data_2000200
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  2508
_journal_page_last  2510
loop_
_publ_author_name
 'Vichet, A.'
 'Galy, J.P.'
 'Baldy, A.'
 'Barbe, J.'
 'Feneau-Dupont, J.'
 'Declercq, J.P.'
_chemical_formula_sum  'C24 H29 N1 O7'
_chemical_formula_weight  443.5
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_cell_length_a  8.426(2)
_cell_length_b  11.420(2)
_cell_length_c  11.739(4)
_cell_angle_alpha  87.20(3)
_cell_angle_beta  79.33(3)
_cell_angle_gamma  77.88(2)
_cell_volume  1085.3(5)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.36
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  472
_exptl_absorpt_coefficient_mu  0.108
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 C1 .9787(2) .84650(10)    .69000(10)    .0470(10)
 O2 1.14590(10)  .81680(10)  .64140(10)     .0580(10)
 C3 1.1949(2) .8684(2) .5287(2) .0560(10)
 C4 1.2850(2) .9669(2) .5342(2) .0550(10)
 O5 1.17380(10)  1.06950(10)   .58510(10)   .0560(10)
 C6 1.2488(2) 1.1669(2) .5967(2) .0570(10)
 C7 1.1219(3) 1.2641(2) .6608(2) .0600(10)
 O8 1.01270(10)  1.32400(10)   .58770(10)   .0550(10)
 C9 .8774(3) 1.4033(2) .6524(2) .0600(10)
 C10 .7673(2) 1.4659(2) .5712(2) .0600(10)
 O11 .61440(10)  1.52940(10)   .63430(10)   .0610(10)
 C12 .4975(2) 1.4549(2) .6688(2) .0610(10)
 C13 .3536(2) 1.5193(2) .7537(2) .0580(10)
 O14 .40130(10)  1.52570(10)   .86270(10)   .0530(10)
 C15 .2652(2) 1.5624(2) .9551(2) .0570(10)
 C16 .2268(2) 1.4618(2) 1.0344(2) .0540(10)
 O17 .14970(10)  1.38050(10)   .98490(10)   .0570(10)
 C18 .2398(2) 1.26890(10)   .95060(10)   .0430(10)
 C19 .1483(2) 1.1803(2) .94870(10)   .0480(10)
 C20 .2236(2) 1.0667(2) .91220(10)   .0470(10)
 C21 .3957(2) 1.03590(10)   .87500(10)   .0390(10)
 N22 .4732(2) .92120(10)  .83590(10)     .0420(10)
 C23 .6406(2) .89530(10)  .78920(10)     .0400(10)
 C24 .7187(2) .7831(2) .7391(2) .0520(10)
 C25 .8831(2) .7604(2) .6912(2) .0540(10)
 C26 .9067(2) .95510(10)  .73970(10)     .0460(10)
 C27 .7383(2) .98180(10)  .78890(10)     .0410(10)
 C28 .6662(2) 1.10030(10)   .83840(10)   .0440(10)
 C29 .4878(2) 1.12500(10)   .87680(10)   .0390(10)
 C30 .4072(2) 1.24140(10)   .91510(10)   .0430(10)
 C31 .3765(2) .8270(2) .8481(2) .0560(10)
 O32 .75150(10)  1.17500(10)   .84620(10)   .0640(10)
 H3 1.095(2)   .8958(16) .4941(15) ?
 H3' 1.272(2)   .8028(16) .4820(15) ?
 H4 1.332(2)   .9895(15) .4507(16) ?
 H4' 1.371(2)   .9416(15) .5786(15) ?
 H6 1.337(2)   1.1418(15) .6417(15) ?
 H6' 1.297(2)   1.1946(16) .5192(16) ?
 H7 1.061(2)   1.2281(16) .7318(16) ?
 H7' 1.178(2)   1.3219(16) .6864(15) ?
 H9 .919(2)   1.4648(17) .6919(15) ?
 H9' .818(2)   1.3568(16) .7123(15) ?
 H10 .821(2)   1.5245(17) .5222(15) ?
 H10' .749(2)   1.4062(16) .5169(15) ?
 H12 .550(2)   1.3794(17) .7033(16) ?
 H12' .461(2)   1.4342(16) .6001(16) ?
 H13 .305(2)   1.6019(17) .7244(15) ?
 H13' .264(2)   1.4743(16) .7622(15) ?
 H15 .169(2)   1.5979(16) .9207(15) ?
 H15' .296(2)   1.6227(17) 1.0019(15) ?
 H16 .142(2)   1.4944(15) 1.1000(15) ?
 H16' .329(2)   1.4171(16) 1.0624(15) ?
 H19 .030(2)   1.2005(16) .9728(15) ?
 H20 .156(2)   1.0094(16) .9103(15) ?
 H24 .660(2)   .7244(16) .7364(15) ?
 H25 .937(2)   .6846(17) .6560(15) ?
 H26 .970(2)   1.0148(15) .7415(15) ?
 H30 .473(2)   1.2978(16) .9127(15) ?
 H31 .314(2)   .8342(16) .7923(16) ?
 H31' .449(2)   .7489(17) .8478(15) ?
 H31" .303(2)   .8345(16) .9231(16) ?