#------------------------------------------------------------------------------
#$Date: 2008-01-26 13:05:32 +0000 (Sat, 26 Jan 2008) $
#$Revision: 19 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000365.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000365
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  2172
_journal_page_last  2174
loop_
_publ_author_name
 'Giordano, F.'
_chemical_formula_sum  'C17 H15 N1 O4'
_chemical_formula_weight  297.3
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'C 2/c'
_symmetry_space_group_name_Hall  ?
_cell_length_a  26.157(5)
_cell_length_b  5.9790(10)
_cell_length_c  19.492(3)
_cell_angle_alpha  90.
_cell_angle_beta  97.790(10)
_cell_angle_gamma  90.
_cell_volume  3020.0(10)
_cell_formula_units_Z  8
_exptl_crystal_density_diffrn  1.31
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  1248
_exptl_absorpt_coefficient_mu  0.736
_diffrn_radiation_type  Cu
_diffrn_radiation_wavelength  1.5418
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 O(1) .04280(10)
      .5042(4) .32700(10)
 O(2) .08140(10)
      .3919(4) .29130(10)
 O(3) .14940(10)
      -.0258(6) .39970(10)
 O(4) .16510(10)
      .3377(6) .3891(2)
 N .04640(10)
      .1494(5) .3655(2)
 C(1) .02410(10)
      .3394(5) .3641(2)
 C(2) .08910(10)
      .1750(6) .3248(2)
 C(3) -.01900(10)
       .4042(5) .4002(2)
 C(4) -.03420(10)
       .2537(6) .4480(2)
 C(5) -.0747(2) .3125(7) .4840(2)
 C(6) -.0996(2) .5149(7) .4724(2)
 C(7) -.0845(2) .6586(7) .4243(2)
 C(8) -.0440(2) .6058(6) .3881(2)
 C(9) .08840(10)
      -.0040(6) .2690(2)
 C(10) .13540(10)
       -.0028(5) .2310(2)
 C(11) .14420(10)
       .1740(6) .1883(2)
 C(12) .1866(2) .1682(7) .1522(2)
 C(13) .2194(2) -.0123(7) .1581(2)
 C(14) .2110(2) -.1882(7) .2009(2)
 C(15) .1687(2) -.1842(6) .2373(2)
 C(16) .13900(10)
       .1794(7) .3743(2)
 C(17) .1958(2) -.0571(9) .4464(3)
 H(1) -.016 .116 .457
 H(2) -.086 .210 .517
 H(3) -.128 .551 .497
 H(4) -.102 .801 .416
 H(5) -.033 .710 .356
 H(6) .058 .016 .237
 H(7) .087 -.147 .291
 H(8) .121 .297 .183
 H(9) .193 .288 .123
 H(10) .249 -.017 .134
 H(11) .234 -.313 .206
 H(12) .163 -.306 .269
 H(13) .201 -.200 .464
 H(14) .226 -.008 .426
 H(15) .196 .046 .488