data_2000271
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  1709
_journal_page_last  1711
loop_
_publ_author_name
 'Wang, S.-L.'
 'Lee, W.-C.'
_chemical_formula_moiety  'O1 V1,2(H2 As1 O4)'
_chemical_formula_sum  'H4 As2 O9 V1'
_chemical_formula_weight  348.8
_symmetry_cell_setting  tetragonal
_symmetry_space_group_name_H-M  'P 4/n c c {origin @  -1 @ n 1(c,n)}'
_symmetry_space_group_name_Hall  '-P 4a 2ac'
_cell_length_a  9.1310(10)
_cell_length_b  9.1310(10)
_cell_length_c  8.146(3)
_cell_angle_alpha  90
_cell_angle_beta  90
_cell_angle_gamma  90
_cell_volume  679.1(4)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  3.412
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  660
_exptl_absorpt_coefficient_mu  11.089
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 As(1) .46680(10)
    .53320(10)
    .2500 .0080(10)
 V(1) .2500 .2500 .1952(3) .0080(10)
 O(1) .3886(6) .6123(5) .0793(6) .0180(10)
 O(2) .4345(4) .3549(5) .2435(6) .0120(10)
 O(3) .2500 .2500 -.008(9) .015(2)
 H(1) .4436 .6853 .0463 .05