data_2000523
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1794
_journal_page_last  1798
loop_
_publ_author_name
 'Csoregh, I.'
_chemical_formula_moiety  'C15 H22 N2 O1,H1 Cl1'
_chemical_formula_sum  'C15 H23 Cl1 N2 O1'
_chemical_formula_weight  282.81
_symmetry_cell_setting  orthorhombic
_symmetry_space_group_name_H-M  'P 21 21 21'
_symmetry_space_group_name_Hall  ?
_cell_length_a  9.7768(4)
_cell_length_b  10.6279(3)
_cell_length_c  15.3157(4)
_cell_angle_alpha  90.
_cell_angle_beta  90.
_cell_angle_gamma  90.
_cell_volume  1591.40(10)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.18040(10)
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  608
_exptl_absorpt_coefficient_mu  1.98
_diffrn_radiation_type  Cu
_diffrn_radiation_wavelength  1.54183
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Cl -1.21551(9) -.51661(7) -.87094(6) .0538
 N(1) -.9024(3) -.2590(3) -.6978(2) .0410(10)
 C(1') -.8378(4) -.2575(5) -.7860(3) .062(2)
 C(2) -1.0484(3) -.3010(3) -.7039(2) .0420(10)
 C(3) -1.1103(4) -.3180(5) -.6140(3) .064(2)
 C(4) -1.0251(5) -.4041(4) -.5554(3) .068(2)
 C(5) -.8825(5) -.3495(4) -.5486(3) .058(2)
 C(6) -.8183(4) -.3392(4) -.6370(3) .0520(10)
 C(7) -1.1282(4) -.1985(3) -.7510(3) .0440(10)
 O(7) -1.1045(3) -.0869(2) -.7355(2) .0590(10)
 N(8) -1.2280(3) -.2396(3) -.8031(2) .0460(10)
 C(9) -1.3270(4) -.1578(3) -.8430(3) .0440(10)
 C(10) -1.4244(4) -.0996(4) -.7907(3) .0530(10)
 C(11) -1.5215(4) -.0241(4) -.8313(3) .061(2)
 C(12) -1.5212(4) -.0092(4) -.9212(3) .066(2)
 C(13) -1.4244(4) -.0670(4) -.9710(3) .060(2)
 C(14) -1.3240(4) -.1432(3) -.9335(3) .0480(10)
 C(15) -1.2158(5) -.2068(4) -.9876(3) .071(2)
 C(16) -1.4274(5) -.1172(5) -.6934(3) .073(2)
 H(1) -.8967 -.1672 -.6790 .10(2)
 H(1'a) -.8323 -.3442 -.8112 .120(10)
 H(1'b) -.7439 -.2203 -.7828 .120(10)
 H(1'c) -.8969 -.2037 -.8239 .120(10)
 H(2) -1.0522 -.3831 -.7356 .08(2)
 H3a) -1.1178 -.2337 -.5854 .050(10)
 H(3b) -1.2036 -.3554 -.6207 .10(2)
 H(4a) -1.0206 -.4903 -.5815 .06(2)
 H(4b) -1.0675 -.4090 -.4961 .13(3)
 H(5a) -.8251 -.4055 -.5110 .07(2)
 H(5b) -.8878 -.2639 -.5216 .07(2)
 H(6a) -.7255 -.3008 -.6308 .09(2)
 H(6b) -.8095 -.4254 -.6626 .060(10)
 H(8) -1.2224 -.3207 -.8168 .060(10)
 H(11) -1.5922 .0199 -.7954 .07(2)
 H(12) -1.5926 .0442 -.9497 .09(2)
 H(13) -1.4252 -.0545 -1.0357 .050(10)
 H(15a) -1.2253 -.1723 -1.0480 .120(10)
 H(15b) -1.2291 -.3000 -.9889 .120(10)