data_2000591
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1590
_journal_page_last  1594
loop_
_publ_author_name
 'Kawata, T.'
 'Ohba, S.'
 'Tokii, T.'
 'Muto, Y.'
 'Kato, M.'
_chemical_formula_moiety  '2(C19 H13 Cl2 Cu1 N1 O4),2(C1 Cl4)'
_chemical_formula_sum  'C40 H26 Cl12 Cu2 N2 O8'
_chemical_formula_weight  1215.2
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 21/a'
_symmetry_space_group_name_Hall  ?
_cell_length_a  23.365(3)
_cell_length_b  10.6880(10)
_cell_length_c  20.542(2)
_cell_angle_alpha  90.
_cell_angle_beta  100.030(10)
_cell_angle_gamma  90.
_cell_volume  5051.5(9)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.60
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  2424
_exptl_absorpt_coefficient_mu  1.533
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Cu(1) .24066(4) .22499(9) .27069(5) .0341
 Cu(2) .26599(4) -.00077(9) .22672(5) .0342
 Cl(1) .39590(10)
       .0727(3) .44430(10)
          .0953
 Cl(2) .38640(10)
       .1404(3) .0906(2) .1044
 Cl(3) .11360(10)
       .1735(3) .05480(10)
          .0860
 Cl(4) .11700(10)
       .0375(3) .39750(10)
          .0900
 O(1) .3242(2) .2330(5) .3090(2) .0461
 O(2) .2597(2) .2842(5) .1859(2) .0495
 O(3) .1608(2) .1864(5) .2256(3) .0503
 O(4) .2274(2) .1229(4) .3478(2) .0424
 O(5) .3458(2) .0488(5) .2690(3) .0513
 O(6) .2761(2) .0922(5) .1478(2) .0485
 O(7) .1814(2) -.0069(5) .1920(2) .0456
 O(8) .2518(2) -.0630(5) .3120(2) .0490
 N(1) .2178(3) .4026(6) .3083(3) .0428
 N(2) .2910(3) -.1752(5) .1881(3) .0369
 C(1) .3588(3) .1465(7) .3003(3) .0403
 C(2) .4213(4) .1660(8) .3295(4) .0465
 C(3) .4433(4) .1302(8) .3950(4) .0562
 C(4) .5011(4) .1404(9) .4220(5) .0726
 C(5) .5382(4) .1860(10)
        .3846(5) .0887
 C(6) .5182(4) .2210(10)
        .3187(5) .0807
 C(7) .4601(3) .2099(9) .2909(4) .0693
 C(8) .2729(3) .2089(7) .1424(3) .0430
 C(9) .2843(3) .2690(8) .0798(3) .0405
 C(10) .3319(4) .2404(8) .0528(4) .0592
 C(11) .3422(4) .2970(10)
         -.0061(4) .0791
 C(12) .3011(5) .3780(10)
         -.0360(4) .0888
 C(13) .2550(5) .4103(9) -.0089(4) .0788
 C(14) .2439(4) .3567(8) .0483(4) .0627
 C(15) .1477(3) .0844(8) .1958(3) .0444
 C(16) .0856(3) .0722(8) .1658(4) .0447
 C(17) .0663(4) .1091(8) .1000(4) .0592
 C(18) .0079(4) .0992(9) .0701(4) .0700
 C(19) -.0304(4) .0460(10)
       .1068(5) .0841
 C(20) -.0125(4) .0080(10)
       .1719(5) .0941
 C(21) .0457(4) .0180(10)
         .1993(4) .0716
 C(22) .2354(3) .0093(7) .3537(3) .0349
 C(23) .2272(3) -.0528(7) .4173(3) .0399
 C(24) .1755(4) -.0476(7) .4404(4) .0479
 C(25) .1671(4) -.1135(8) .4972(4) .0630
 C(26) .2111(4) -.1814(9) .5309(4) .0643
 C(27) .2635(4) -.1878(9) .5100(4) .0676
 C(28) .2721(4) -.1278(8) .4520(4) .0532
 C(29) .2571(4) .4901(8) .3265(5) .0657
 C(30) .2421(4) .6036(9) .3543(5) .0927
 C(31) .1868(5) .6216(9) .3620(5) .0934
 C(32) .1468(4) .5330(10)
         .3434(6) .1039
 C(33) .1641(4) .4232(9) .3174(5) .0771
 C(34) .2615(3) -.2806(8) .1914(4) .0548
 C(35) .2762(4) -.3917(8) .1652(5) .0821
 C(36) .3223(4) -.3933(9) .1338(5) .0877
 C(37) .3537(4) -.2892(9) .1298(5) .0744
 C(38) .3366(3) -.1804(8) .1584(4) .0511
 Cl(5) .3970(2) -.2265(5) .3296(2) .1898
 Cl(6) .4225(2) -.3426(4) .4485(2) .2137
 Cl(7) .4412(2) -.4739(5) .3417(3) .2332
 Cl(8) .5105(2) -.2641(5) .3874(3) .2599
 Cl(9) .5931(2) -.2081(5) .1659(2) .1969
 Cl(10) .5013(2) -.1278(5) .0704(2) .2120
 Cl(11) .5022(2) -.0734(5) .2024(2) .2196
 Cl(12) .5796(3) .0425(6) .1370(3) .3564
 C(39) .4448(5) -.3290(10)
       .3730(5) .1102
 C(40) .5456(6) -.0860(10)
       .1426(5) .1378