#------------------------------------------------------------------------------ #$Date: 2026-08-18 15:37:54 +0100 (Tue, 18 Aug 2026) $ #$Revision: 306722 $ #$URL: svn://www.crystallography.net/cod/cif/1/57/74/1577471.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1577471 loop_ _publ_author_name 'Nasipuri, Diptam' 'Karmakar, Sougata' 'Sarkar, Akram Hossain' 'Goyal, Naveen' 'Banerjee, Souvik' 'Das, Rajdeep' 'Ravishankar, N.' 'Rao, K. D. M.' 'Pradhan, Narayan' _publ_section_title ; Facet‐Engineered Rubidium Lead Halide Nanocrystals for Pyro‐Phototronic Broadband Photodetection ; _journal_issue 7 _journal_name_full 'Advanced Materials' _journal_page_first e10226 _journal_paper_doi 10.1002/adma.202510226 _journal_volume 38 _journal_year 2025 _chemical_formula_moiety 'Cl5 Pb2 Rb' _chemical_formula_sum 'Cl5 Pb2 Rb' _chemical_formula_weight 677.10 _chemical_name_systematic RbPb2Cl5 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens . _atom_sites_solution_primary dual _audit_creation_date 2024-09-16 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _audit_update_record ; 2024-09-24 deposited with the CCDC. 2025-05-18 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90.10(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.052(6) _cell_length_b 8.032(4) _cell_length_c 12.592(6) _cell_measurement_reflns_used 4316 _cell_measurement_temperature 171.33 _cell_measurement_theta_max 33.51 _cell_measurement_theta_min 3.01 _cell_volume 915.5(9) _computing_cell_refinement 'SAINT V8.38A (Bruker, 2018)' _computing_data_reduction 'SAINT V8.38A (Bruker, 2018)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 171.33 _diffrn_detector 'Bruker APEX2 area detector' _diffrn_detector_area_resol_mean 7.9 _diffrn_detector_type 'CCD area detector' _diffrn_measured_fraction_theta_full 0.992 _diffrn_measured_fraction_theta_max 0.872 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker SMART APEX2 area detector' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_monochromator 'mirror optics' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0749 _diffrn_reflns_av_unetI/netI 0.0744 _diffrn_reflns_Laue_measured_fraction_full 0.992 _diffrn_reflns_Laue_measured_fraction_max 0.872 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 11140 _diffrn_reflns_point_group_measured_fraction_full 0.992 _diffrn_reflns_point_group_measured_fraction_max 0.872 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 34.336 _diffrn_reflns_theta_min 2.250 _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_current 1.0 _diffrn_source_power 0.05 _diffrn_source_type 'Incoatec I\ms' _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 43.381 _exptl_absorpt_correction_T_max 0.7468 _exptl_absorpt_correction_T_min 0.2250 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1599 before and 0.0997 after correction. The Ratio of minimum to maximum transmission is 0.3013. