#------------------------------------------------------------------------------
#$Date: 2008-01-26 13:05:32 +0000 (Sat, 26 Jan 2008) $
#$Revision: 19 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000613.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000613
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1661
_journal_page_last  1663
loop_
_publ_author_name
 'Litster, S.A.'
 'Redhouse, A.D.'
 'Simpson, S.J.'
_chemical_formula_sum  'C32 H32 P2 Ru1'
_chemical_formula_weight  579.6
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 21/n'
_symmetry_space_group_name_Hall  ?
_cell_length_a  9.188(2)
_cell_length_b  19.307(3)
_cell_length_c  15.545(3)
_cell_angle_alpha  90.
_cell_angle_beta  102.980(10)
_cell_angle_gamma  90.
_cell_volume  2687.0(8)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.43
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  1192
_exptl_absorpt_coefficient_mu  0.707
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.7107
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Ru(1) .12530(10)
       .13120(10)
       .29510(10)
          .0270(10)
 C(6) -.0512(6) .0038(3) .1097(3) .032(2)
 C(7) .0030(6) -.0277(3) .2023(3) .030(2)
 C(8) -.1319(5) .0723(2) .1085(3) .032(2)
 P(1) -.00990(10)
       .14310(10)
       .15860(10)
          .0270(10)
 C(11) -.1381(5) .2172(2) .1494(3) .031(2)
 C(12) -.2800(6) .2104(3) .1642(4) .048(2)
 C(13) -.3704(7) .2674(4) .1682(4) .062(3)
 C(14) -.3155(8) .3325(3) .1598(4) .060(3)
 C(15) -.1754(7) .3413(3) .1457(4) .050(2)
 C(16) -.0876(6) .2841(3) .1399(3) .041(2)
 C(21) .0896(5) .1598(2) .0703(3) .0250(10)
 C(22) .0184(6) .1824(2) -.0137(3) .030(2)
 C(23) .0968(6) .1908(2) -.0789(3) .037(2)
 C(24) .2483(7) .1773(3) -.0614(3) .041(2)
 C(25) .3209(6) .1549(3) .0212(4) .041(2)
 C(26) .2421(6) .1464(3) .0865(3) .034(2)
 P(2) .15900(10)
      .01820(10)
         .27490(10)
         .0260(10)
 C(31) .1888(5) -.0382(2) .3734(3) .028(2)
 C(32) .2329(6) -.1065(3) .3711(3) .042(2)
 C(33) .2498(7) -.1492(3) .4449(4) .051(2)
 C(34) .2224(7) -.1233(3) .5212(4) .055(2)
 C(35) .1787(8) -.0553(3) .5249(4) .061(3)
 C(36) .1639(7) -.0129(3) .4513(3) .047(2)
 C(41) .3195(5) -.0084(2) .2301(3) .028(2)
 C(42) .3110(6) -.0527(3) .1585(3) .036(2)
 C(43) .4367(6) -.0660(3) .1259(3) .045(2)
 C(44) .5724(6) -.0373(3) .1643(4) .043(2)
 C(45) .5833(6) .0053(3) .2357(4) .043(2)
 C(46) .4584(6) .0193(3) .2685(3) .034(2)
 C(1) .1804(8) .1907(3) .4228(4) .056(3)
 C(2) .1375(7) .2375(3) .3514(4) .053(2)
 C(3) .2436(7) .2325(3) .2997(4) .049(2)
 C(4) .3501(7) .1837(3) .3360(4) .048(2)
 C(5) .3111(7) .1570(3) .4130(3) .047(2)
 H(10) -.019(5)   .105(2)   .320(3)   ?
 H(6C) -.110(5)   -.031(2)   .073(3)   ?
 H(6D) .031(5)   .009(2)   .086(3)   ?
 H(7C) .034(5)   -.077(2)   .198(3)   ?
 H(7D) -.073(5)   -.027(2)   .233(3)   ?
 H(8C) -.211(5)   .068(2)   .144(3)   ?
 H(8D) -.182(5)   .087(2)   .049(3)   ?
 H(12A) -.322(6)   .171(3)   .172(3)   ?
 H(13A) -.467(6)   .258(3)   .179(4)   ?
 H(14A) -.370(6)   .373(3)   .164(2)   ?
 H(15B) -.140(6)   .383(3)   .136(3)   ?
 H(16B) .009(5)   .291(2)   .127(3)   ?
 H(22A) -.086(5)   .193(2)   -.028(3)   ?
 H(23A) .039(5)   .205(2)   -.138(3)   ?
 H(24A) .301(5)   .183(2)   -.102(3)   ?
 H(25A) .418(5)   .148(2)   .031(3)   ?
 H(26A) .285(5)   .138(3)   .133(3)   ?
 H(32A) .246(5)   -.123(2)   .317(3)   ?
 H(33B) .281(6)   -.193(3)   .444(3)   ?
 H(34A) .235(6)   -.149(3)   .568(3)   ?
 H(35A) .156(6)   -.036(3)   .572(3)   ?
 H(36A) .139(6)   .028(2)   .454(3)   ?
 H(42B) .211(5)   -.073(2)   .126(3)   ?
 H(43A) .425(5)   -.099(2)   .080(3)   ?
 H(44A) .645(6)   -.051(3)   .143(3)   ?
 H(45B) .665(5)   .028(3)   .262(3)   ?
 H(46A) .476(5)   .046(2)   .321(3)   ?
 H(1A) .127(7)   .180(3)   .457(4)   ?
 H(2A) .047(6)   .266(3)   .343(3)   ?
 H(3A) .242(6)   .259(3)   .249(3)   ?
 H(4A) .432(6)   .169(3)   .317(3)   ?
 H(5A) .360(6)   .123(2)   .448(3)   ?