#------------------------------------------------------------------------------
#$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $
#$Revision: 14 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000269.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000269
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  1680
_journal_page_last  1683
_chemical_formula_sum  'C14 H20 N2 O6'
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_h-m  P21/c
_symmetry_space_group_name_hall  ?
_cell_length_a  11.3480(10)
_cell_length_b  4.8540(10)
_cell_length_c  14.6290(10)
_cell_angle_alpha  90
_cell_angle_beta  99.870(10)
_cell_angle_gamma  90
_cell_volume  793.9
_cell_formula_units_z  2
_exptl_crystal_density_diffrn  1.306
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  332
_diffrn_radiation_type  Cu
_diffrn_radiation_wavelength  1.54178
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 N(1) .0425(3) .1488(6) .1184(2)
 C(1) -.0341(3) .0427(8) .0372(2)
 C(2) .1009(3) -.0184(7) .1844(2)
 O(2) .0935(2) -.2699(5) .1786(2)
 C(3) .1751(3) .1276(7) .2629(2)
 C(4) .2343(3) .0020(7) .3365(2)
 C(5) .3021(3) .1658(8) .4128(2)
 O(5) .3365(3) .3962(5) .4056(2)
 O(6) .3209(2) .0242(6) .4919(2)
 C(7) .3838(4) .1712(9) .5736(3)
 C(8) .4013(4) -.0277(11) .6523(3)
 H(1) .048(3) .307(6) .128(2)
 H(11) -.094(3) .176(7) .014(2)
 H(12) -.079(3) -.113(7) .052(2)
 H(3) .173(2) .308(6) .259(2)
 H(4) .228(3) -.184(6) .344(2)
 H(71) .336(3) .329(8) .585(3)
 H(72) .457(3) .241(6) .555(2)
 H(81) .442(4) .080(9) .710(3)
 H(82) .450(4) -.171(9) .640(3)
 H(83) .315(4) -.111(11) .662(3)