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 4.912 _exptl_crystal_description plate _exptl_crystal_F_000 1144 _exptl_crystal_recrystallization_method 'Hydrothermal Method' _exptl_crystal_size_max 0.03 _exptl_crystal_size_mid 0.02 _exptl_crystal_size_min 0.01 _refine_diff_density_max 7.855 _refine_diff_density_min -10.667 _refine_diff_density_rms 1.705 _refine_ls_extinction_coef 0.0243(16) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2016/6 (Sheldrick 2016)' _refine_ls_goodness_of_fit_ref 1.009 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 74 _refine_ls_number_reflns 3344 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.009 _refine_ls_R_factor_all 0.0870 _refine_ls_R_factor_gt 0.0759 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1589P)^2^+32.3137P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1967 _refine_ls_wR_factor_ref 0.2243 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 2891 _reflns_number_total 3344 _reflns_threshold_expression 'I > 2\s(I)' _journal_article_reference e10226 _cod_data_source_file 2386436_dn.cif _cod_data_source_block final_a _cod_database_code 1577471 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.671 _shelx_estimated_absorpt_t_min 0.356 _olex2_refinement_description ; ; _shelx_res_file ; TITL final_a.res in P2(1)/c final_a.res created by SHELXL-2016/6 at 18:44:55 on 16-Sep-2024 REM Old TITL final in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.119, Rweak 0.006, Alpha 0.023, Orientation as input REM Formula found by SHELXT: Cl5 Pb2 Rb CELL 0.71073 9.0522 8.0318 12.5921 90 90.102 90 ZERR 4 0.0057 0.0041 0.0064 0 0.023 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC Cl Pb Rb UNIT 20 8 4 L.S. 100 PLAN 5 SIZE 0.02 0.03 0.01 TEMP -101.82 CONF LIST 6 fmap 2 MORE -1 ACTA REM REM REM WGHT 0.158900 32.313698 EXTI 0.024294 FVAR 0.23065 PB01 2 0.751792 0.561882 0.494006 11.00000 0.00603 0.02130 = 0.02315 -0.00179 -0.00253 -0.00053 PB02 2 0.506519 0.507285 0.173814 11.00000 0.00929 0.02307 = 0.02496 0.00188 -0.00201 -0.00166 RB03 3 1.010214 -0.058324 0.667488 11.00000 0.00994 0.02434 = 0.02945 0.00455 -0.00290 -0.00206 CL04 1 0.715721 0.543227 -0.001318 11.00000 0.01096 0.02169 = 0.02215 0.00041 -0.00288 0.00082 CL05 1 0.542673 0.166420 0.097337 11.00000 0.00557 0.01932 = 0.02623 -0.00426 -0.00229 -0.00167 CL06 1 0.723796 0.348665 0.311120 11.00000 0.01700 0.02538 = 0.02607 -0.00660 -0.00881 0.00699 CL07 1 0.959536 0.320166 0.573873 11.00000 0.00536 0.02164 = 0.03644 0.00924 -0.00148 -0.00016 CL08 1 0.271725 0.313958 0.280380 11.00000 0.00961 0.02221 = 0.02536 0.00320 0.00028 -0.00119 HKLF 4 REM final_a.res in P2(1)/c REM R1 = 0.0759 for 2891 Fo > 4sig(Fo) and 0.0870 for all 3344 data REM 74 parameters refined using 0 restraints END WGHT 0.1441 20.2688 REM Highest difference peak 7.855, deepest hole-10.667, 1-sigma level 1.705 Q1 1 0.4181 0.5102 0.1356 11.00000 0.05 7.86 Q2 1 0.6629 0.5822 0.4623 11.00000 0.05 5.74 Q3 1 0.8430 0.5658 0.5265 11.00000 0.05 5.51 Q4 1 0.5026 0.4354 0.1771 11.00000 0.05 5.15 Q5 1 0.6771 0.5030 0.2929 11.00000 0.05 4.93 ; _shelx_res_checksum 15414 _shelx_hkl_file ; 1 0 0 552.64 47.50 -1 0 0 453.05 47.70 2 0 0 172.58 18.70 -2 0 0 183.58 18.10 3 0 0 447.36 46.30 -3 0 0 482.05 45.40 -3 0 0 465.45 45.70 5 0 0 3208.08 287.27 -5 0 0 3413.86 286.67 5 0 0 2519.15 284.27 -6 0 0 29.70 9.80 6 0 0 23.60 6.90 6 0 0 42.80 10.10 -7 0 0 154.28 21.80 7 0 0 191.98 21.10 -8 0 0 7116.89 775.12 8 0 0 9490.65 775.02 -9 0 0 1343.47 132.09 10 0 0 22.50 11.00 11 0 0 163.48 23.60 -11 0 0 156.08 28.20 -12 0 0 2974.20 255.87 12 0 0 2324.97 250.07 0 1 0 0.70 0.80 0 -1 0 1.10 0.80 0 -1 0 0.70 0.40 -1 1 0 465.05 44.10 1 1 0 447.26 44.50 -1 -1 0 494.05 44.50 -1 -1 0 497.35 44.30 1 -1 0 442.76 44.40 2 1 0 6.30 2.70 2 1 0 8.50 2.30 -2 1 0 7.00 2.90 -2 1 0 6.00 1.50 -2 -1 0 9.50 2.60 -2 -1 0 8.50 2.60 2 -1 0 6.60 2.60 2 -1 0 8.40 2.00 3 1 0 1202.28 113.59 -3 