data_2000594
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1603
_journal_page_last  1606
loop_
_publ_author_name
 'Marsh, R.E.'
 'Schaefer, W.P.'
 'Lyon, D.K.'
 'Labinger, J.A.'
 'Bercaw, J.E.'
_chemical_formula_sum  'C14 H32 Co1 O9 P3 Pt1'
_chemical_formula_weight  691.35
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
_symmetry_space_group_name_Hall  ?
_cell_length_a  9.106(3)
_cell_length_b  14.803(3)
_cell_length_c  15.147(3)
_cell_angle_alpha  112.95(2)
_cell_angle_beta  103.68(2)
_cell_angle_gamma  95.10(2)
_cell_volume  1788.9(9)
_cell_formula_units_Z  3
_exptl_crystal_density_diffrn  1.93
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  1014
_exptl_absorpt_coefficient_mu  6.869
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Pt1 .25110(4) .00830(2) .27640(3) .04800(10)
 Co1 .16460(10)
     .28600(10)
        .38350(10)
           .0461(2)
 P1 .1247(3) .1786(2) .4439(2) .0562(5)
 P2 .3894(3) .2538(2) .3770(2) .0637(6)
 P3 .0563(3) .1736(2) .2313(2) .0637(6)
 O1 .1582(7) .0757(4) .4009(4) .0660(15)
 O2 .4151(6) .1493(4) .3355(5) .0768(19)
 O3 .0893(7) .0700(4) .1966(4) .0757(19)
 C1 .3991(12) -.0443(7) .3551(8) .096(3)
 C2 .0988(11) -.1194(6) .2237(8) .085(3)
 C3 .3368(12) -.0498(7) .1599(8) .091(3)
 O4 -.0508(8) .1675(6) .4439(7) .125(3)
 O5 .2122(10) .2288(5) .5607(5) .112(3)
 O6 .5049(7) .3125(5) .4892(6) .117(3)
 O7 .4580(11) .3103(6) .3232(8) .152(3)
 O8 .0918(11) .2203(5) .1579(5) .125(3)
 O9 -.1258(8) .1631(5) .2068(6) .117(3)
 C1p .0007(14) .3730(8) .3829(18) .116(5)
 C2p .116(3)   .4061(11) .3524(10) .119(5)
 C3p .2464(17) .4364(8) .4272(19) .114(5)
 C4p .217(2)   .4224(9) .5059(10) .110(5)
 C5p .062(3)   .3823(10) .4782(17) .112(5)
 C4 -.1368(17) .0858(12) .4427(16) .198(7)
 C5 .2962(16) .1859(9) .6117(9) .130(5)
 C6 .6446(14) .2898(10) .5192(9) .124(5)
 C7 .518(2)   .2723(13) .2487(14) .176(6)
 C8 .0841(19) .1643(10) .0591(9) .146(6)
 C9 -.2308(16) .0774(11) .1611(14) .174(7)
 Pt2 .63920(10)
     .47940(10)
        -.11490(10)
         .0432(2)
 Co2 .4044(4) .5141(3) .0853(3) .0496(7)
 P4 .4576(5) .6252(3) .0315(3) .0500(10)
 P5 .3303(5) .3954(3) -.0666(4) .0628(12)
 P6 .6382(5) .4890(4) .1072(3) .0586(11)
 O10 .5174(12) .6014(7) -.0570(8) ?
 O11 .7285(12) .4954(8) .0383(8) ?
 O12 .4351(12) .3774(8) -.1325(8) ?
 O13 .5742(15) .7213(10) .1257(10) ?
 O14 .2668(16) .2880(11) -.0738(11) ?
 O15 .1678(16) .4155(11) -.1246(11) ?
 O16 .7445(18) .5615(11) .2199(11) ?
 O17 .6316(17) .3796(11) .1048(11) ?
 O18 .3124(16) .6774(10) .0094(11) ?
 C13 .6636(12) .7956(7) .1095(9) .096(3)
 C14 .8953(13) .6202(9) .2375(8) .116(4)
 C15 .7574(12) .3243(9) .0834(9) .105(3)
 C10 .5512 .4616 -.2574 ?
 C11 .8227 .5795 -.0964 ?
 C12 .7528 .3673 -.1623 ?
 C6p .4257 .5588 .2375 ?
 C7p .3485 .4587 .1833 ?
 C8p .2131 .4551 .1139 ?
 C9p .2066 .5530 .1253 ?
 C10p .3380 .6170 .2017 ?
 HCp1 -.1051 .3478 .3459 ?
 HCp2 .10380 .4068 .2888 ?
 HCp3 .3442 .4634 .4257 ?
 HCp4 .2922 .4382 .5680 ?
 HCp5 .0100 .3655 .5191 ?
 H1a .4921 .0048 .3916 ?
 H1b .3552 -.0584 .4000 ?
 H1c .4211 -.1036 .3102 ?
 H2a .0372 -.1134 .2671 ?
 H2b .0355 -.1325 .1586 ?
 H2c .1524 -.1722 .2197 ?
 H3a .2836 -.0349 .1068 ?
 H3b .4436 -.0207 .1805 ?
 H3c .3238 -.1200 .1380 ?
 H4a -.2363 .0984 .4444 ?
 H4b -.1401 .0291 .3866 ?
 H4c -.0872 .0792 .5030 ?
 H5a .3352 .2324 .6798 ?
 H5b .2323 .1285 .6053 ?
 H5c .3782 .1679 .5845 ?
 H6a .6937 .3341 .5872 ?
 H6b .6297 .2231 .5106 ?
 H6c .7060 .2988 .4788 ?
 H7a .5515 .3262 .2334 ?
 H7b .6057 .2486 .2725 ?
 H7c .4450 .2225 .1947 ?
 H8a .11097 .2079 .0309 ?
 H8b .1547 .1207 .0571 ?
 H8c -.0177 .1265 .0240 ?
 H9a -.3300 .0934 .1560 ?
 H9b -.2212 .0421 .0959 ?