#------------------------------------------------------------------------------
#$Date: 2008-11-20 19:58:43 +0000 (Thu, 20 Nov 2008) $
#$Revision: 481 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000422.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000422
_journal_name_full 'Acta Crystallographica Section C'
_journal_year  1992
_journal_volume 48
_journal_page_first  1920
_journal_page_last  1923
loop_
_publ_author_name
 'Fettouhi, M.'
 'Ouahab, L.'
 'Grandjean, D.'
 'Mousdis, G.'
 'Delhaes, P.'
_chemical_formula_moiety  'C28 H16 S24,C4 N4 Pt1,2(H2 O1)'
_chemical_formula_sum  'C32 H20 N4 O2 Pt1 S24'
_chemical_formula_weight  1457.2
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
_symmetry_space_group_name_Hall  ?
_cell_length_a  8.569(9)
_cell_length_b  9.991(5)
_cell_length_c  14.811(5)
_cell_angle_alpha  108.84(3)
_cell_angle_beta  95.10(4)
_cell_angle_gamma  90.37(7)
_cell_volume  1194.5
_cell_formula_units_Z  1
_exptl_crystal_density_diffrn  2.03
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  718
_exptl_absorpt_coefficient_mu  4.016
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Pt 0 0 0
 C1 .0490(10)
      -.1670(10)
      .0408(7)
 C2 .2150(10)
      .0880(10)
        .0498(7)
 N1 .0770(10)
      -.2640(10)
      .0628(7)
 N2 .3350(10)
      .1390(10)
        .0794(7)
 S1 .3826(3) .1555(2) .3879(2)
 S2 .1994(3) -.0772(3) .4098(2)
 S3 .2924(3) .0377(2) .6376(2)
 S4 .4713(3) .2770(2) .6176(2)
 S5 .3596(3) .1547(3) .8562(2)
 S6 .5406(4) .3992(3) .8363(2)
 C3 .3160(10)
      .0734(9) .4642(6)
 C4 .3560(10)
      .1254(9) .5623(6)
 C5 .2850(10)
      .0400(10)
        .2854(7)
 C6 .2010(10)
      -.0670(10)
      .2954(7)
 C7 .4580(10)
      .2718(9) .7319(7)
 C8 .3770(10)
      .1611(9) .7412(6)
 C9 .5210(10)
      .2850(10)
        .9090(7)
 S7 .0625(3) .3652(3) .6736(2)
 S8 -.2118(3) .5460(3) .6953(2)
 S9 -.2961(3) .4443(2) .4674(2)
 S1O -.0139(3) .2668(2) .4400(2)
 S11 -.1261(3) .1322(3) .2261(2)
 S12 -.4140(3) .3036(3) .2549(2)
 C1O -.0980(10)
     .4250(8) .6171(6)
 C11 .0260(10)
    .4690(10)
      .7886(7)
 C12 -.0970(10)
     .5510(10)
       .7990(7)
 C13 -.1320(10)
     .3812(8) .5206(6)
 C14 -.2710(10)
     .3335(9) .3522(6)
 C15 -.1430(10)
     .2541(9) .3403(6)
 C16 -.2780(10)
     .2120(10)
       .1688(7)
 O1W .2180(10)
    .4700(10)
      -.0097(7)
 H1 .2911 .0531 .2162
 H2 .1368 -.1440 .2345
 H3 .6298 .2306 .9127
 H4 .4974 .3496 .9810
 H5 .1026 .4670 .8502
 H6 -.1249 .6175 .8686
 H7 -.3423 .1296 .1098
 H8 -.2237 .2878 .1409