 -1 12.499 14.177 1.317 8.160 o
-4 -6 0 10.041 9.667 0.735 16.467 o
-4 -5 -5 10.323 9.739 0.933 13.496 o
-4 -5 -4 16.201 16.068 0.973 7.735 o
-4 -5 -3 30.224 26.488 1.279 2.832 o
-4 -5 -2 52.197 58.839 1.708 1.038 o
-4 -5 -1 114.293 120.375 2.067 0.246 o
-4 -5 0 27.009 27.770 0.921 3.641 o
-4 -4 -6 8.466 7.512 0.920 16.471 o
-4 -4 -5 3.635 3.799 0.701 38.866 o
-4 -4 -4 2.279 2.074 0.579 62.026 o
-4 -4 -3 4.223 3.138 0.465 55.759 o
-4 -4 -2 10.377 11.771 0.588 17.463 o
-4 -4 -1 85.565 84.301 1.372 0.441 o
-4 -4 0 48.295 47.689 0.984 1.311 o
-4 -3 -7 6.361 6.035 0.929 20.044 o
-4 -3 -6 6.085 6.739 0.272 46.633 o
-4 -3 -5 18.859 19.185 0.733 6.868 o
-4 -3 -4 80.124 68.869 1.651 0.500 o
-4 -3 -3 93.214 95.079 1.604 0.370 o
-4 -3 -2 86.538 93.631 1.523 0.424 o
-4 -3 -1 98.028 101.008 1.362 0.339 o
-4 -3 0 53.020 47.028 0.943 1.122 o
-4 -2 -7 8.218 9.035 0.566 23.980 o
-4 -2 -6 11.155 9.376 0.863 13.281 o
-4 -2 -5 0.356 0.389 0.020 1900.700 o
-4 -2 -4 6.340 5.100 0.597 31.385 o
-4 -2 -3 9.086 7.242 0.506 22.882 o
-4 -2 -2 7.064 5.858 0.439 33.464 o
-4 -2 -1 76.453 72.803 1.283 0.550 o
-4 -2 0 64.324 62.165 1.182 0.763 o
-4 -1 -7 15.732 14.173 1.069 7.682 o
-4 -1 -6 32.126 30.098 1.253 2.569 o
-4 -1 -5 2.758 1.544 0.524 66.085 o
-4 -1 -4 51.182 46.841 1.089 1.179 o
-4 -1 -3 5.818 4.444 0.366 46.279 o
-4 -1 -2 494.012 501.044 5.358 0.014 o
-4 -1 -1 133.542 129.705 1.661 0.187 o
-4 -1 0 90.962 87.316 1.453 0.393 o
-4 0 1 0.724 1.881 0.228 326.171 o
-4 0 2 9.748 9.332 0.343 22.740 o
-4 0 3 52.222 49.717 0.824 1.154 o
-4 0 4 2.656 2.326 0.073 176.542 o
-4 0 5 523.653 514.028 11.793 0.012 o
-4 0 6 7.147 6.517 0.616 27.002 o
-4 0 7 78.267 77.597 2.110 0.498 o
-4 0 8 80.459 77.778 2.745 0.453 o
-4 0 9 48.489 50.953 1.988 1.138 o
-4 1 1 23.393 23.759 0.664 4.923 o
-4 1 2 15.992 16.338 0.671 9.074 o
-4 1 3 56.449 58.091 0.988 0.978 o
-4 1 4 47.075 46.125 1.119 1.356 o
-4 1 5 147.269 151.804 4.032 0.143 o
-4 1 6 5.782 4.692 0.211 54.253 o
-4 1 7 30.338 30.006 1.571 2.574 o
-4 1 8 58.168 53.528 1.975 0.856 o
-4 1 9 18.834 19.174 1.200 5.659 o
-4 2 1 112.912 111.097 1.735 0.257 o
-4 2 2 33.478 33.744 0.863 2.558 o
-4 2 3 92.907 93.970 1.834 0.369 o
-4 2 4 230.539 231.226 2.982 0.063 o
-4 2 5 82.375 80.085 1.614 0.469 o
-4 2 6 31.253 27.264 0.964 2.878 o
-4 2 7 40.237 39.605 1.894 1.564 o
-4 2 8 21.898 19.609 1.240 4.601 o
-4 2 9 32.876 37.316 1.909 2.061 o
-4 3 1 26.915 26.045 0.811 3.780 o
-4 3 2 1.290 1.319 0.356 151.433 o
-4 3 3 100.841 99.477 1.966 0.316 o
-4 3 4 5.013 4.832 0.618 36.952 o
-4 3 5 23.312 24.372 0.812 4.758 o
-4 3 6 50.502 49.492 1.263 1.178 o
-4 3 7 67.611 68.745 2.375 0.627 o
