#------------------------------------------------------------------------------
#$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $
#$Revision: 14 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000612.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000612
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1660
_journal_page_last  1661
loop_
_publ_author_name
 'Deshayes, L.'
 'Keller, N.'
 'Lance, M.'
 'Nierlich, M.'
 'Vigner, D.'
_chemical_formula_moiety  'C15 H35 N5 O7 U1,2(B1 F4)'
_chemical_formula_sum  'C15 H35 B2 F8 N5 O7 U1'
_chemical_formula_weight  809.11
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_cell_length_a  21.077(5)
_cell_length_b  13.296(3)
_cell_length_c  11.525(2)
_cell_angle_alpha  90.
_cell_angle_beta  112.24(2)
_cell_angle_gamma  90.
_cell_volume  2989.0(10)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.798
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  1560
_exptl_absorpt_coefficient_mu  5.234
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 U .000 .05533(3) .250
 F1 .3111(3) .1681(7) .3457(7)
 F2 .3768(4) .0437(5) .3439(7)
 F3 .4122(3) .1984(7) .3440(9)
 F4 .3313(4) .1365(8) .1808(6)
 O1 .0406(2) .0556(5) .1415(4)
 O2 .000 .2309(7) .250
 O3 .0647(3) -.0881(4) .3514(5)
 O4 -.1051(3) .1092(4) .0922(5)
 N2 .000 .3973(7) .250
 N3 .1022(3) -.2168(5) .4864(5)
 N4 -.1917(3) .0942(5) -.0962(6)
 C2 .0285(8) .3110(10)
      .3080(10)
 C3 .0540(4) -.1663(6) .4012(7)
 C4 -.1258(4) .0982(7) -.0248(8)
 C21 .0428(7) .455(2) .3500(10)
 C31 .0875(5) -.3113(7) .5378(9)
 C32 .1738(4) -.1822(8) .5340(10)
 C41 -.2100(5) .0820(10)
        -.2329(8)
 C42 -.2458(4) .1050(10)
        -.0480(10)
 B .3587(5) .1400(10)
        .3050(10)