#------------------------------------------------------------------------------
#$Date: 2008-11-20 19:58:43 +0000 (Thu, 20 Nov 2008) $
#$Revision: 481 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000610.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000610
_journal_name_full 'Acta Crystallographica Section C'
_journal_year  1992
_journal_volume 48
_journal_page_first  1657
_journal_page_last  1658
loop_
_publ_author_name
 'Lo, K.M.'
 'Ng. S.W.'
 'Wei, C.'
 'Kumar Das, V.G.'
_chemical_formula_sum  'C21 H19 N1 O3 Sn1'
_chemical_formula_weight  452.08
_symmetry_cell_setting  orthorhombic
_symmetry_space_group_name_H-M  'P 21 21 21'
_symmetry_space_group_name_Hall  ?
_cell_length_a  9.7484(7)
_cell_length_b  10.3086(6)
_cell_length_c  19.2656(8)
_cell_angle_alpha  90.
_cell_angle_beta  90.
_cell_angle_gamma  90.
_cell_volume  1936.0(2)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.551
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  904
_exptl_absorpt_coefficient_mu  1.341
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Sn .51399(5) .06664(5) .78956(3)
 O1 .5984(6) -.0926(5) .8511(3)
 O2 .5522(5) -.2481(5) .7748(3)
 O3 .8697(7) -.3398(7) .9403(4)
 N .7781(8) -.2506(7) .9151(4)
 C1 .3028(8) .0222(8) .8118(4)
 C2 .2139(9) .1313(9) .8185(5)
 C3 .0765(9) .1070(10)
      .8415(5)
 C4 .0340(9) -.0200(10)
       .8569(5)
 C5 .1240(10)
      -.1230(10)
      .8488(6)
 C6 .2592(9) -.1012(8) .8252(5)
 C7 .5926(8) .1979(8) .8654(4)
 C8 .7090(9) .2747(9) .8539(5)
 C9 .7550(10)
      .3570(10)
        .9071(6)
 C10 .6870(10)
    .3640(10)
      .9700(5)
 C11 .5700(10)
    .2880(10)
      .9813(5)
 C12 .5260(10)
    .2035(9) .9295(4)
 C13 .6480(8) .0255(7) .7045(5)
 C14 .6080(10)
    .0080(9) .6378(5)
 C15 .7060(10)
    -.0150(10)
       .5850(5)
 C16 .8460(10)
    -.0240(10)
       .6045(6)
 C17 .8850(10)
    -.0050(10)
       .6701(6)
 C18 .7883(9) .0190(10)
       .7205(5)
 C19 .6145(8) -.2068(7) .8274(4)
 C20 .7186(9) -.2909(8) .8611(5)
 C21 .9360(10)
    -.2940(10)
       1.0024(6)
 H1 .244435 .216604 .808002
 H2 .013926 .177180 .846501
 H3 -.056708 -.035764 .872904
 H4 .094057 -.208737 .859056
 H5 .319883 -.172279 .818742
 H6 .756082 .271136 .810767
 H7 .834042 .409125 .899776
 H8 .719062 .420321 1.005441
 H9 .521454 .293633 1.023890
 H10 .449528 .148825 .937954
 H11 .513295 .011052 .626277
 H12 .679189 -.023524 .537910
 H13 .912395 -.043991 .570242
 H14 .979964 -.007148 .681895
 H15 .816938 .030927 .767158
 H16 .739997 -.373626 .842328
 H17 .998716 -.357892 1.018482
 H18 .984344 -.216127 .992459
 H19 .869089 -.277830 1.037102