data_2000140
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  2547
_journal_page_last  2550
loop_
_publ_author_name
 'Whang, D.'
 'Kim, K.'
_chemical_formula_sum  'C37 H47 N4 Rh1'
_chemical_formula_weight  650.72
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_cell_length_a  10.9730(10)
_cell_length_b  11.8750(10)
_cell_length_c  14.2110(10)
_cell_angle_alpha  108.030(10)
_cell_angle_beta  105.410(10)
_cell_angle_gamma  100.920(10)
_cell_volume  1616.0(7)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.337
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  684
_exptl_absorpt_coefficient_mu  0.55
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.7093
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Rh -.20009(3) .03034(3) .01373(3)
 N1 -.2849(3) .1189(3) -.0763(2)
 N2 -.2112(3) .1537(3) .1438(2)
 N3 -.1110(3) -.0544(3) .1044(2)
 N4 -.1857(3) -.0897(3) -.1155(2)
 C1 -.3183(4) .0831(3) -.1822(3)
 C2 -.3812(4) .1685(3) -.2170(3)
 C3 -.3837(4) .2526(3) -.1295(3)
 C4 -.3242(4) .2235(3) -.0402(3)
 C5 -.3108(4) .2848(3) .0630(3)
 C6 -.2609(4) .2546(3) .1480(3)
 C7 -.2566(4) .3164(4) .2537(3)
 C8 -.2059(4) .2547(4) .3147(3)
 C9 -.1775(4) .1538(4) .2422(3)
 C10 -.1204(4) .0688(4) .2730(3)
 C11 -.0903(4) -.0270(3) .2080(3)
 C12 -.0294(4) -.1139(3) .2420(3)
 C13 -.0175(4) -.1928(3) .1562(3)
 C14 -.0688(4) -.1564(3) .0693(3)
 C15 -.0766(4) -.2152(3) -.0330(3)
 C16 -.1319(4) -.1874(3) -.1197(3)
 C17 -.1471(4) -.2567(3) -.2267(3)
 C18 -.2090(4) -.2015(3) -.2881(3)
 C19 -.2330(4) -.0985(3) -.2160(3)
 C20 -.2953(4) -.0175(3) -.2477(3)
 C21 -.4261(5) .1622(4) -.3280(4)
 C22 -.5595(6) .0790(6) -.3852(5)
 C23 -.4403(4) .3630(4) -.1217(4)
 C24 -.5799(4) .3334(4) -.1176(4)
 C25 -.3024(4) .4322(4) .2883(4)
 C26 -.4509(5) .3982(5) .2596(4)
 C27 -.1808(5) .2841(4) .4295(4)
 C28' -.0699(9) .3653(9) .5012(7)
 C28 -.2620(10)  .2290(10)    .4527(7)
 C29 .0114(5) -.1106(4) .3522(4)
 C30 -.0983(6) -.1813(5) .3763(4)
 C31 .0360(4) -.3032(3) .1466(4)
 C32 -.0748(5) -.4245(4) .1050(4)
 C33 -.1044(4) -.3728(4) -.2625(3)
 C34 -.2098(5) -.4886(4) -.2781(4)
 C35 -.2451(5) -.2365(4) -.4052(3)
 C36 -.3827(6) -.3181(5) -.4675(4)
 C37 -.3735(4) -.0819(4) -.0120(3)
 H1 -.340 .357 .077
 H2 -.101 .078 .345
 H3 -.040 -.283 -.046
 H4 -.324 -.033 -.321
 H5 -.442 .383 -.182
 H6 -.384 .432 -.059
 H7 -.611 .404 -.113
 H8 -.637 .265 -.180
 H9 -.578 .314 -.058
 H10 -.276 .485 .255
 H11 -.262 .474 .363
 H12 -.476 .472 .282
 H13 -.492 .357 .185
 H14 -.478 .346 .293
 H15 .041 -.026 .400
 H16 .083 -.145 .362
 H17 -.065 -.175 .447
 H18 -.170 -.147 .367
 H19 -.127 -.265 .330
 H20 .094 -.291 .214
 H21 .084 -.308 .099
 H22 -.038 -.491 .100
 H23 -.123 -.421 .152
 H24 -.133 -.437 .037
 H25 -.024 -.364 -.211
 H26 -.091 -.382 -.327
 H27 -.180 -.559 -.300
 H28 -.224 -.480 -.213
 H29 -.291 -.499 -.330
 H30 -.190 -.282 -.430
 H31 -.233 -.163 -.420
 H32 -.411 -.337 -.540
 H33 -.406 -.391 -.454
 H34 -.449 -.272 -.444
 H35 -.367 .133 -.361
 H36 -.424 .243 -.327
 H37 -.586 .077 -.455
 H38 -.561 -.001 -.386
 H39 -.617 .109 -.352
 H45 .359 .146 .037
 H46 .426 .090 .076
 H47 .608 .937 .043