data_2000213
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  2101
_journal_page_last  2104
loop_
_publ_author_name
 'Bostrom, D.'
 'Strandberg, R.'
 'Noren, B.'
 'Oskarson, A.'
_chemical_formula_sum  'C4 H12 N2 O8 Pt1 S2'
_chemical_formula_weight  475.36
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_cell_length_a  9.0060(10)
_cell_length_b  14.209(2)
_cell_length_c  10.908(2)
_cell_angle_alpha  90
_cell_angle_beta  117.880(10)
_cell_angle_gamma  90
_cell_volume  1233.9(2)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  2.559
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  896
_exptl_absorpt_coefficient_mu  11.84
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.7107
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Pt .68507(6) .01137(3) .19513(5) .0217(2)
 S1 .8090(4)   .1469(2)   .2886(4)   .0292(12)
 O1 .7110(13) .2118(7) .3269(11) .041(2)
 C11 .867(2)   .2040(12) .1689(18) .050(4)
 C12 1.006(2)   .1300(11) .4408(18) .047(4)
 S2 .5517(4)   .0110(2)   .3218(3)   .0243(11)
 O2 .6649(12) .0220(7) .4707(10) .040(2)
 C21 .3889(19) .0963(10) .2595(16) .039(3)
 C22 .4365(17) -.0959(9) .2908(15) .033(3)
 N1 .9449(15) -.0477(9) .1259(14) .038(5)
 O11 .7940(11) -.0036(7) .0690(10) .037(4)
 O12 1.0416(14) -.0391(10) .2474(13) .062(6)
 O13 .9761(16) -.0954(9) .0462(14) .059(6)
 N2 .6365(16) -.1813(8) .1037(14) .039(6)
 O21 .5507(11) -.1036(6) .0834(10) .032(4)
 O22 .7667(15) -.1908(8) .2092(14) .064(6)
 O23 .5751(18) -.2407(8) .0154(14) .070(6)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
 Pt S1 2.220(3)
 Pt S2 2.214(3)
 Pt O11 2.040(9)
 Pt O21 2.059(9)
 S1 O1 1.470(10)
 S1 C11 1.81(2)
 S1 C12 1.79(2)
 S2 O2 1.470(10)
 S2 C21 1.77(2)
 S2 C22 1.780(10)
 N1 O11 1.35(2)
 N1 O12 1.20(2)
 N1 O13 1.23(2)
 N2 O21 1.310(10)
 N2 O22 1.21(2)
 N2 O23 1.20(2)