1 0 1065.59 114.19 3 1 0 1031.50 113.39 3 1 0 1167.98 113.39 3 -1 0 1394.96 113.09 -3 -1 0 1183.38 113.79 3 -1 0 1355.46 114.79 4 1 0 3.00 2.50 -4 1 0 -0.30 2.00 4 1 0 1.60 3.10 -4 1 0 -0.80 3.20 -4 -1 0 2.90 3.10 4 -1 0 1.90 2.50 4 -1 0 8.00 4.60 -4 -1 0 -1.00 2.80 5 1 0 43.20 8.80 -5 1 0 26.70 7.70 5 1 0 25.30 6.10 -5 1 0 30.90 6.10 -5 -1 0 20.50 6.40 -5 -1 0 49.10 9.90 5 -1 0 28.00 6.30 -6 1 0 30.60 7.20 6 1 0 24.90 6.70 -6 1 0 20.10 8.00 6 1 0 37.30 9.30 6 -1 0 41.10 10.40 6 -1 0 18.80 6.30 -6 -1 0 16.90 6.90 -6 -1 0 38.60 10.20 -7 1 0 1221.68 123.29 7 1 0 1385.36 121.79 7 -1 0 1325.77 121.29 -7 -1 0 1113.19 121.69 8 1 0 15.00 7.20 -8 1 0 11.50 9.00 8 -1 0 7.90 7.50 -8 -1 0 16.90 8.80 -9 1 0 56.49 15.20 9 1 0 39.80 11.30 -9 -1 0 54.09 14.00 9 -1 0 34.20 11.00 10 1 0 53.69 13.50 -10 1 0 43.00 15.40 -10 -1 0 49.80 14.90 10 -1 0 28.60 12.30 11 1 0 395.96 43.40 -11 1 0 482.85 48.90 -11 -1 0 312.77 44.70 11 -1 0 365.36 42.60 -12 1 0 31.60 17.90 12 1 0 7.60 11.60 -12 -1 0 28.50 15.20 -13 1 0 117.59 34.90 -13 -1 0 160.68 29.90 1 2 0 1321.67 111.49 -1 2 0 1091.79 110.99 1 -2 0 1148.59 110.99 -2 2 0 664.43 58.29 -2 2 0 619.94 57.19 2 2 0 573.84 57.89 -2 -2 0 635.64 57.89 2 -2 0 525.85 57.49 -2 -2 0 604.94 57.39 3 2 0 1117.69 115.89 3 2 0 1208.88 115.29 3 -2 0 1329.27 116.09 -3 -2 0 1139.79 115.39 -3 -2 0 1319.77 116.09 -4 2 0 5169.88 473.75 4 2 0 4525.65 472.05 4 2 0 5251.57 471.75 -4 -2 0 5283.27 472.55 -5 2 0 872.11 78.99 5 2 0 835.62 80.89 5 2 0 695.83 80.49 5 -2 0 911.81 81.99 -6 2 0 506.95 47.50 6 2 0 508.15 49.50 -6 2 0 384.26 50.39 -6 -2 0 569.04 51.19 6 -2 0 457.15 48.20 7 2 0 742.33 75.39 -7 2 0 864.21 78.59 -7 2 0 792.32 73.69 -7 -2 0 734.43 75.49 7 -2 0 668.33 73.99 8 2 0 4950.90 483.85 -8 2 0 5951.90 487.85 -8 -2 0 4646.24 483.95 8 -2 0 5125.19 483.25 -9 2 0 569.34 56.49 9 2 0 442.06 51.69 -9 -2 0 483.85 52.89 10 2 0 428.16 52.29 -10 2 0 610.64 59.39 -10 -2 0 487.25 61.59 11 2 0 586.84 71.29 -11 2 0 828.12 78.09 -11 -2 0 711.83 73.99 -12 2 0 2702.23 279.87 12 2 0 2597.14 269.57 -12 -2 0 3202.58 273.17 -13 -2 0 173.88 31.50 0 3 0 0.20 1.60 0 3 0 4.00 1.20 0 -3 0 3.60 1.20 0 -3 0 4.20 2.30 1 3 0 1828.52 175.28 -1 3 0 1789.92 173.98 -1 3 0 1806.62 174.78 -1 -3 0 2070.29 175.18 1 -3 0 1781.52 174.68 1 -3 0 1946.51 174.68 2 3 0 8.10 3.90 -2 3 0 6.00 2.80 -2 3 0 12.10 3.70 -2 -3 0 8.70 3.50 2 -3 0 7.00 2.80 3 3 0 1780.22 181.28 -3 3 0 1846.52 180.28 -3 3 0 2114.49 179.98 -3 3 0 2026.00 181.98 3 -3 0 1828.02 180.78 -3 -3 0 1963.00 180.58 -3 -3 0 1899.31 180.98 4 3 0 10.20 5.80 -4 3 0 32.80 8.30 -4 3 0 11.40 3.20 -4 3 0 16.10 5.50 -4 -3 0 27.30 6.10 -4 -3 0 20.60 6.10 4 -3 0 21.80 5.50 5 3 0 1053.99 111.59 -5 3 0 1015.60 112.89 -5 3 0 1175.08 109.09 -5 -3 0 1185.48 111.39 -5 -3 0 1242.08 111.99 5 -3 0 1259.17 111.79 6 3 0 15.90 7.10 -6 3 0 9.60 8.50 6 3 0 7.20 7.30 6 3 0 18.80 6.70 -6 3 0 16.60 4.20 -6 -3 0 13.30 8.20 -7 3 0 1182.18 105.09 7 3 0 1196.78 108.39 -7 -3 0 934.21 106.89 -8 3 0 67.59 16.50 8 3 0 45.10 11.80 -8 3 0 46.40 8.90 -8 -3 0 66.59 13.20 -9 3 0 784.92 72.79 -9 3 0 639.24 64.99 9 3 0 564.04 67.09 -9 -3 0 661.63 67.79 -10 3 0 10.80 8.10 -10 3 0 18.40 14.70 10 3 0 23.60 10.80 -10 -3 0 21.80 13.30 -11 3 0 1077.09 110.79 11 3 0 958.10 104.79 -11 -3 0 1128.49 106.49 -12 3 0 198.18 34.00 -12 -3 0 169.38 29.30 -13 -3 0 381.16 47.00 0 4 0 1439.26 136.19 0 -4 0 1322.97 134.49 0 -4 0 1419.56 135.39 0 -4 0 1606.34 135.99 -1 4 0 