-4 3 8 74.990 72.826 2.733 0.510 o
-4 3 9 10.976 10.814 1.166 10.400 o
-4 4 1 14.464 16.847 0.738 10.049 o
-4 4 2 39.049 35.025 0.985 1.943 o
-4 4 3 25.586 21.716 0.934 4.047 o
-4 4 4 110.166 107.749 2.509 0.262 o
-4 4 5 31.797 27.462 0.856 2.852 o
-4 4 6 20.310 20.734 1.013 5.529 o
-4 4 7 25.312 25.224 1.302 3.630 o
-4 4 8 11.775 11.907 1.132 10.013 o
-4 5 1 18.909 17.010 0.971 6.313 o
-4 5 2 26.775 21.368 1.058 3.662 o
-4 5 3 39.073 38.514 1.113 1.886 o
-4 5 4 32.688 33.780 1.345 2.421 o
-4 5 5 55.430 57.356 2.893 0.802 o
-4 5 6 24.446 23.045 1.105 4.096 o
-4 5 7 10.154 9.125 0.933 13.752 o
-4 6 1 7.272 6.801 0.832 20.564 o
-4 6 2 16.106 16.820 1.083 7.310 o
-4 6 3 15.730 15.054 1.062 7.675 o
-4 6 4 6.218 5.196 1.309 12.738 o
-4 6 5 37.105 36.976 2.597 1.477 o
-4 6 6 37.942 38.048 1.473 1.862 o
-4 7 1 36.687 42.068 1.678 1.854 o
-4 7 2 33.845 36.277 1.586 2.160 o
-4 7 3 5.967 6.037 1.112 16.369 o
-4 7 4 26.629 25.977 2.402 2.284 o
-4 7 5 16.307 14.739 2.038 4.152 o
-4 8 1 7.634 8.358 1.325 11.346 o
-4 8 2 21.513 21.305 1.745 3.753 o
-3 -8 -3 12.883 14.407 1.687 6.082 o
-3 -8 -2 12.587 15.875 1.604 6.518 o
-3 -8 -1 33.123 33.550 1.612 2.230 o
-3 -8 0 4.382 4.165 0.873 26.487 o
-3 -7 -5 9.176 7.719 1.137 12.416 o
-3 -7 -4 9.565 9.475 1.095 12.429 o
-3 -7 -3 13.013 12.632 1.085 9.401 o
-3 -7 -2 21.753 21.549 1.598 3.958 o
-3 -7 -1 28.916 32.658 1.731 2.590 o
-3 -7 0 25.339 28.107 1.134 3.776 o
-3 -6 -6 41.235 41.072 1.529 1.609 o
-3 -6 -5 2.801 1.729 0.657 48.139 o
-3 -6 -4 5.677 5.604 0.708 29.291 o
-3 -6 -3 2.802 3.962 0.578 56.068 o
-3 -6 -2 56.493 62.861 1.747 0.903 o
-3 -6 -1 5.400 4.396 0.617 35.173 o
-3 -6 0 36.628 35.562 1.051 2.134 o
-3 -5 -7 21.720 21.593 1.265 4.563 o
-3 -5 -6 9.116 9.685 0.914 15.347 o
-3 -5 -5 51.200 51.157 1.500 1.117 o
-3 -5 -4 66.544 65.629 1.584 0.695 o
-3 -5 -3 19.938 21.068 0.883 5.948 o
-3 -5 -2 6.188 6.132 0.430 39.132 o
-3 -5 -1 136.708 132.700 1.850 0.178 o
-3 -5 0 54.288 55.014 0.984 1.053 o
-3 -4 -7 13.520 12.364 1.032 9.393 o
-3 -4 -6 22.430 21.500 1.084 4.684 o
-3 -4 -5 3.300 2.660 0.571 53.457 o
-3 -4 -4 33.942 31.834 1.051 2.442 o
-3 -4 -3 122.029 124.580 1.826 0.220 o
-3 -4 -2 3.554 2.832 0.334 83.148 o
-3 -4 -1 50.988 55.747 1.001 1.169 o
-3 -4 0 65.849 64.142 1.054 0.735 o
-3 -3 -8 9.467 10.423 1.042 13.090 o
-3 -3 -7 57.177 55.343 1.689 0.905 o
-3 -3 -6 27.779 25.407 1.108 3.365 o
-3 -3 -5 21.604 26.670 1.019 4.927 o
-3 -3 -4 31.039 27.953 0.959 2.904 o
-3 -3 -3 20.722 19.258 0.629 6.150 o
-3 -3 -2 96.781 99.714 1.287 0.348 o
-3 -3 -1 30.958 29.869 0.662 3.043 o
-3 -3 0 40.032 42.298 0.845 1.853 o
-3 -2 -8 4.663 4.351 0.856 26.467 o
