data_2000184
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  2433
_journal_page_last  2435
loop_
_publ_author_name
 'Mullica, D.F.'
 'Sappenfield, E.L.'
_chemical_formula_moiety  'Fe1 Gd1 6(C1 N1),4(H2 O1)'
_chemical_formula_sum  'C6 H8 Fe1 Gd1 N6 O4'
_chemical_formula_weight  441.26
_symmetry_cell_setting  orthorhombic
_symmetry_space_group_name_H-M  'C m c m'
_symmetry_space_group_name_Hall  '-C 2c 2'
_cell_length_a  7.3964(3)
_cell_length_b  12.8372(5)
_cell_length_c  13.6726(4)
_cell_angle_alpha  90
_cell_angle_beta  90
_cell_angle_gamma  90
_cell_volume  1298.21(8)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  2.26
_exptl_crystal_density_meas  2.23(2)
_exptl_crystal_F_000  832
_exptl_absorpt_coefficient_mu  6.223
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Gd .0 .323500(10)  .25 0.01081(4)
 Fe .0 .0 .0 0.01100(10)
 C(1) .3147(3) .4526(2) .0890(2) 0.0183(4)
 C(2) .0 .1359(2) .0593(2) 0.0181(6)
 N(1) .2025(3) .4233(2) .1405(2) 0.0226(5)
 N(2) .0 .2161(2) .0972(2) 0.0260(7)
 O(1) .2610(4) .2164(2) .25 0.0341(6)
 O(2) .0 .6567(2) .0996(3) 0.0372(8)