#------------------------------------------------------------------------------
#$Date: 2008-01-26 13:05:32 +0000 (Sat, 26 Jan 2008) $
#$Revision: 19 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000212.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000212
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  2092
_journal_page_last  2094
loop_
_publ_author_name
 'Davies, J.A.'
 'Pinkerton, A.A.'
 'Vilmer, M.'
_chemical_formula_sum  'C10 H28 Cl4 P4 Pd2'
_chemical_formula_weight  626.84
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_cell_length_a  8.8930(10)
_cell_length_b  9.712
_cell_length_c  12.745(3)
_cell_angle_alpha  90
_cell_angle_beta  103.380(10)
_cell_angle_gamma  90
_cell_volume  1071.00(6)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.94
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  616
_exptl_absorpt_coefficient_mu  2.45
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Pd(1) .57415(4) .43823(4) .36202(2)
 Cl(1) .4911(2) .59280(10)
    .21736(9)
 Cl(2) .8294(2) .4702(2) .34450(10)
 P(1) .67650(10)
   .31000(10)
   .50957(9)
 P(2) .31870(10)
   .41710(10)
   .35613(9)
 C(1) .7698(5) .4184(5) .6226(4)
 C(2) .5656(6) .1915(5) .5698(4)
 C(3) .8323(6) .1977(6) .4920(5)
 C(4) .2380(6) .2985(6) .4372(4)
 C(5) .2122(6) .3661(6) .2230(4)
 H(1) .871 .438 .614
 H(2) .777 .365 .686
 H(3) .631 .149 .631
 H(4) .486 .240 .592
 H(5) .522 .123 .519
 H(6) .870 .147 .556
 H(7) .795 .136 .434
 H(8) .913 .252 .476
 H(9) .129 .308 .421
 H(10) .264 .207 .422
 H(11) .279 .318 .511
 H(12) .106 .358 .223
 H(13) .225 .434 .172
 H(14) .250 .280 .205