-3 -2 -7 15.272 11.739 0.915 8.807 o
-3 -2 -6 0.101 0.251 0.490 117.693 o
-3 -2 -5 74.341 77.522 1.705 0.559 o
-3 -2 -4 51.939 49.764 1.037 1.146 o
-3 -2 -3 0.510 1.279 0.236 359.678 o
-3 -2 -2 160.417 172.483 1.637 0.129 o
-3 -2 -1 63.185 68.789 0.852 0.791 o
-3 -2 0 158.396 179.797 2.130 0.130 o
-3 -1 -8 17.640 19.072 1.008 6.720 o
-3 -1 -7 4.447 3.909 0.600 41.807 o
-3 -1 -6 26.156 22.190 0.843 3.994 o
-3 -1 -5 179.716 167.222 2.397 0.104 o
-3 -1 -4 65.161 58.386 1.129 0.754 o
-3 -1 -3 0.893 0.895 0.214 332.501 o
-3 -1 -2 101.180 104.117 1.085 0.321 o
-3 -1 -1 14.546 15.301 0.305 11.976 o
-3 -1 0 39.632 47.151 0.602 1.899 o
-3 0 1 0.489 1.471 0.150 619.006 o
-3 0 2 871.446 963.151 9.198 0.004 o
-3 0 3 14.126 13.735 0.375 12.437 o
-3 0 4 211.116 215.093 2.324 0.076 o
-3 0 5 35.502 35.725 0.753 2.341 o
-3 0 6 46.787 36.500 0.812 1.448 o
-3 0 7 1.381 1.074 0.321 168.795 o
-3 0 8 3.725 2.855 0.493 58.295 o
-3 0 9 0.025 0.063 0.489 119.546 o
-3 0 10 102.907 102.189 2.432 0.297 o
-3 1 1 23.465 29.397 0.533 4.891 o
-3 1 2 0.768 0.744 0.136 548.041 o
-3 1 3 158.092 161.757 1.939 0.133 o
-3 1 4 10.974 9.538 0.306 19.429 o
-3 1 5 256.020 251.527 2.950 0.052 o
-3 1 6 4.220 2.716 0.320 72.129 o
-3 1 7 6.708 6.954 0.508 32.439 o
-3 1 8 10.161 10.870 0.663 17.059 o
-3 1 9 4.725 5.559 0.745 31.074 o
-3 1 10 7.716 8.692 1.197 12.908 o
-3 2 1 210.705 235.049 3.006 0.074 o
-3 2 2 80.184 86.429 1.378 0.493 o
-3 2 3 25.107 22.168 0.460 4.596 o
-3 2 4 104.391 105.509 1.413 0.301 o
-3 2 5 182.883 174.761 2.456 0.101 o
-3 2 6 21.627 20.063 0.699 5.623 o
-3 2 7 7.192 5.403 0.556 29.080 o
-3 2 8 45.624 48.199 1.355 1.381 o
-3 2 9 66.241 67.568 2.274 0.656 o
-3 2 10 46.773 43.326 2.005 1.219 o
-3 3 1 75.601 79.677 1.357 0.553 o
-3 3 2 1.481 1.394 0.199 252.469 o
-3 3 3 93.417 99.405 1.304 0.371 o
-3 3 4 348.538 349.768 3.891 0.028 o
-3 3 5 70.068 69.734 1.259 0.645 o
-3 3 6 21.535 22.362 0.748 5.516 o
-3 3 7 18.233 18.224 0.954 6.630 o
-3 3 8 17.384 17.576 1.171 6.361 o
-3 3 9 9.589 7.224 1.001 13.748 o
-3 4 1 35.035 31.920 1.059 2.317 o
-3 4 2 205.978 203.183 2.433 0.080 o
-3 4 3 49.320 49.075 0.691 1.288 o
-3 4 4 47.718 49.421 0.865 1.346 o
-3 4 5 42.034 38.520 0.826 1.730 o
-3 4 6 55.047 50.576 1.424 1.001 o
-3 4 7 52.385 50.025 1.517 1.077 o
-3 4 8 1.175 1.709 0.742 47.183 o
-3 4 9 64.841 67.624 2.367 0.671 o
-3 5 1 4.691 4.481 0.575 41.732 o
-3 5 2 26.679 27.443 1.059 3.590 o
-3 5 3 12.053 9.683 0.507 15.360 o
-3 5 4 26.908 28.278 0.812 3.744 o
-3 5 5 10.482 9.989 0.581 17.611 o
-3 5 6 37.710 38.812 1.124 1.992 o
-3 5 7 8.558 8.155 0.698 20.389 o
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