data_2000473
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  2036
_journal_page_last  2039
loop_
_publ_author_name
 'Bryant, G.L.'
 'King, J.A.'
_chemical_formula_moiety  'C7 H11 N2,Cl1'
_chemical_formula_sum  'C7 H11 Cl1 N2'
_chemical_formula_weight  158.6
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'C 2/c'
_symmetry_space_group_name_Hall  ?
_cell_length_a  17.113(3)
_cell_length_b  7.460(2)
_cell_length_c  14.570(3)
_cell_angle_alpha  90.
_cell_angle_beta  120.840(10)
_cell_angle_gamma  90.
_cell_volume  1597.0
_cell_formula_units_Z  8
_exptl_crystal_density_diffrn  1.319
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  672
_exptl_absorpt_coefficient_mu  0.403
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Cl(1) .34710(10)
       .07740(10)
       .52860(10)
          .0190(10)
 N(1) .29850(10)
      -.3344(3) .2029(2) .0210(10)
 C(1) .3830(2) -.2639(3) .2598(2) .0200(10)
 C(2) .4296(2) -.2627(3) .3687(2) .0190(10)
 C(3) .38970(10)
      -.3360(3) .4252(2) .0170(10)
 N(2) .43440(10)
      -.3436(3) .53200(10)
          .0180(10)
 C(4) .5215(2) -.2540(4) .5981(2) .0220(10)
 C(5) .3892(2) -.4085(4) .5872(2) .0230(10)
 C(6) .2992(2) -.4051(3) .3617(2) .0200(10)
 C(7) .2587(2) -.4026(4) .2533(2) .0220(10)
 H(1B) .2695 -.3355 .1309 .080
 H(1A) .4109 -.2133 .2227 .080
 H(2A) .4899 -.2127 .4076 .080
 H(4C) .5412 -.2015 .5536 .080
 H(4B) .5658 -.3395 .6456 .080
 H(4A) .5146 -.1616 .6398 .080
 H(5C) .3625 -.5386 .5612 .080
 H(5B) .4376 -.4104 .6665 .080
 H(5A) .3403 -.3392 .5737 .080
 H(6A) .2681 -.4526 .3956 .080
 H(7A) .1975 -.4496 .2112 .080