#------------------------------------------------------------------------------
#$Date: 2008-11-20 19:58:43 +0000 (Thu, 20 Nov 2008) $
#$Revision: 481 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000388.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000388
_journal_name_full 'Acta Crystallographica Section C'
_journal_year  1992
_journal_volume 48
_journal_page_first  2222
_journal_page_last  2224
loop_
_publ_author_name
 'Barnes, C.L.'
 'Soderquist, J.A.'
_chemical_formula_sum  'C19 H22 O1 Si1'
_chemical_formula_weight  294.5
_symmetry_cell_setting  orthorhombic
_symmetry_space_group_name_H-M  'P 21 21 21'
_symmetry_space_group_name_Hall  ?
_cell_length_a  8.896(3)
_cell_length_b  11.006(3)
_cell_length_c  17.310(6)
_cell_angle_alpha  90.
_cell_angle_beta  90.
_cell_angle_gamma  90.
_cell_volume  1695(2)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.154
_exptl_crystal_density_meas  1.150
_exptl_crystal_F_000  632
_exptl_absorpt_coefficient_mu  0.10
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Si1 .1587(2) .0432(2) .06410(10)
           .0480(10)
 C2 .2517(6) .0468(5) .1636(3) .048(3)
 C3 .1274(6) .0483(6) .2253(3) .057(3)
 C4 .0300(6) -.0611(6) .2221(3) .059(4)
 O4 .0296(5) -.1377(4) .2731(3) .086(3)
 C5 -.0672(7) -.0771(6) .1509(3) .072(4)
 C6 .0211(6) -.0875(5) .0758(3) .056(4)
 C7 .0618(7) .1891(5) .0419(3) .062(4)
 C8 .2992(6) .0058(5) -.0111(3) .062(4)
 C9 .3665(7) .1452(5) .1709(3) .047(3)
 C10 .3306(7) .2658(6) .1862(3) .062(4)
 C11 .4418(10) .3547(6) .1889(4) .074(5)
 C12 .5889(9) .3253(7) .1785(4) .075(5)
 C13 .6255(7) .2068(8) .1622(3) .074(5)
 C14 .5181(7) .1173(6) .1586(3) .057(4)
 C15 -.0735(7) -.1062(5) .0042(3) .057(4)
 C16 -.2107(7) -.0515(7) -.0083(3) .065(4)
 C17 -.2896(7) -.0711(7) -.0765(4) .077(5)
 C18 -.2331(9) -.1432(7) -.1339(4) .077(5)
 C19 -.0981(10) -.1983(6) -.1228(4) .077(5)
 C20 -.0190(8) -.1812(5) -.0546(4) .070(4)
 H2 .318 -.034 .172 .06
 H3A .058 .128 .217 .06
 H3B .179 .053 .282 .06
 H5A -.133 -.159 .158 .06
 H5B -.141 .000 .147 .06
 H6 .084 -.171 .081 .06
 H7A -.019 .209 .087 .06
 H7B .005 .182 -.013 .06
 H7C .144 .262 .039 .06
 H8A .354 -.079 .003 .06
 H8B .382 .077 -.014 .06
 H8C .244 -.003 -.066 .06
 H10 .215 .291 .196 .06
 H11 .411 .448 .199 .06
 H12 .675 .394 .183 .06
 H13 .742 .183 .152 .06
 H14 .551 .025 .146 .06
 H16 -.257 .007 .035 .06
 H17 -.398 -.028 -.084 .06
 H18 -.295 -.156 -.187 .06
 H19 -.052 -.256 -.167 .06
 H20 .087 -.227 -.047 .06