#------------------------------------------------------------------------------
#$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $
#$Revision: 14 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000508.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000508
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1756
_journal_page_last  1759
loop_
_publ_author_name
 'Chattopadahay, T.K.'
 'Palmer, R.A.'
 'Lisgarten, J.N.'
 'Wyns, L.'
 'Gazi, D.M.'
_chemical_formula_moiety  'C10 H24 Br1 Cl1 Cr1 N4,Br1'
_chemical_formula_sum  'C10 H24 Br2 Cl1 Cr1 N4'
_chemical_formula_weight  447.7
_symmetry_cell_setting  tetragonal
_symmetry_space_group_name_H-M  'P 42/m'
_symmetry_space_group_name_Hall  '-P 4c'
_cell_length_a  7.7750(10)
_cell_length_b  7.7750(10)
_cell_length_c  13.686(2)
_cell_angle_alpha  90.
_cell_angle_beta  90.
_cell_angle_gamma  90.
_cell_volume  827.2(3)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.81
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  446.0
_exptl_absorpt_coefficient_mu  5.61
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Br(1) .3012(10) .2466(8) .0 .0420(10)
 Cr(1) .5 .0 .0 .0240(10)
 Cl(1) .326(3)   .253(2)   .0 .0390(10)
 N(1) .6470(4) .1027(5) -.1113(3) .0390(10)
 C(2) .5425(6) .0878(7) -.2009(3) .036(2)
 C(3) .7174(6) .2783(6) -.0944(4) .049(3)
 C(4) .8167(10) .2893(9) .0 .051(3)
 Br(2) .0 .0 .25 .052(5)
 H(11) .7530(4) .0133(5) -.1150(3) ?
 H(21) .4452(6) .1905(7) -.2040(3) ?
 H(22) .6275(6) .0966(7) -.2632(3) ?
 H(31) .8027(6) .3107(6) -.1538(4) ?
 H(32) .6118(6) .3685(6) -.0924(4) ?
 H(41) .8835(10) .4111(9) .0 ?
 H(42) .9093(10) .1858(9) .0 ?