#------------------------------------------------------------------------------
#$Date: 2008-01-26 13:05:32 +0000 (Sat, 26 Jan 2008) $
#$Revision: 19 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000452.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000452
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  2002
_journal_page_last  2004
loop_
_publ_author_name
 'Lane, H.P.'
 'McAuliffe, C.A.'
 'Pritchard, R.G.'
_chemical_formula_moiety  'C18 H16 O1 P1,Br1'
_chemical_formula_sum  'C18 H16 Br1 O1 P1'
_chemical_formula_weight  359.2
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 21/n'
_symmetry_space_group_name_Hall  ?
_cell_length_a  9.540(3)
_cell_length_b  17.763(5)
_cell_length_c  10.390(6)
_cell_angle_alpha  90.
_cell_angle_beta  106.91(4)
_cell_angle_gamma  90.
_cell_volume  1685.0(10)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.416
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  728
_exptl_absorpt_coefficient_mu  2.504
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Br(1) .23830(10)
       .45541(7) .74450(10)
 P(1) .4472(2) .34920(10)
         .5081(2)
 O(1) .4676(6) .4024(3) .6304(6)
 C(1) .3503(8) .2659(5) .5240(10)
 C(2) .3550(10)
     .2394(6) .6500(10)
 C(3) .2860(10)
     .1729(6) .6650(10)
 C(4) .2140(10)
     .1317(5) .5550(10)
 C(5) .2080(10)
     .1584(6) .4320(10)
 C(6) .2760(10)
     .2254(6) .4130(10)
 C(7) .3517(8) .3940(4) .3562(8)
 C(8) .4180(10)
     .4113(5) .2590(10)
 C(9) .3430(10)
     .4464(7) .1410(10)
 C(10) .1970(10)
      .4613(6) .1170(10)
 C(11) .1300(10)
      .4464(7) .2150(10)
 C(12) .2060(10)
      .4115(6) .3340(10)
 C(13) .6291(8) .3259(5) .5519(8)
 C(14) .7390(10)
      .3761(6) .5590(10)
 C(15) .8840(10)
      .3612(9) .5710(10)
 C(16) .9180(10)
      .2920(10)
        .5370(10)
 C(17) .8130(10)
      .2390(7) .4890(10)
 C(18) .6650(10)
      .2557(6) .4760(10)