data_2000615
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1663
_journal_page_last  1665
loop_
_publ_author_name
 'Florke, U.'
 'Ortmann, U.'
 'Haupt, H.-J.'
_chemical_formula_moiety  'C15 H24 Cl1 N2 Rh1,0.5(C4 H8 O2)'
_chemical_formula_sum  'C17 H28 Cl1 N2 O1 Rh1'
_chemical_formula_weight  414.8
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 1 21/c 1'
_symmetry_space_group_name_Hall  '-P 2ybc'
_cell_length_a  7.2310(10)
_cell_length_b  15.870(3)
_cell_length_c  15.918(3)
_cell_angle_alpha  90.
_cell_angle_beta  100.400(10)
_cell_angle_gamma  90.
_cell_volume  1796.7
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.533
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  856
_exptl_absorpt_coefficient_mu  1.09
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Rh(1) .21840(10)
       .16290(10)
       .12930(10)
          .0460(10)
 Cl(1) .3691(2) .20420(10)
       .26830(10)
          .0700(10)
 N(1) .0620(6) .0762(3) .1880(3) .062(3)
 N(2) .0163(6) -.0497(3) .2546(3) .061(2)
 C(1) -.0981(9) .1096(4) .2238(5) .092(5)
 C(2A) -.144(3)   .0759(9) .2921(12) .096(13)
 C(2B) -.2346(19) .0530(9) .2406(10) .071(9)
 C(3) -.1464(9) -.0210(4) .2912(4) .088(4)
 C(4) .1022(10) -.1315(4) .2697(4) .078(4)
 C(5) .2657(12) -.1299(4) .2276(5) .097(5)
 C(6) .2671(8) -.0470(3) .1837(4) .069(3)
 C(7) .1048(7) .0003(3) .2079(3) .051(3)
 C(8) .1488(8) .1065(4) .0081(3) .065(3)
 C(9) .0088(8) .1627(4) .0202(4) .070(4)
 C(10) -.0262(9) .2503(5) -.0137(5) .096(5)
 C(11) .1461(9) .3045(4) -.0007(4) .079(4)
 C(12) .2902(7) .2777(3) .0756(3) .055(3)
 C(13) .4308(7) .2198(3) .0731(3) .055(3)
 C(14) .4554(9) .1717(4) -.0061(4) .080(4)
 C(15) .2897(10) .1252(5) -.0486(4) .089(4)
 O(20) .3135(7) .5138(4) -.0372(4) .102(4)
 C(21) .4382(12) .4771(5) -.0824(4) .090(5)
 C(22) .4149(11) .5696(4) .0252(4) .085(5)
 H(1A) -.1712 .1443 .1807 .080
 H(1B) -.0446 .1461 .2699 .080
 H(3A) -.1072 -.0142 .3517 .080
 H(3B) -.2438 -.0629 .2815 .080
 H(4A) .0164 -.1751 .2461 .080
 H(4B) .1407 -.1411 .3298 .080
 H(5A) .2584 -.1750 .1869 .080
 H(5B) .3795 -.1365 .2687 .080
 H(6A) .2489 -.0543 .1229 .080
 H(6B) .3830 -.0175 .2026 .080
 H(8A) .1145 .0482 .0100 .080
 H(9A) -.1040 .1348 .0290 .080
 H(10A) -.1201 .2767 .0130 .080
 H(10B) -.0751 .2469 -.0738 .080
 H(11A) .1097 .3617 .0070 .080
 H(11B) .2017 .3025 -.0511 .080
 H(12A) .3243 .3217 .1169 .080
 H(13A) .5449 .2309 .1126 .080
 H(14A) .5564 .1323 .0097 .080
 H(14B) .4929 .2108 -.0459 .080
 H(15A) .2288 .1575 -.0966 .080
 H(15B) .3288 .0727 -.0698 .080
 H(21A) .4989 .5197 -.1105 .080
 H(21B) .3708 .4404 -.1253 .080
 H(22A) .3286 .5956 .0566 .080
 H(22B) .4748 .6131 -.0021 .080