data_2000266
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  1614
_journal_page_last  1617
_chemical_formula_sum  'Na C11 H23 Co O9 P3'
_symmetry_cell_setting  Orthorhombic
_symmetry_space_group_name_h-m  Pna21
_symmetry_space_group_name_hall  ?
_cell_length_a  18.195(8)
_cell_length_b  9.436(3)
_cell_length_c  11.316(5)
_cell_angle_alpha  90
_cell_angle_beta  90
_cell_angle_gamma  90
_cell_volume  1943
_cell_formula_units_z  4
_exptl_crystal_density_diffrn  1.621
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  976
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Co .59455(5) .19024(9) .694
 P1 .60490(10)
 -.0298(2) .7514(2)
 P2 .63350(10)
 .2749(2) .8618(2)
 P3 .47930(10)
 .1975(2) .7485(2)
 Na .4759(2) -.0562(3) .5067(3)
 O1 .6879(3) -.0809(7) .7302(6)
 O2 .5646(4) -.1220(5) .6500(6)
 O3 .5801(3) -.0802(5) .8698(6)
 O4 .6200(4) .4431(6) .8544(6)
 O5 .7219(3) .2660(8) .8539(7)
 O6 .6090(3) .2213(6) .9797(6)
 O7 .4452(4) .3485(6) .7101(7)
 O8 .4358(3) .0978(7) .6554(6)
 O9 .4547(3) .1634(6) .8685(6)
 C1 .7318(6) -.139(2) .820(2)
 C2 .5617(8) -.2742(9) .6600(10)
 C4 .6157(8) .5280(10)
   .9520(10)
 C5 .7653(6) .262(2) .9620(10)
 C7 .4216(8) .4490(10)
   .788(2)
 C8 .3580(5) .0800(10)
   .6680(10)
 C9 .6637(5) .3378(8) .6082(8)
 C10 .6859(5) .2000(10)
    .5832(8)
 C11 .6274(5) .1340(10)
    .5179(9)
 C12 .5675(5) .2331(9) .5158(8)
 C13 .5912(5) .3592(9) .5718(8)
 H1A .7787 -.1622 .7890
 H1B .7371 -.0721 .8821
 H1C .7090 -.2225 .8498
 H2A .5363 -.3125 .5942
 H2B .6102 -.3111 .6626
 H2C .5365 -.2992 .7308
 H4A .6075 .6228 .9278
 H4B .5762 .4970 1.0003
 H4C .6604 .5219 .9947
 H5A .8160 .2569 .9429
 H5B .7562 .3455 1.0070
 H5C .7518 .1813 1.0074
 H7A .4038 .5286 .7461
 H7B .3834 .4104 .8356
 H7C .4615 .4765 .8373
 H8A .3403 .0191 .6073
 H8B .3474 .0396 .7428
 H8C .3344 .1696 .6616
 H9 .6936 .4075 .6449
 H10 .7312 .1574 .6050
 H11 .6281 .0426 .4829
 H12 .5203 .2168 .4827
 H13 .5630 .4429 .5825