data_2000308
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  1310
_journal_page_last  1312
_chemical_formula_moiety  Os3Pt(H)2(CO)10,P(C6H11)3,P(C3H7)3
_chemical_formula_sum  'C37 H56 O10 P2 Os3 Pt1'
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_h-m  P21/c
_symmetry_space_group_name_hall  ?
_cell_length_a  10.678(2)
_cell_length_b  15.924(4)
_cell_length_c  27.237(5)
_cell_angle_alpha  90
_cell_angle_beta  100.92(2)
_cell_angle_gamma  90
_cell_volume  4547(2)
_cell_formula_units_z  4
_exptl_crystal_density_diffrn  2.17
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  2776
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Pt .37918(7) .20832(4) .07005(3)
 Os(1) .36448(7) .16819(4) .16585(3)
 Os(2) .28384(7) .32698(4) .13393(3)
 Os(3) .54048(7) .31906(4) .19064(3)
 P(1) .3765(4) .2376(3) -.0145(2)
 P(2) .7546(4) .2843(3) .2271(2)
 O(1) .2766(14) .1673(9) .2646(6)
 O(2) .5020(14) .0027(9) .1850(5)
 O(3) .1176(15) .0958(9) .1094(6)
 O(4) .2938(16) .5069(11) .1004(6)
 O(5) .2034(14) .3718(9) .2299(6)
 O(6) .0142(16) .2919(9) .0833(6)
 O(7) .5396(14) .5077(9) .1932(5)
 O(8) .4638(13) .3138(7) .2939(5)
 O(9) .6278(14) .3337(8) .0902(6)
 O(10) .4769(14) .0340(9) .0692(5)
 C(1) .3122(19) .1689(11) .2271(8)
 C(2) .4468(17) .0662(11) .1774(7)
 C(3) .213(2) .1240(10)
    .1320(10)
 C(4) .288(2) .4370(10)
    .1140(10)
 C(5) .2366(18) .3525(11) .1932(7)
 C(6) .123(2) .3050(10)
    .1030(10)
 C(7) .5452(17) .4336(12) .1931(7)
 C(8) .4883(18) .3169(11) .2544(7)
 C(9) .5894(18) .3262(11) .1273(7)
 C(10) .4401(17) .1008(11) .0701(7)
 C(11) .7708(17) .2286(11) .2878(7)
 C(12) .710(2) .1410(10)
  .2800(10)
 C(13) .904(2) .2200(10)
  .3190(10)
 C(14) .8374(18) .2302(11) .1822(7)
 C(15) .975(2) .1990(10)
  .2060(10)
 C(16) .766(2) .1560(10)
  .1540(10)
 C(17) .8605(19) .3766(12) .2438(8)
 C(18) .874(2) .4300(10)
  .1970(10)
 C(19) .815(2) .4290(10)
  .2840(10)
 C(111) .2997(14) .1497(9) -.0537(6)
 C(112) .1881(18) .1108(11) -.0347(7)
 C(113) .1390(18) .0331(11) -.0638(7)
 C(114) .1031(19) .0518(12) -.1173(7)
 C(115) .2029(19) .0901(12) -.1382(7)
 C(116) .2550(18) .1717(11) -.1082(7)
 C(121) .2942(17) .3349(11) -.0412(7)
 C(122) .1602(19) .3364(12) -.0354(7)
 C(123) .085(2) .416(2) -.0590(10)
 C(124) .155(3) .492(2) -.0390(10)
 C(125) .287(3) .493(2) -.0420(10)
 C(126) .3610(18) .4135(12) -.0187(7)
 C(131) .5384(16) .2471(10) -.0252(7)
 C(132) .625(2) .1750(10)
   -.0050(10)
 C(133) .767(3) .191(2) -.0070(10)
 C(134) .780(3) .208(2) -.0590(10)
 C(135) .699(3) .283(2) -.0770(10)
 C(136) .557(2) .2650(10)
   -.0750(10)
 H(1) .34160 .32050 .07390
 H(2) .53200 .20380 .18380
 H(11) .72558 .26081 .31072
 H(12A) .61817 .14645 .26364
 H(12B) .75540 .10856 .25673
 H(12C) .71826 .11105 .31239
 H(13A) .94025 .27800 .32561
 H(13B) .91246 .19045 .35176
 H(13C) .95631 .18898 .29805
 H(14) .84411 .27010 .15452
 H(15A) .96801 .15957 .23331
 H(15B) 1.02663 .24914 .21972
 H(15C) 1.01960 .17056 .18129
 H(16A) .68283 .17768 .1352
 H(16B) .81134 .12728 .12955
 H(16C) .75031 .11415 .17919
 H(17) .94701 .35691 .26057
 H(18A) .78799 .44987 .18047
 H(18B) .93112 .47993 .20664
 H(18C) .91112 .39399 .17349
 H(19A) .72572 .44871 .27042
 H(19B) .81380 .39384 .31431
 H(19C) .87121 .47905 .29346
 H(111) .36453 .10451 -.05411
 H(112A) .21509 .09697 .00155
 H(112B) .11766 .15305 -.03873
 H(113A) .06454 .00947 -.05102
 H(113B) .20877 -.00971 -.05943
 H(114A) .031 .09286 -.12118
 H(114B) .07314 -.00054 -.13617
 H(115A) .17055 .10431 -.17412
 H(115B) .27391 .04854 -.13599
 H(116A) .3279 .19578 -.12185
 H(116B) .18579 .21478 -.111
 H(121) .29621 .33766 -.0777
 H(122A) .15891 .33468 .00118
 H(122B) .11661 .28509 -.05164
 H(123A) -.00293 .41543 -.05159
 H(123B) .07841 .41498 -.09647
 H(124A) .15152 .49611 -.00233
 H(124B) .11218 .54265 -.05629
 H(125A) .32957 .54421 -.02582
 H(125B) .29023 .49355 -.07842
 H(126A) .45089 .41419 -.02425
 H(126B) .36186 .41317 .01812
 H(131) .57805 .29862 -.00782
 H(132A) .61514 .16218 .02978
 H(132B) .59665 .12523 -.02688
 H(133A) .82128 .14216 .00667
 H(133B) .79521 .24192 .01317
 H(134A) .74531 .15916 -.07980
 H(134B) .87115 .21717 -.06167
 H(135A) .71090 .29913 -.11177
 H(135B) .72860 .32987 -.05385
 H(136A) .5284 .21538 -.09679
 H(136B) .50277 .31473 -.08858