1490.55 146.79 1 4 0 1494.65 147.19 -1 4 0 1650.23 145.49 1 -4 0 1671.33 146.59 1 -4 0 1472.65 146.49 -1 -4 0 1696.93 147.09 -1 -4 0 1456.05 145.29 2 4 0 1644.64 158.68 -2 4 0 1570.34 157.68 -2 4 0 1700.43 156.98 -2 4 0 1502.45 157.78 2 -4 0 1783.02 157.48 2 -4 0 1739.83 157.98 -2 -4 0 1813.62 158.38 -3 4 0 1288.27 128.89 3 4 0 1437.56 129.59 -3 4 0 1426.36 128.29 -3 -4 0 1217.58 127.79 3 -4 0 1416.76 128.59 4 4 0 1319.37 126.79 -4 4 0 1235.28 126.99 -4 4 0 1303.57 125.29 -4 4 0 1469.25 124.59 4 -4 0 1223.38 125.49 -4 -4 0 1227.48 125.19 -4 -4 0 1458.25 126.39 -5 4 0 1193.18 113.19 -5 4 0 1106.99 110.29 -5 4 0 1123.79 108.49 5 4 0 1029.20 111.19 -5 -4 0 1278.17 110.79 -6 4 0 1172.98 109.89 -6 4 0 1068.49 115.09 -6 4 0 1282.67 113.59 6 4 0 1120.19 113.49 -6 -4 0 1155.28 112.49 7 4 0 801.02 86.49 -7 4 0 795.62 88.79 -7 4 0 932.41 87.59 -7 4 0 851.01 82.89 7 4 0 959.50 87.59 -7 -4 0 860.21 85.89 8 4 0 842.12 78.19 -8 4 0 672.73 79.69 -8 4 0 746.23 73.39 -8 -4 0 766.92 76.49 -9 4 0 463.25 47.70 9 4 0 480.75 51.89 10 4 0 753.22 92.29 -10 4 0 955.20 98.29 -10 -4 0 1052.09 93.39 -11 4 0 807.72 91.39 -11 -4 0 805.92 82.79 -12 4 0 769.32 83.39 -12 -4 0 662.43 73.89 -13 4 0 167.68 27.40 0 5 0 -0.40 3.40 0 5 0 -0.90 2.70 0 -5 0 4.40 3.50 0 -5 0 0.40 2.60 -1 5 0 1933.51 195.78 -1 5 0 1931.21 197.68 1 5 0 2021.70 198.28 1 -5 0 2317.67 197.48 1 -5 0 2112.99 197.38 -1 -5 0 2322.27 198.88 -1 -5 0 2106.49 195.78 2 5 0 59.19 10.50 -2 5 0 50.19 8.20 -2 5 0 54.09 6.30 2 -5 0 55.39 7.50 -2 -5 0 50.09 5.90 2 -5 0 42.60 7.70 -2 -5 0 49.00 7.80 3 5 0 1490.75 142.39 -3 5 0 1507.75 140.09 -3 5 0 1442.56 141.09 -3 5 0 1376.06 141.39 -3 -5 0 1641.14 142.99 4 5 0 1.80 4.90 -4 5 0 6.90 6.00 -4 5 0 -3.30 3.60 -4 -5 0 -3.30 4.60 -5 5 0 1370.86 152.98 5 5 0 1615.04 153.18 -5 5 0 1558.14 151.38 -5 5 0 1765.72 150.08 -5 -5 0 1612.04 151.08 6 5 0 147.59 21.70 -6 5 0 152.28 20.30 -6 5 0 139.19 17.30 -6 5 0 193.18 24.80 -6 -5 0 166.18 20.30 7 5 0 604.74 69.19 -7 5 0 668.33 69.09 -7 5 0 671.83 65.09 7 5 0 727.53 70.69 -7 5 0 659.63 72.29 -7 -5 0 675.93 67.89 -8 5 0 5.40 5.20 -8 5 0 1.30 11.60 -8 5 0 4.50 10.50 8 5 0 -1.00 7.90 8 5 0 8.50 10.80 -8 -5 0 25.40 9.70 -9 5 0 478.45 58.59 -9 5 0 410.56 54.29 -9 -5 0 588.84 54.19 -10 5 0 119.89 28.20 -10 -5 0 125.19 20.40 11 5 0 412.86 57.79 -11 5 0 563.74 65.89 -11 -5 0 618.44 58.29 12 5 0 16.80 15.40 -12 5 0 44.20 15.30 -12 -5 0 66.49 15.30 0 6 0 456.45 48.00 0 -6 0 483.35 47.20 0 -6 0 487.35 46.90 1 6 0 1759.52 163.18 -1 6 0 1600.54 159.78 -1 6 0 1696.53 162.58 -1 -6 0 1641.24 161.18 1 -6 0 1620.44 161.68 1 -6 0 1991.40 162.08 2 6 0 2144.79 226.08 -2 6 0 2657.03 223.28 -2 6 0 2097.19 225.08 -2 -6 0 2439.56 222.88 2 -6 0 2362.96 224.48 2 -6 0 2630.04 225.48 -3 6 0 1182.68 127.49 3 6 0 1281.67 128.99 -3 6 0 1365.06 125.99 -3 -6 0 1487.15 125.49 -3 -6 0 1348.07 126.89 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-4 3 -16 244.28 32.00 -4 -3 -16 262.27 31.80 3 3 16 108.99 26.40 -3 3 -16 147.99 21.80 -3 3 -16 147.39 19.50 -3 -3 -16 126.99 20.20 -3 -3 -16 93.59 16.30 -2 3 -16 29.30 10.70 2 3 16 6.80 11.70 -2 -3 -16 12.20 8.00 -2 -3 -16 7.60 6.20 -1 3 -16 318.37 34.70 1 3 16 360.56 40.70 -1 -3 -16 268.67 35.10 0 3 -16 206.68 24.50 0 3 16 205.38 26.90 0 -3 -16 176.08 24.60 -1 -3 16 6.80 8.70 2 3 -16 19.30 8.30 -2 3 16 8.00 7.00 -2 3 16 11.30 18.60 -2 -3 16 10.40 9.60 4 3 -16 143.79 19.20 -5 -3 16 123.09 18.20 -6 -3 16 -2.10 8.90 -7 -3 16 79.99 17.80 -7 4 -16 35.50 14.60 -6 4 -16 66.39 17.70 -5 4 -16 44.50 13.30 -5 4 -16 18.60 14.40 -4 4 -16 30.10 14.10 4 4 16 4.40 15.50 -4 4 -16 24.40 10.70 -4 -4 -16 21.30 10.60 -3 4 -16 29.80 13.40 -3 4 -16 7.60 11.50 -3 -4 -16 26.50 10.40 2 4 16 -0.50 14.80 -2 4 -16 25.30 10.70 -2 -4 -16 28.80 12.90 1 4 16 13.60 11.80 -1 4 -16 16.80 9.50 1 4 16 4.70 10.60 -1 -4 -16 9.60 8.50 0 4 -16 30.70 9.90 0 4 16 15.60 12.70 0 4 16 9.50 11.20 0 -4 -16 14.90 9.00 -1 4 16 -2.00 8.50 1 4 -16 3.50 7.50 -1 4 16 10.80 11.30 2 4 -16 22.40 9.00 -2 4 16 9.40 8.40 -2 4 16 10.90 11.40 -2 -4 16 10.30 9.10 -3 4 16 2.90 9.40 3 4 -16 7.30 8.00 -3 -4 16 1.30 9.30 4 4 -16 6.40 7.90 -4 -4 16 -7.10 9.00 -5 -4 16 13.30 11.40 -6 -4 16 -11.90 8.40 3 5 16 252.07 41.10 -3 5 -16 274.17 34.80 2 5 16 -11.30 13.80 -2 -5 -16 9.30 7.70 -1 5 -16 248.58 30.00 1 5 16 254.47 35.50 -1 -5 -16 209.18 29.50 0 5 16 204.68 31.40 0 5 -16 211.38 27.70 1 5 -16 285.07 34.80 -1 5 16 304.27 36.60 2 5 -16 10.90 8.10 3 5 -16 265.37 32.00 4 5 -16 104.49 16.90 5 5 -16 185.38 24.40 -2 6 -16 113.19 23.50 2 6 16 97.79 27.50 -1 6 -16 53.59 14.90 1 6 16 56.09 33.50 0 6 16 3.90 12.90 0 6 -16 20.70 10.90 1 6 -16 25.80 11.20 -1 6 16 12.00 12.60 2 6 -16 67.19 16.00 3 6 -16 68.89 15.50 4 6 -16 73.59 16.10 1 7 16 3.70 15.00 0 7 16 60.79 21.10 -6 0 -17 13.40 7.80 -6 0 -17 -0.20 9.70 -5 0 -17 7.10 7.60 -5 0 -17 5.30 10.80 -4 0 -17 2.20 7.50 -4 0 -17 6.40 6.20 4 0 17 7.00 13.90 -3 0 -17 4.40 8.30 -3 0 -17 2.90 6.40 -2 0 -17 9.40 5.30 -2 0 -17 -3.70 6.20 2 0 17 10.30 11.10 1 0 17 14.60 11.40 -1 0 -17 0.40 6.00 -1 0 -17 5.90 4.90 0 0 -17 5.60 4.20 0 0 -17 -1.70 5.60 0 0 17 21.60 12.20 -1 0 17 7.80 14.00 -2 0 17 9.70 12.10 2 0 -17 1.00 3.70 3 0 -17 -4.80 3.20 -4 0 17 3.10 9.30 -5 0 17 1.40 8.70 -6 1 -17 700.43 74.69 -5 1 -17 33.40 9.70 -5 -1 -17 19.40 8.80 -5 -1 -17 4.60 9.40 -4 1 -17 33.80 12.00 4 1 17 27.60 17.00 -4 -1 -17 56.19 17.50 4 -1 17 35.30 17.10 -4 -1 -17 30.60 11.40 -3 1 -17 339.37 39.90 -3 -1 -17 367.16 41.10 -2 1 -17 574.64 66.69 2 1 17 762.72 73.59 -2 1 -17 690.93 66.79 -2 -1 -17 605.24 67.39 -2 -1 -17 680.33 65.49 1 1 17 12.80 9.80 1 1 17 12.50 19.80 -1 1 -17 7.90 5.40 -1 1 -17 8.80 7.20 -1 -1 -17 7.30 5.60 -1 -1 -17 7.90 6.30 0 1 -17 74.49 11.30 0 1 17 2.00 16.30 0 1 17 94.69 16.90 0 1 -17 83.09 12.80 0 -1 -17 48.70 11.00 1 1 -17 403.46 44.10 1 -1 -17 453.15 45.60 -3 1 17 -3.50 10.40 -3 -1 17 3.60 10.50 3 -1 -17 -7.90 4.10 -4 1 17 -3.20 9.10 -4 -1 17 -8.90 14.50 -5 -1 17 643.84 66.49 -6 2 -17 105.99 18.30 -5 2 -17 62.89 17.60 -5 -2 -17 89.19 25.20 -4 2 -17 6.60 10.90 4 2 17 -8.20 12.60 -4 -2 -17 5.60 7.20 -4 -2 -17 3.30 7.00 -3 2 -17 55.39 14.30 3 2 17 14.10 20.00 -3 -2 -17 33.40 17.80 -3 -2 -17 33.00 10.80 2 2 17 65.69 19.10 -2 2 -17 54.99 13.60 -2 2 -17 80.99 11.90 -2 -2 -17 57.79 13.20 -2 -2 -17 48.50 10.50 1 2 17 56.69 15.70 -1 2 -17 59.19 12.00 1 2 17 18.90 13.50 -1 2 -17 61.99 10.40 -1 -2 -17 44.20 11.20 0 2 17 12.50 10.50 0 2 -17 14.00 5.40 0 2 17 5.40 11.70 0 -2 -17 5.40 6.40 0 -2 17 13.90 9.00 -1 2 17 47.30 11.40 -1 2 17 15.20 12.80 1 2 -17 49.20 10.50 1 -2 -17 27.20 9.00 -1 -2 17 8.10 10.10 2 -2 -17 58.09 12.90 -3 2 17 1.40 11.30 -3 -2 17 2.40 11.10 -4 -2 17 -3.30 10.50 -5 -2 17 53.09 13.40 -6 3 -17 985.90 101.29 -5 3 -17 281.07 35.60 4 3 17 70.99 24.10 -4 3 -17 95.69 19.80 -4 -3 -17 95.69 23.10 -4 -3 -17 62.69 14.30 3 3 17 96.89 25.40 -3 3 -17 72.79 16.50 -3 -3 -17 89.49 17.20 -2 3 -17 367.86 40.80 2 3 17 416.16 48.40 -2 -3 -17 323.97 42.60 -1 3 -17 172.58 22.40 1 3 17 168.88 27.80 -1 -3 -17 146.09 23.60 0 3 17 142.49 22.10 0 3 -17 128.69 17.30 0 -3 -17 88.99 17.80 1 3 -17 109.39 16.40 -1 3 17 115.39 18.10 1 -3 -17 86.19 17.00 -3 -3 17 5.40 10.60 -4 -3 17 -0.50 8.90 -5 -3 17 -5.00 11.10 -6 -3 17 85.59 17.80 -4 4 -17 20.10 14.00 -3 4 -17 228.18 30.00 3 4 17 204.68 36.90 -2 4 -17 66.99 17.30 2 4 17 62.79 21.30 -2 -4 -17 67.19 15.00 -1 4 -17 28.90 11.60 1 4 17 22.00 14.70 -1 -4 -17 19.20 9.60 0 4 -17 33.60 10.50 0 4 17 10.50 11.20 0 -4 -17 1.20 7.80 1 4 -17 274.37 31.50 -1 4 17 250.07 32.40 3 4 -17 39.00 9.50 -3 -4 17 -3.60 11.20 -4 -4 17 -15.60 10.20 -2 5 -17 46.40 16.00 2 5 17 24.40 18.60 -1 5 -17 200.98 27.00 0 5 17 238.88 32.60 0 5 -17 199.78 30.60 -1 5 17 94.99 20.30 1 5 -17 121.99 20.90 2 5 -17 111.69 19.20 3 5 -17 165.98 23.00 1 6 17 -4.70 16.20 0 6 17 -27.40 15.40 2 6 -17 86.49 18.90 -5 0 -18 158.28 26.60 -5 0 -18 208.88 28.40 -4 0 -18 541.75 54.09 -4 0 -18 413.26 50.99 3 0 18 46.30 18.20 -3 0 -18 35.10 10.90 -3 0 -18 40.20 10.30 -2 0 -18 12.40 6.20 -2 0 -18 1.30 7.00 2 0 18 -5.00 10.70 -1 0 -18 240.88 28.60 -1 0 18 -4.10 12.20 1 0 -18 16.20 5.60 -2 0 18 23.90 15.40 2 0 -18 12.30 5.20 -3 0 18 2.20 17.30 -5 1 -18 156.68 20.70 -4 1 -18 18.00 12.00 -4 -1 -18 29.40 9.60 -4 -1 -18 12.40 9.30 -3 1 -18 28.50 11.90 -3 1 -18 31.80 9.20 3 1 18 17.80 15.20 -3 -1 -18 32.30 11.70 -3 -1 -18 37.20 12.50 -2 1 -18 18.40 8.60 2 1 18 16.50 15.10 -2 -1 -18 24.70 8.50 -1 1 -18 124.79 18.50 1 1 18 138.39 22.90 -1 1 -18 147.19 18.10 -1 -1 -18 116.89 18.30 0 1 18 26.70 14.70 0 -1 -18 9.40 6.50 0 -1 18 19.40 10.80 -1 1 18 9.80 15.30 -1 -1 18 8.50 12.50 1 -1 -18 17.70 7.10 -2 1 18 9.00 18.10 2 -1 -18 5.20 5.40 -2 -1 18 10.30 11.20 3 -1 -18 42.50 9.90 -3 -1 18 -3.50 10.90 -4 -1 18 -4.20 18.30 -5 2 -18 237.08 29.70 -4 2 -18 244.88 36.30 -4 2 -18 333.07 35.30 -3 2 -18 4.00 9.60 3 2 18 -22.40 10.90 -3 -2 -18 14.00 7.50 2 2 18 0.90 12.80 -2 2 -18 6.10 7.80 -2 -2 -18 7.50 6.70 -1 2 -18 126.59 18.70 1 2 18 125.39 24.30 0 2 -18 469.45 45.90 0 2 18 511.45 50.19 0 -2 -18 347.97 45.90 -1 -2 18 4.10 11.10 1 -2 -18 0.90 6.40 -2 -2 18 3.60 12.80 2 -2 -18 20.20 8.60 3 -2 -18 80.29 15.60 -4 -2 18 -13.10 11.90 -3 3 -18 82.19 17.50 -2 3 -18 112.69 18.20 2 3 18 91.89 23.90 -2 -3 -18 87.79 21.70 -1 3 -18 127.29 19.40 -1 -3 -18 109.49 18.80 0 3 -18 37.40 11.50 0 3 18 38.40 13.80 0 -3 -18 20.40 8.80 -1 3 18 76.49 16.50 1 3 -18 84.79 14.20 1 -3 -18 58.79 13.90 2 -3 -18 27.60 9.90 -2 -3 18 -2.30 10.80 -3 -3 18 -4.00 12.90 -4 -3 18 -16.90 10.50 -2 4 -18 17.20 11.90 2 4 18 9.10 16.10 -1 4 -18 47.40 13.20 1 4 18 42.20 16.80 0 4 -18 141.09 21.00 0 4 18 107.69 23.40 1 4 -18 111.19 18.20 1 5 18 18.60 17.80 0 5 -18 51.39 13.70 0 5 18 19.00 16.80 1 5 -18 79.19 17.20 -3 0 -19 11.30 6.00 -2 0 -19 14.80 6.90 -1 0 -19 16.40 5.50 -4 1 -19 144.39 22.80 -3 -1 -19 22.50 11.50 -2 -1 -19 29.80 8.00 -1 -1 -19 154.98 29.30 0 -1 -19 88.19 14.50 1 -1 -19 4.60 5.30 -3 2 -19 27.50 11.20 1 2 19 77.59 21.10 -1 -2 -19 88.19 16.20 0 -2 -19 54.09 12.20 -1 -2 19 27.80 15.50 1 -2 -19 9.20 6.70 2 -2 -19 6.70 6.90 3 -2 -19 27.40 10.50 -2 3 -19 -2.90 9.30 0 3 19 17.60 14.50 -2 -3 19 15.90 13.