#------------------------------------------------------------------------------
#$Date: 2008-11-20 19:58:43 +0000 (Thu, 20 Nov 2008) $
#$Revision: 481 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000421.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000421
_journal_name_full 'Acta Crystallographica Section C'
_journal_year  1992
_journal_volume 48
_journal_page_first  1917
_journal_page_last  1920
loop_
_publ_author_name
 'Slougui, A.'
 'Perrin, A.'
 'Sergent, M.'
_chemical_formula_moiety  'Br9 Re6 S5,K1'
_chemical_formula_sum  'Br9 K1 Re6 S5'
_chemical_formula_weight  2035.8
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'C 2/c'
_symmetry_space_group_name_Hall  ?
_cell_length_a  16.914(11)
_cell_length_b  9.526(4)
_cell_length_c  17.671(11)
_cell_angle_alpha  90.
_cell_angle_beta  127.41(2)
_cell_angle_gamma  90.
_cell_volume  2261.5
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  5.979
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  3456
_exptl_absorpt_coefficient_mu  39.423
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Re1 .05305(3) .07929(6) .11710(3)
 Re2 .03298(3) -.17530(6) .05552(3)
 Re3 -.12232(3) -.01296(6) -.02419(3)
 Br1 .13024(8) .1817(2) .27946(8)
 Br2 .07880(10)
     .4143(2) .63270(10)
 Br3 -.28604(8) .0396(2) .44887(9)
 S1 -.13950(10)
     .2603(2) .41680(10)
 S2 .10190(10)
    .2362(2) .46630(10)
 S3 .1965(2) .0787(3) .6864(2)
 S4 -.4649(2) .3972(3) .3613(2)
 K .500 -.0330(8) .250