#------------------------------------------------------------------------------
#$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $
#$Revision: 14 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000234.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000234
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  2220
_journal_page_last  2222
loop_
_publ_author_name
 'Prince, P.'
 'Fronczek, F.R.'
 'Gandour, R.D.'
_chemical_formula_sum  'C24 H20 O6 S2'
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
_symmetry_space_group_name_Hall  ?
_cell_length_a  8.4835(7)
_cell_length_b  11.801(2)
_cell_length_c  12.036(2)
_cell_angle_alpha  82.321(10)
_cell_angle_beta  76.560(8)
_cell_angle_gamma  73.261(8)
_cell_volume  1119.4(3)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.39
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  488
_exptl_absorpt_coefficient_mu  2.438
_diffrn_radiation_type  Cu
_diffrn_radiation_wavelength  1.54184
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 S1 .31557(5) .40685(3) .38225(4)
 S2 .88225(5) .99781(3) .17912(3)
 O1 .27350(10)
 .54638(9) .39484(9)
 O2 .2621(2) .36240(10)
    .49570(10)
 O3 .4855(2) .36680(10)
    .3237(2)
 O4 .89860(10)
 .86695(9) .14730(9)
 O5 1.0494(2) 1.00820(10)
   .14160(10)
 O6 .7480(2) 1.08040(10)
  .13520(10)
 C1 .4853(2) .64620(10)
    .31180(10)
 C2 .3447(2) .61730(10)
    .30370(10)
 C3 .2605(2) .66080(10)
    .21310(10)
 C4 .3253(2) .73280(10)
    .12730(10)
 C5 .5387(2) .84120(10)
    .04300(10)
 C6 .6770(2) .87540(10)
    .04890(10)
 C7 .7514(2) .83430(10)
    .14490(10)
 C8 .6952(2) .75930(10)
    .23040(10)
 C9 .5527(2) .72240(10)
    .22490(10)
 C10 .4721(2) .76510(10)
  .13020(10)
 C11 .1810(2) .39590(10)
  .29700(10)
 C12 .0138(2) .4062(2) .34600(10)
 C13 -.0936(2) .3972(2) .2796(2)
 C14 -.0374(3) .3787(2) .1649(2)
 C15 .1296(3) .3710(2) .1165(2)
 C16 .2416(3) .3778(2) .1818(2)
 C17 -.1552(3) .3671(2) .0937(2)
 C18 .8279(2) .98850(10)
  .32910(10)
 C19 .6950(2) 1.0733(2) .3841(2)
 C20 .6544(3) 1.0658(2) .5020(2)
 C21 .7446(2) .97480(10)
  .56600(10)
 C22 .8793(2) .89350(10)
  .50940(10)
 C23 .9235(2) .8984(2) .39110(10)
 C24 .6945(3) .9641(2) .6957(2)
 H1 .533(2) .6170(10)
  .3790(10)
 H3 .162(2) .6420(10)
  .2130(10)
 H4 .268(2) .766(2) .0640(10)
 H5 .490(2) .8620(10)
  -.0190(10)
 H6 .717(2) .9340(10)
  -.0040(10)
 H8 .759(2) .7280(10)
  .2900(10)
 H12 -.025(2) .417(2) .426(2)
 H13 -.199(3) .400(2) .313(2)
 H15 .178(3) .356(2) .033(2)
 H16 .359(3) .377(2) .150(2)
 H19 .625(3) 1.141(2) .339(2)
 H20 .568(2) 1.112(2) .537(2)
 H22 .941(2) .8340(10)
   .5660(10)
 H23 1.002(2) .844(2) .3580(10)
 H171 -.197(4) .301(3) .115(2)
 H172 -.113(3) .376(2) .023(2)
 H173 -.260(4) .455(3) .106(3)
 H241 .703(3) 1.030(2) .724(2)
 H242 .790(3) .906(2) .728(2)
 H243 .612(4) .943(3) .725(3)