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 63438 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pb01 Pb 0.75179(5) 0.56188(7) 0.49401(4) 0.0168(2) Uani 1 1 d . . . . . Pb02 Pb 0.50652(6) 0.50729(8) 0.17381(4) 0.0191(2) Uani 1 1 d . . . . . Rb03 Rb 1.01021(15) -0.0583(2) 0.66749(12) 0.0212(4) Uani 1 1 d . . . . . Cl04 Cl 0.7157(4) 0.5432(5) -0.0013(3) 0.0183(6) Uani 1 1 d . . . . . Cl05 Cl 0.5427(3) 0.1664(4) 0.0973(3) 0.0170(6) Uani 1 1 d . . . . . Cl06 Cl 0.7238(4) 0.3487(5) 0.3111(3) 0.0228(7) Uani 1 1 d . . . . . Cl07 Cl 0.9595(3) 0.3202(5) 0.5739(3) 0.0211(7) Uani 1 1 d . . . . . Cl08 Cl 0.2717(4) 0.3140(5) 0.2804(3) 0.0191(6) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pb01 0.0060(3) 0.0213(3) 0.0232(3) -0.00179(17) -0.00253(19) -0.00053(15) Pb02 0.0093(3) 0.0231(4) 0.0250(3) 0.00188(18) -0.0020(2) -0.00166(16) Rb03 0.0099(6) 0.0243(8) 0.0294(7) 0.0045(5) -0.0029(5) -0.0021(4) Cl04 0.0110(13) 0.0217(15) 0.0222(14) 0.0004(12) -0.0029(10) 0.0008(11) Cl05 0.0056(12) 0.0193(14) 0.0262(14) -0.0043(12) -0.0023(10) -0.0017(10) Cl06 0.0170(15) 0.0254(16) 0.0261(15) -0.0066(13) -0.0088(12) 0.0070(12) Cl07 0.0054(12) 0.0216(15) 0.0364(17) 0.0092(13) -0.0015(11) -0.0002(11) Cl08 0.0096(13) 0.0222(15) 0.0254(14) 0.0032(12) 0.0003(11) -0.0012(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _audit_author_name _audit_author_address 'Diptam Nasipuri' ;Indian Association for the Cultivation of Science India ; loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 Cl05 Pb01 Rb03 123.52(8) 4_566 1_565 Cl05 Pb01 Rb03 117.54(8) 2_655 1_565 Cl05 Pb01 Cl05 76.91(11) 4_566 2_655 Cl05 Pb01 Cl08 75.11(10) 4_566 3_666 Cl06 Pb01 Rb03 148.35(9) . 1_565 Cl06 Pb01 Cl05 85.83(12) . 4_566 Cl06 Pb01 Cl05 77.56(10) . 2_655 Cl06 Pb01 Cl07 86.27(11) . . Cl06 Pb01 Cl07 92.09(12) . 3_766 Cl06 Pb01 Cl08 160.47(11) . 3_666 Cl07 Pb01 Rb03 56.33(9) 3_766 1_565 Cl07 Pb01 Rb03 87.02(9) . 1_565 Cl07 Pb01 Cl05 153.48(10) . 2_655 Cl07 Pb01 Cl05 81.13(10) . 4_566 Cl07 Pb01 Cl05 155.82(9) 3_766 4_566 Cl07 Pb01 Cl05 126.17(10) 3_766 2_655 Cl07 Pb01 Cl07 74.70(12) . 3_766 Cl07 Pb01 Cl08 86.63(11) . 3_666 Cl07 Pb01 Cl08 103.52(10) 3_766 3_666 Cl08 Pb01 Rb03 49.08(7) 3_666 1_565 Cl08 Pb01 Cl05 101.71(10) 3_666 2_655 Rb03 Pb02 Rb03 169.46(4) 4_465 4_565 Cl04 Pb02 Rb03 132.01(8) 3_665 4_565 Cl04 Pb02 Rb03 128.61(8) . 4_465 Cl04 Pb02 Rb03 48.06(8) . 4_565 Cl04 Pb02 Rb03 47.92(8) 3_665 4_465 Cl04 Pb02 Cl04 84.33(11) . 3_665 Cl04 Pb02 Cl08 149.48(11) . . Cl05 Pb02 Rb03 101.04(6) . 4_465 Cl05 Pb02 Rb03 88.05(6) . 4_565 Cl05 Pb02 Cl04 73.05(10) . 3_665 Cl05 Pb02 Cl04 76.75(10) . . Cl05 Pb02 Cl08 74.83(10) . . Cl06 Pb02 Rb03 51.50(9) . 4_565 Cl06 Pb02 Rb03 136.23(9) . 4_465 Cl06 Pb02 Cl04 145.75(11) . 3_665 Cl06 Pb02 Cl04 93.06(11) . . Cl06 Pb02 Cl05 73.11(10) . . Cl06 Pb02 Cl08 89.20(12) . . Cl08 Pb02 Rb03 140.51(7) . 4_565 Cl08 Pb02 Rb03 48.63(7) . 4_465 Cl08 Pb02 Cl04 76.99(11) . 3_665 Pb01 Rb03 Pb02 126.70(4) 1_545 4_666 Rb03 Rb03 Pb01 69.25(5) 3_756 1_545 Rb03 Rb03 Pb02 92.20(5) 3_756 4_666 Cl04 Rb03 Pb01 45.86(7) 4_566 1_545 Cl04 Rb03 Pb01 104.56(8) 2_745 1_545 Cl04 Rb03 Pb02 141.76(8) 4_566 4_666 Cl04 Rb03 Pb02 41.43(7) 2_745 4_666 Cl04 Rb03 Rb03 49.61(7) 4_566 3_756 Cl04 Rb03 Rb03 50.82(7) 2_745 3_756 Cl04 Rb03 Cl04 100.43(10) 2_745 4_566 Cl04 Rb03 Cl06 137.58(11) 2_745 4_566 Cl04 Rb03 Cl06 71.81(11) 2_745 3_756 Cl04 Rb03 Cl06 74.47(10) 4_566 4_566 Cl04 Rb03 Cl07 64.53(9) 2_745 3_756 Cl04 Rb03 Cl07 131.84(10) 4_566 2_746 Cl04 Rb03 Cl07 64.39(9) 4_566 3_756 Cl04 Rb03 Cl07 127.45(10) 2_745 2_746 Cl04 Rb03 Cl08 66.61(9) 2_745 4_666 Cl06 Rb03 Pb01 