data_2000584
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1574
_journal_page_last  1576
loop_
_publ_author_name
 'John, E.'
 'Schugar, H.J.'
 'Potenza, J.A.'
_chemical_formula_moiety  'H15 Cl1 N5 Ru1,2(H1 O4 S1),4(H2 O1)'
_chemical_formula_sum  'H25 Cl1 N5 O12 Ru1 S2'
_chemical_formula_weight  487.88
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
_symmetry_space_group_name_Hall  ?
_cell_length_a  10.0422(5)
_cell_length_b  14.1044(7)
_cell_length_c  6.3273(6)
_cell_angle_alpha  100.369(5)
_cell_angle_beta  98.655(6)
_cell_angle_gamma  81.354(4)
_cell_volume  864.5(3)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.874
_exptl_crystal_density_meas  1.86
_exptl_crystal_F_000  498
_exptl_absorpt_coefficient_mu  1.33
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Ru .492360(10)
     .236420(10)
         .08119(2)
 Cl .42704(5) .16031(4) .34828(8)
 S(1) .74820(4) .50234(3) .26578(7)
 S(2) .09984(5) .84746(3) .25229(7)
 O(1) .7065(2) .44760(10)
         .4175(2)
 O(2) .7281(2) .60720(10)
         .3540(3)
 O(3) .6670(2) .48390(10)
         .0534(3)
 O(4) .8919(2) .47170(10)
         .2416(4)
 O(5) .0438(2) .79610(10)
         .3938(3)
 O(6) .2307(2) .8773(2) .3582(3)
 O(7) .0062(2) .93360(10)
         .2073(4)
 O(8) .1207(2) .7820(2) .0504(3)
 O(9) .7338(2) .98400(10)
         .2538(3)
 O(10) .0887(2) .59300(10)
       .2409(3)
 O(11) .1180(2) .3249(2) .2536(4)
 O(12) .0974(2) .1171(2) .2696(3)
 N(1) .6886(2) .23810(10)
         .2506(3)
 N(2) .5538(2) .30340(10)
         -.1517(3)
 N(3) .4350(2) .37640(10)
         .2477(3)
 N(4) .5560(2) .09870(10)
         -.0949(3)
 N(5) .2946(2) .23790(10)
         -.0897(3)
 H(N11) .746(2) .226(2) .167(4)
 H(N12) .707(2) .297(2) .313(4)
 H(N13) .694(2) .203(2) .350(4)
 H(N21) .591(2) .352(2) -.100(4)
 H(N22) .494(3) .325(2) -.237(4)
 H(N23) .609(2) .280(2) -.219(4)
 H(N31) .391(2) .418(2) .153(4)
 H(N32) .506(2) .402(2) .304(4)
 H(N33) .385(2) .384(2) .340(4)
 H(N41) .609(3) .096(2) -.196(4)
 H(N42) .504(2) .078(2) -.165(4)
 H(N43) .601(3) .062(2) -.010(4)
 H(N51) .227(3) .254(2) -.003(4)
 H(N52) .285(3) .274(2) -.177(4)
 H(N53) .284(3) .182(2) -.139(4)
 H(O101) .163(3) .577(2) .371(5)
 H(O91) .812(3) .978(2) .229(5)
 H(O121) .196(3) .136(2) .284(5)
 H(O102) .004(3) .555(2) .254(5)
 H(O111) .045(3) .349(2) .233(5)
 H(O122) .086(3) .051(2) .294(5)
 H(O92) .746(3) 1.024(2) .333(5)
 H(O112) .160(3) .342(2) .335(5)