data_2000482
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  2055
_journal_page_last  2057
loop_
_publ_author_name
 'Soriano-Garcia, M.'
_chemical_formula_sum  'C20 H26 N2 O1'
_chemical_formula_weight  310.4
_symmetry_cell_setting  orthorhombic
_symmetry_space_group_name_H-M  'P 21 21 21'
_symmetry_space_group_name_Hall  ?
_cell_length_a  10.485(5)
_cell_length_b  16.892(8)
_cell_length_c  19.750(6)
_cell_angle_alpha  90.
_cell_angle_beta  90.
_cell_angle_gamma  90.
_cell_volume  3498(2)
_cell_formula_units_Z  8
_exptl_crystal_density_diffrn  1.18
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  1344
_exptl_absorpt_coefficient_mu  0.068
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.7107
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 C1A .4834(7) 1.1926(5) .8254(4) .072(3)
 C2A .5012(9) 1.2562(5) .8817(4) .079(4)
 C3A .4280(8) 1.3291(4) .8639(4) .091(4)
 C4A .2865(8) 1.3083(4) .8524(4) .068(3)
 C5A .2680(7) 1.2222(4) .8730(3) .052(2)
 N6A .3153(6) 1.2134(3) .9430(2) .054(2)
 C7A .2638(6) 1.1472(4) .9809(3) .056(3)
 C8A .3094(7) 1.0637(4) .9637(3) .052(2)
 C9A .2969(6) 1.0393(4) .8906(3) .042(2)
 C10A .2686(5) .9594(4) .8689(3) .037(2)
 C11A .2434(6) .8883(4) .9041(3) .039(2)
 C12A .2163(6) .8233(3) .8672(3) .044(2)
 C13A .2189(7) .8220(4) .7965(4) .051(3)
 C14A .2477(7) .8902(4) .7616(3) .054(3)
 C15A .2706(6) .9589(4) .7976(3) .043(2)
 N16A .2976(5) 1.0349(3) .7776(3) .1048(2)
 C17A .3138(6) 1.0832(4) .8338(3) .042(2)
 C18A .3390(7) 1.1707(4) .8227(4) .054(3)
 C19A .4527(7) 1.2227(5) .9464(4) .074(3)
 C20A .1911(11) 1.3641(5) .8875(5) .092(4)
 C21A .0563(9) 1.3579(5) .8656(5) .118(5)
 O1A .1803(5) .7503(3) .8945(2) .057(2)
 C22A .1846(8) .7428(4) .9663(3) .073(3)
 C1B .9085(7) .9326(4) .9496(3) .060(3)
 C2B .8366(8) 1.0106(5) .9582(4) .073(3)
 C3B .9043(9) 1.0746(5) .9192(5) .093(4)
 C4B .9250(7) 1.0469(4) .8463(4) .079(4)
 C5B .8420(6) .9747(4) .8351(4) .049(3)
 N6B .7118(5) .9960(3) .8558(3) .050(2)
 C7B .6085(7) .9532(4) .8240(4) .060(3)
 C8B .5805(6) .8703(4) .8510(4) .055(3)
 C9B .6906(6) .8152(4) .8594(3) .044(2)
 C10B .6741(7) .7317(4) .8660(3) .048(2)
 C11B .5652(8) .6830(4) .8642(3) .055(3)
 C12B .5818(10) .6034(5) .8753(4) .070(4)
 C13B .6979(11) .5706(4) .8880(4) .073(4)
 C14B .8060(9) .6174(4) .8911(3) .061(3)
 C15B .7937(8) .6983(4) .8794(3) .051(3)
 N16B .8814(5) .7597(3) .8808(3) .051(2)
 C17B .8180(7) .8309(4) .8675(3) .047(2)
 C18B .8948(6) .9057(4) .8749(3) .047(2)
 C19B .7040(7) 1.0031(5) .9294(4) .079(3)
 C20B .9005(8) 1.1137(5) .7963(5) .098(4)
 C21B .9530(9) 1.1041(6) .7334(6) .171(7)
 O1B .4826(7) .5481(3) .8723(3) .088(3)
 C22B .3674(10) .5759(5) .8477(5) .103(5)
 H1AA .5116 1.2133 .7827 ?
 H1AB .5319 1.1461 .8364 ?
 H2A .5897 1.2699 .8860 ?
 H3AA .4348 1.366 .9002 ?
 H3AB .4627 1.3518 .8233 ?
 H4A .2676 1.3161 .8054 ?
 H5A .1805 1.2054 .8729 ?
 H7AA .2827 1.1563 1.0277 ?
 H7AB .1730 1.1480 .9749 ?
 H8AA .2608 1.0270 .9904 ?
 H8AB .3978 1.0600 .9758 ?
 H11A .2453 .8863 .9526 ?
 H13A .2006 .7740 .7724 ?
 H14A .2519 .8899 .7130 ?
 H16A .308(5)   1.052(3)   .742(3)   ?
 H18A .3071 1.1811 .7780 ?
 H19A .4736 1.2579 .9829 ?
 H19B .4916 1.1721 .9543 ?
 H20A .2185 1.4175 .8795 ?
 H20B .1938 1.3532 .9352 ?
 H21A .0265 1.3048 .8725 ?
 H21B .0501 1.3710 .8184 ?
 H21C .0050 1.3939 .8915 ?
 H22A .1637 .6896 .9791 ?
 H22B .1243 .7787 .9862 ?
 H22C .2688 .7555 .9821 ?
 H1BA .9968 .9403 .9607 ?
 H1BB .8728 .8930 .9788 ?
 H2B .8323 1.0230 1.0056 ?
 H3BA .8536 1.1219 .9191 ?
 H3BB .9853 1.0853 .9400 ?
 H4B 1.0121 1.0319 .8384 ?
 H5B .8399 .9584 .7885 ?
 H7BA .5325 .9843 .8290 ?
 H7BB .6289 .9480 .7769 ?
 H8BA .5212 .8458 .8204 ?
 H8BB .5412 .8765 .8946 ?
 H11B .4823 .7047 .8556 ?
 H13B .7049 .5146 .8951 ?
 H14B .8877 .5947 .9011 ?
 H16B .963(5)   .753(3)   .881(3)   ?
 H18B .9768 .8915 .8570 ?
 H19C .6555 1.0494 .9409 ?
 H19D .6631 .9571 .9479 ?
 H20C .9348 1.1615 .8153 ?
 H20D .8099 1.1191 .7910 ?
 H21D 1.0421 1.0920 .7378 ?
 H21E .9430 1.1518 .7075 ?
 H21F .9107 1.0612 .7107 ?
 H22D .3008 .5656 .8799 ?
 H22E .3482 .5497 .8058 ?
 H22F .3736 .6319 .8400 ?