#------------------------------------------------------------------------------ #$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $ #$Revision: 14 $ #$URL: svn://www.crystallography.net/cod/cif/2/2000581.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_2000581 _journal_name_full 'Acta Cryst.' _journal_year 1992 _journal_volume C48 _journal_page_first 1569 _journal_page_last 1571 loop_ _publ_author_name 'Ichikawa, M.' 'Sato, S.' 'Komukae, M.' 'Osaka, T.' _chemical_formula_moiety 'H1,3K1,2(O4 Se1)' _chemical_formula_sum 'H1 K3 O8 Se2' _chemical_formula_weight 404.2 _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'A 1 1 2/a' _symmetry_space_group_name_Hall '-A 2a' _cell_length_a 10.1291(8) _cell_length_b 5.9038(5) _cell_length_c 14.9610(10) _cell_angle_alpha 90. _cell_angle_beta 103.640(8) _cell_angle_gamma 90. _cell_volume 869.50(10) _cell_formula_units_Z 4 _exptl_crystal_density_diffrn 3.086 _exptl_crystal_density_meas ? _exptl_crystal_F_000 760 _exptl_absorpt_coefficient_mu 9.86 _diffrn_radiation_type Mo _diffrn_radiation_wavelength 0.71073 loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z K(1) .25000 .75538(18) .0 K(2) .65190(7) .73701(13) .19654(5) Se .46014(3) .23210(5) .11609(2) O(1) .3988(3) .0129(4) .15747(16) O(2) .4348(2) .1814(4) .00184(14) O(3) .62361(19) .2498(5) .15443(15) O(4) .3826(3) .4641(4) .12910(17) H .50000 .0 .0