data_2000175
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  2339
_journal_page_last  2343
loop_
_publ_author_name
 'Burns, J.H.'
 'Sachleben, R.A.'
_chemical_formula_moiety  'Li(C25H26PO6)C2H5OH'
_chemical_formula_sum  'C27 H32 O7 P Li'
_chemical_formula_weight  505.46
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P 1'
_symmetry_space_group_name_Hall  'P 1'
_cell_length_a  10.1580(10)
_cell_length_b  10.6630(10)
_cell_length_c  12.766(2)
_cell_angle_alpha  100.930(10)
_cell_angle_beta  109.550(10)
_cell_angle_gamma  99.100(10)
_cell_volume  1242.2(6)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.35
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  536
_exptl_absorpt_coefficient_mu  0.149
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 P .56730(10)   .40450(10)   .24139(9)
 O1 .3956(3) .1938(3) -.3547(2)
 O2 .6765(3) .3161(3) -.3178(2)
 O3 .7493(3) .3403(3) -.1026(2)
 O4 .4667(3) .2178(3) -.1407(2)
 O5 .6500(3) .4449(3) .3686(2)
 O6 .4921(3) .4990(3) .1859(2)
 O7 .1122(5) .3777(6) .4958(4)
 C1 .3634(5) .1858(5) -.4757(3)
 C2 .4685(5) .2984(5) -.4823(3)
 C3 .6223(5) .2895(5) -.4426(3)
 C4 .8166(4) .3120(4) -.2627(3)
 C5 .9152(5) .2975(5) -.3137(3)
 C6 1.0545(5) .2956(5) -.2473(4)
 C7 1.0957(4) .3111(5) -.1299(4)
 C8 .9976(4) .3264(4) -.0778(4)
 C9 .8580(4) .3266(4) -.1436(3)
 C10 .7767(4) .3315(4) .0138(3)
 C11 .6465(4) .3457(4) .0436(3)
 C12 .5182(4) .2290(4) -.0195(3)
 C13 .3472(4) .1170(4) -.2091(3)
 C14 .2679(4) .0350(4) -.1683(3)
 C15 .1503(5) -.0631(5) -.2486(4)
 C16 .1151(5) -.0789(5) -.3636(4)
 C17 .1931(5) .0045(4) -.4051(4)
 C18 .3083(4) .1037(4) -.3269(3)
 C19 .6903(4) .3625(4) .1740(3)
 C20 .4311(4) .2550(4) .2107(3)
 C21 .2871(5) .2536(5) .1620(4)
 C22 .1808(5) .1431(6) .1447(5)
 C23 .2187(5) .0342(5) .1757(4)
 C24 .3601(5) .0325(4) .2221(4)
 C25 .4664(4) .1419(4) .2395(3)
 C26 .086(2) .4000(10)   .4110(10)
 C27 .079(2) .379(2) .317(2)
 Li .5505(7) .3431(7) -.2197(5)
 H(1) .267 .194 -.511
 H(2) .374 .104 -.513
 H(3) .464 .378 -.436
 H(4) .439 .302 -.561
 H(5) .628 .203 -.476
 H(6) .677 .352 -.465
 H(7) .888 .289 -.394
 H(8) 1.122 .283 -.283
 H(9) 1.192 .311 -.085
 H(10) 1.026 .336 .003
 H(11) .858 .400 .065
 H(12) .796 .248 .021
 H(13) .618 .420 .021
 H(14) .546 .151 -.006
 H(15) .443 .241 .008
 H(16) .293 .045 -.088
 H(17) .093 -.120 -.222
 H(18) .037 -.148 -.417
 H(19) .168 -.006 -.486
 H(20) .709 .281 .188
 H(21) .777 .430 .211
 H(22) .260 .329 .140
 H(23) .082 .143 .111
 H(24) .146 -.041 .165
 H(25) .386 -.044 .243
 H(26) .565 .140 .272
 H(27) .800 .558 .453