data_2000382
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  2209
_journal_page_last  2211
loop_
_publ_author_name
 'Deshayes, L.'
 'Keller, N.'
 'Lance, M.'
 'Nierlich, M.'
 'Vigner, D.'
_chemical_formula_moiety  'C10 H30 O7 S5 U1,2(B1 F4)'
_chemical_formula_sum  'C10 H30 B2 F8 O7 S5 U1'
_chemical_formula_weight  834.28
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_cell_length_a  11.455(3)
_cell_length_b  12.401(4)
_cell_length_c  12.549(3)
_cell_angle_alpha  72.64(2)
_cell_angle_beta  64.20(2)
_cell_angle_gamma  62.74(2)
_cell_volume  1415(2)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  3.914
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  1600
_exptl_absorpt_coefficient_mu  11.73
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 U .21479(5) .47438(4) .22685(4)
 S1 .2265(4) .7413(3) .0124(3)
 S2 .2642(3) .4338(3) -.0591(3)
 S3 .2719(3) .1762(3) .2223(3)
 S4 .2931(3) .2917(3) .4902(3)
 S5 .1752(5) .6366(4) .4416(4)
 F1 .2189(9) .9110(10)
      .7536(8)
 F2 .1280(10)
      .7887(9) .7490(10)
 F3 .1680(10)
      .9240(10)
        .5957(8)
 F4 -.0010(10)
    .0190(10)
      .2350(10)
 F5 .4858(9) .8266(9) .1770(8)
 F6 .3200(10)
      .1740(10)
        .8250(10)
 F7 .4330(10)
      .2810(10)
        .6733(9)
 F8 .4790(10)
      .9183(9) .3132(9)
 O1 .2424(9) .6622(7) .1296(7)
 O2 .1818(8) .5182(7) .0400(6)
 O3 .1752(8) .3107(6) .2084(7)
 O4 .2200(8) .3271(7) .4010(7)
 O5 .2657(8) .5461(7) .3505(7)
 O11 .0316(8) .5541(8) .2944(8)
 O12 .3979(7) .3939(7) .1574(7)
 C1 .2830(10)
      .8610(10)
        .0010(10)
 C2 .039(2) .8290(10)
        .0500(10)
 C3 .397(2) .4900(10)
        -.166(2)
 C4 .1490(10)
      .489(2) -.1440(10)
 C5 .279(2) .1120(10)
        .1070(10)
 C6 .1620(10)
      .1070(10)
        .3470(10)
 C7 .473(2) .201(2) .411(2)
 C8 .240(2) .1730(10)
        .5920(10)
 C9 .189(2) .7760(10)
        .3770(10)
 C10 .284(2) .594(2) .528(2)
 B1 .133(2) .9000(10)
        .7130(10)
 B2 .450(2) .176(2) .750(2)