#------------------------------------------------------------------------------
#$Date: 2008-11-20 19:58:43 +0000 (Thu, 20 Nov 2008) $
#$Revision: 481 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000611.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000611
_journal_name_full 'Acta Crystallographica Section C'
_journal_year  1992
_journal_volume 48
_journal_page_first  1658
_journal_page_last  1660
loop_
_publ_author_name
 'Blake, A.J.'
 'Cockman, R.W.'
 'Ebsworth, E.A.V.'
_chemical_formula_sum  'C13 H30 Cl3 Ir1 O2 P2 S1'
_chemical_formula_weight  610.96
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 2 1/c'
_symmetry_space_group_name_Hall  ?
_cell_length_a  14.5752(17)
_cell_length_b  9.7304(8)
_cell_length_c  15.163(5)
_cell_angle_alpha  90.
_cell_angle_beta  97.454(15)
_cell_angle_gamma  90.
_cell_volume  2132
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.903
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  1192
_exptl_absorpt_coefficient_mu  7.09
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Ir .25888(2)   -.08396(4) .19221(2)   .0361(2)
 P(2) .16359(18) .0920(3) .24370(18) .0438(15)
 Cl(1) .35738(18) -.0608(3) .33320(18) .0515(16)
 Cl(2) .3433(2)   .0982(4) .1340(2)   .0648(19)
 P(1) .36319(19) -.2549(4) .1495(2)   .0545(18)
 S .1766(2)   -.0676(4) .05226(19) .0592(18)
 Cl(3) .0497(2)   -.1759(5) .0679(3)   .085(3)
 O(1) .2188(7) -.1410(11) -.0163(5) .078(6)
 C(2) .1859(7) -.2261(13) .2331(7) .046(6)
 O(2) .1477(6) -.3067(9) .2589(6) .063(6)
 C(111) .3076(9) -.4027(12) .0913(8) .059(7)
 C(112) .3641(9) -.5219(12) .0760(8) .062(8)
 C(121) .4326(11) -.334(2)   .2425(13) .135(16)
 C(122) .3755(16) -.412(2)   .3022(11) .126(16)
 C(131) .4327(14) -.173(2)   .0628(15) .065(14)
 C(132) .5196(16) -.251(3) .0512(17) .089(17)
 C(211) .2302(8) .2228(13) .3102(8) .061(8)
 C(212) .1753(10) .3368(14) .3458(9) .075(9)
 C(221) .0853(8) .1828(12) .1596(8) .056(7)
 C(222) .1335(9) .2889(13) .1054(9) .071(9)
 C(231) .0826(8) .0238(14) .3152(8) .058(7)
 C(232) .1250(9) -.0363(15) .4011(8) .068(8)
 C(133) .480(2)   -.220(4) .122(2)   .051(11)
 C(134) .476(3) -.191(5) .028(3) .061(12)
 H(1) .2758 -.3671 .0271 ?
 H(2) .2546 -.4378 .1296 ?
 H(3) .3209 -.5999 .0410 ?
 H(4) .3960 -.5623 .1389 ?
 H(5) .4172 -.4916 .0364 ?
 H(6) .4706 -.2547 .2815 ?
 H(7) .4806 -.4042 .2177 ?
 H(8) .4204 -.4576 .3568 ?
 H(9) .3376 -.4927 .2641 ?
 H(10) .3275 -.3432 .3279 ?
 H(11) .4160 -.0649 .0627 ?
 H(12) .3701 -.2320 .0461 ?
 H(13) .5692 -.2970 .0131 ?
 H(14) .4825 -.3303 .0813 ?
 H(15) .5555 -.1862 .1025 ?
 H(11A) .5103 -.1401 .1657 ?
 H(12A) .4509 -.2984 .1597 ?
 H(13A) .5013 -.1791 -.0360 ?
 H(14A) .4698 -.0905 .0569 ?
 H(15A) .4097 -.2406 .0184 ?
 H(16) .2773 .2689 .2694 ?
 H(17) .2691 .1722 .3664 ?
 H(18) .2219 .4075 .3838 ?
 H(19) .1283 .2940 .3879 ?
 H(20) .1365 .3907 .2909 ?
 H(21) .0346 .2363 .1927 ?
 H(22) .0509 .1079 .1142 ?
 H(23) .0826 .3380 .0575 ?
 H(24) .1840 .2372 .0711 ?
 H(25) .1676 .3656 .1496 ?
 H(26) .0420 -.0555 .2786 ?
 H(27) .0377 .1067 .3299 ?
 H(28) .0710 -.0730 .4376 ?
 H(29) .1652 .0413 .4397 ?
 H(30) .1695 -.1209 .3885 ?