#------------------------------------------------------------------------------
#$Date: 2008-01-26 13:05:32 +0000 (Sat, 26 Jan 2008) $
#$Revision: 19 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000397.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000397
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  2240
_journal_page_last  2244
loop_
_publ_author_name
 'Macias, F.A.'
 'Zubia, E.'
 'Quijano, L.'
 'Fronczek, F.R.'
 'Fischer, N.H.'
_chemical_formula_sum  'C24 H30 O8'
_chemical_formula_weight  446.5
_symmetry_cell_setting  orthorhombic
_symmetry_space_group_name_H-M  'P 21 21 21'
_symmetry_space_group_name_Hall  ?
_cell_length_a  5.5333(5)
_cell_length_b  12.5520(7)
_cell_length_c  31.723(2)
_cell_angle_alpha  90.
_cell_angle_beta  90.
_cell_angle_gamma  90.
_cell_volume  2203.2(2)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.346
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  952
_exptl_absorpt_coefficient_mu  0.80
_diffrn_radiation_type  Cu
_diffrn_radiation_wavelength  1.54184
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 O3 .6922(2) -.12277(7) .70498(2)
 O7 .21020(10)
    -.05107(8) .78727(2)
 O15 .9366(2) .22988(7) .61519(3)
 O17 .6514(2) .19228(7) .54991(2)
 O19 .3083(2) .04134(8) .55249(2)
 O27 .1911(2) .03801(8) .95149(3)
 O29 .5226(2) .19364(7) .95282(3)
 O31 .8085(2) .23066(7) .88704(3)
 C1 .5083(2) .01830(8) .74213(3)
 C2 .5068(2) -.04352(9) .70018(3)
 C4 .6648(3) -.15950(10)
        .74723(3)
 C5 .6239(2) -.06020(9) .77385(3)
 C6 .4354(2) -.07174(8) .80860(3)
 C8 .2568(2) .03830(10)
       .76052(4)
 C9 .5495(2) .01856(9) .66023(3)
 C10 .7323(2) .09535(9) .65790(3)
 C11 .7641(2) .15346(9) .62095(3)
 C12 .6134(2) .13562(9) .58629(3)
 C13 .4363(2) .05640(10)
        .58838(3)
 C14 .4035(2) -.00068(9) .62556(3)
 C16 1.0954(2) .25200(10)
         .64917(4)
 C18 .4661(3) .26810(10)
        .54067(4)
 C20 .1207(3) -.03710(10)
         .55252(4)
 C21 .4649(2) .00088(8) .84648(3)
 C22 .3124(2) -.01565(9) .88093(3)
 C23 .3278(2) .04940(10)
        .91609(3)
 C24 .4963(2) .13267(9) .91731(3)
 C25 .6486(2) .14899(9) .88290(3)
 C26 .6326(2) .08324(9) .84769(3)
 C28 .0034(3) -.04000(10)
         .95100(4)
 C30 .3435(3) .27450(10)
        .95758(5)
 C32 .9787(3) .24680(10)
        .85400(4)