#------------------------------------------------------------------------------
#$Date: 2008-01-26 13:05:32 +0000 (Sat, 26 Jan 2008) $
#$Revision: 19 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000227.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000227
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  2203
_journal_page_last  2205
loop_
_publ_author_name
 'Wang, J.-L.'
 'Sun, M.'
 'Miao, F.-M.'
 'Wu, S.-Y.'
 'Gong, F.-S.'
 'Duan, X.-H.'
_chemical_formula_sum  'C22 H36 Ag2 N8 S4'
_chemical_formula_weight  756.56
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_cell_length_a  12.032(3)
_cell_length_b  7.288(4)
_cell_length_c  16.933(4)
_cell_angle_alpha  90
_cell_angle_beta  90.44(4)
_cell_angle_gamma  90
_cell_volume  1485(2)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.691
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  764
_exptl_absorpt_coefficient_mu  1.6035
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Ag(1) -.04749(4) .16743(5) -.03575(3)
 S(1) .16871(9) .11540(10)
    .03363(7)
 S(2) -.02670(10)
    .3631(2) -.15426(6)
 N(1) .3253(4) -.0024(5) -.0773(3)
 N(2) -.0670(4) .3304(8) .0801(3)
 N(11) .4047(2) -.3645(3) -.10100(10)
 N(12) .5686(2) -.5428(3) -.08200(10)
 C(1) .2609(3) .0408(4) -.0314(3)
 C(2) .0282(3) .5418(6) -.1093(2)
 C(10) .3291(2) -.4324(4) .0360(2)
 C(11) .3342(2) -.4874(4) -.0510(2)
 C(12) .3994(2) -.4163(5) -.1879(2)
 C(13) .4558(3) -.6020(5) -.1999(2)
 C(14) .5750(2) -.6134(5) -.1643(2)
 C(21) .2806(3) -.4131(8) -.2197(2)
 C(22) .6043(4) -.8172(5) -.1622(3)
 C(23) .6593(3) -.5140(8) -.2160(2)
 C(00) .5254(2) -.3608(3) -.0783(2)
 H(001) .525(4) -.325(7) -.025(3)
 H(002) .566(4) -.275(6) -.116(3)
 H(101) .278(7) -.470(10)
   .057(5)
 H(102) .304(7) -.300(10)
   .042(5)
 H(111) .28(2) -.46(3) -.070(10)
 H(112) .381(5) -.599(8) -.058(3)
 H(131) .443(3) -.614(5) -.261(2)
 H(132) .404(6) -.700(10)
   -.173(4)
 H(211) .312(8) -.380(10)
   -.276(6)
 H(212) .249(4) -.315(8) -.194(3)
 H(213) .229(8) -.530(10)
   -.193(6)
 H(221) .570(10)
   -.82(2) -.129(7)
 H(222) .68(2) -.83(3) -.150(10)
 H(223) .591(5) -.895(8) -.217(3)
 H(231) .648(3) -.420(4) -.218(2)
 H(232) .734(9) -.550(10)
   -.196(6)
 H(233) .638(3) -.517(6) -.274(2)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
 Ag(1) S(1) 2.8710(10)
 Ag(1) N(2) 2.3070(10)
 S(1) C(1) 1.6600(10)
 N(1) C(1) 1.146(2)
 N(11) C(1) 1.5010(10)
 N(11) C(00) 1.4990(10)
 N(12) C(14) 1.4890(10)
 C(10) C(11) 1.5280(10)
 C(12) C(21) 1.5240(10)
 C(14) C(22) 1.5270(10)
 Ag(1) S(2) 2.4760(10)
 Ag(1) S(1) 2.5260(10)
 S(2) C(2) 1.6440(10)
 N(2) C(2) 1.151(2)
 N(11) C(12) 1.5190(10)
 N(12) C(10) 1.4640(10)
 C(12) C(13) 1.5280(10)
 C(13) C(14) 1.5540(10)
 C(14) C(23) 1.5270(10)
 N(12) C(00) 1.4260(10)
 C(00) H(001) 0.939(9)
 C(10) H(101) 0.763(7)
 C(11) H(111) 0.752(7)
 C(13) H(132) 1.05(2)
 C(21) H(212) 0.921(9)
 C(22) H(221) 0.700(8)
 C(22) H(223) 1.09(2)
 C(23) H(232) 0.993(9)
 C(00) H(002) 1.017(13)
 C(10) H(102) 0.999(8)
 C(11) H(112) 0.997(8)
 C(13) H(131) 1.053(11)
 C(21) H(211) 1.05(3)
 C(21) H(213) 1.13(2)
 C(22) H(222) 0.937(9)
 C(23) H(231) 0.699(7)
 C(23) H(233) 1.019(12)