101.01(8) 4_566 1_545 Cl06 Rb03 Pb01 86.52(8) 3_756 1_545 Cl06 Rb03 Pb02 132.03(7) 4_566 4_666 Cl06 Rb03 Pb02 49.36(8) 3_756 4_666 Cl06 Rb03 Rb03 104.94(9) 3_756 3_756 Cl06 Rb03 Rb03 111.14(8) 4_566 3_756 Cl06 Rb03 Cl04 129.33(10) 3_756 4_566 Cl06 Rb03 Cl06 143.51(8) 3_756 4_566 Cl06 Rb03 Cl07 137.30(9) 4_566 3_756 Cl06 Rb03 Cl07 67.56(9) 3_756 3_756 Cl06 Rb03 Cl07 70.66(9) 3_756 2_746 Cl06 Rb03 Cl08 82.44(10) 3_756 4_666 Cl07 Rb03 Pb01 108.42(7) 2_746 1_545 Cl07 Rb03 Pb01 40.79(6) 3_756 1_545 Cl07 Rb03 Pb01 112.77(8) . 1_545 Cl07 Rb03 Pb02 93.47(6) . 4_666 Cl07 Rb03 Pb02 86.04(6) 2_746 4_666 Cl07 Rb03 Pb02 89.49(6) 3_756 4_666 Cl07 Rb03 Rb03 47.64(7) 3_756 3_756 Cl07 Rb03 Rb03 175.32(9) 2_746 3_756 Cl07 Rb03 Rb03 56.29(8) . 3_756 Cl07 Rb03 Cl04 68.63(9) . 4_566 Cl07 Rb03 Cl04 69.78(10) . 2_745 Cl07 Rb03 Cl06 140.21(10) . 3_756 Cl07 Rb03 Cl06 73.11(9) 2_746 4_566 Cl07 Rb03 Cl06 69.29(9) . 4_566 Cl07 Rb03 Cl07 128.10(11) . 2_746 Cl07 Rb03 Cl07 127.93(6) 2_746 3_756 Cl07 Rb03 Cl07 103.93(9) . 3_756 Cl07 Rb03 Cl08 73.26(10) . 4_666 Cl07 Rb03 Cl08 122.12(10) . 3_656 Cl08 Rb03 Pb01 167.60(7) 4_666 1_545 Cl08 Rb03 Pb01 43.05(7) 3_656 1_545 Cl08 Rb03 Pb02 40.93(6) 4_666 4_666 Cl08 Rb03 Pb02 144.41(8) 3_656 4_666 Cl08 Rb03 Rb03 107.06(8) 3_656 3_756 Cl08 Rb03 Rb03 108.21(8) 4_666 3_756 Cl08 Rb03 Cl04 141.87(10) 4_666 4_566 Cl08 Rb03 Cl04 63.10(9) 3_656 4_566 Cl08 Rb03 Cl04 147.06(11) 3_656 2_745 Cl08 Rb03 Cl06 68.66(10) 3_656 4_566 Cl08 Rb03 Cl06 96.04(11) 3_656 3_756 Cl08 Rb03 Cl06 91.24(10) 4_666 4_566 Cl08 Rb03 Cl07 72.34(9) 3_656 2_746 Cl08 Rb03 Cl07 128.36(9) 4_666 3_756 Cl08 Rb03 Cl07 73.15(9) 4_666 2_746 Cl08 Rb03 Cl07 82.53(9) 3_656 3_756 Cl08 Rb03 Cl08 143.84(6) 3_656 4_666 Pb02 Cl04 Pb02 95.67(11) . 3_665 Pb02 Cl04 Rb03 92.29(11) . 4_565 Pb02 Cl04 Rb03 158.24(14) . 2_755 Pb02 Cl04 Rb03 90.65(10) 3_665 2_755 Pb02 Cl04 Rb03 169.64(13) 3_665 4_565 Rb03 Cl04 Rb03 79.57(10) 2_755 4_565 Pb01 Cl05 Pb01 103.09(11) 4_565 2_645 Pb02 Cl05 Pb01 143.41(12) . 4_565 Pb02 Cl05 Pb01 106.67(10) . 2_645 Pb01 Cl06 Pb02 105.85(12) . . Pb01 Cl06 Rb03 106.64(11) . 3_756 Pb01 Cl06 Rb03 93.52(11) . 4_565 Pb02 Cl06 Rb03 146.55(13) . 3_756 Pb02 Cl06 Rb03 89.04(11) . 4_565 Rb03 Cl06 Rb03 81.24(9) 3_756 4_565 Pb01 Cl07 Pb01 105.30(12) . 3_766 Pb01 Cl07 Rb03 106.33(10) 3_766 . Pb01 Cl07 Rb03 82.89(10) 3_766 3_756 Pb01 Cl07 Rb03 98.35(11) . 3_756 Pb01 Cl07 Rb03 101.05(12) . 2_756 Pb01 Cl07 Rb03 96.70(11) 3_766 2_756 Pb01 Cl07 Rb03 146.84(12) . . Rb03 Cl07 Rb03 76.07(9) . 3_756 Rb03 Cl07 Rb03 159.97(11) 2_756 3_756 Rb03 Cl07 Rb03 84.92(9) . 2_756 Pb01 Cl08 Rb03 98.81(10) 3_666 4_465 Pb01 Cl08 Rb03 87.88(9) 3_666 3_656 Pb02 Cl08 Pb01 107.80(11) . 3_666 Pb02 Cl08 Rb03 164.13(13) . 3_656 Pb02 Cl08 Rb03 90.44(10) . 4_465 Rb03 Cl08 Rb03 84.55(9) 3_656 4_465 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Pb01 Rb03 4.419(2) 1_565 Pb01 Cl05 2.941(3) 4_566 Pb01 Cl05 3.020(3) 2_655 Pb01 Cl06 2.881(4) . Pb01 Cl07 2.883(4) . Pb01 Cl07 2.909(4) 3_766 Pb01 Cl08 3.019(4) 3_666 Pb02 Rb03 4.579(3) 4_565 Pb02 Rb03 4.512(3) 4_465 Pb02 Cl04 2.924(4) . Pb02 Cl04 2.986(4) 3_665 Pb02 Cl05 2.921(4) . Pb02 Cl06 2.910(4) . Pb02 Cl08 2.956(4) . Rb03 Rb03 4.325(4) 3_756 Rb03 Cl04 3.409(4) 4_566 Rb03 Cl04 3.349(4) 2_745 Rb03 Cl06 3.584(5) 4_566 Rb03 Cl06 3.362(4) 3_756 Rb03 Cl07 3.292(4) . Rb03 Cl07 3.706(5) 3_756 Rb03 Cl07 3.410(5) 2_746 Rb03 Cl08 3.386(4) 4_666 Rb03 Cl08 3.342(4) 3_656