#------------------------------------------------------------------------------
#$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $
#$Revision: 14 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000616.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000616
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1665
_journal_page_last  1666
loop_
_publ_author_name
 'Noltemeyer, M.'
 'Gilje, J.W.'
 'Roesky, H.W.'
_chemical_formula_moiety  'C16 H32 Cl1 O6 U1,C4 H8 Cl5 O1 U1'
_chemical_formula_sum  'C20 H40 Cl6 O7 U2'
_chemical_formula_weight  1081.3
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_cell_length_a  9.272(2)
_cell_length_b  13.031(3)
_cell_length_c  15.240(3)
_cell_angle_alpha  80.04(3)
_cell_angle_beta  79.15(3)
_cell_angle_gamma  73.46(3)
_cell_volume  1719.5(6)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  2.088
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  1004
_exptl_absorpt_coefficient_mu  9.422
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 U(1) .25510(10)
      .15960(10)
         .34300(10)
         .0660(10)
 Cl(1) -.0081(8) .1137(7) .3568(5) .114(4)
 O(1) .1158(16) .2211(13) .4817(11) .078(8)
 C(11) .022(4)   .327(3)   .4849(19) .14(2)
 C(12) -.078(4)   .331(3)   .568(2)   .13(2)
 C(13) -.045(5)   .228(4)   .620(2)   .20(3)
 C(14) .061(4)   .158(3)   .5606(19) .14(2)
 O(2) .4073(16) .2396(13) .4123(10) .078(8)
 C(21) .441(3)   .340(3)   .383(2)   .131(19)
 C(22) .533(5)   .354(4)   .444(3)   .18(3)
 C(23) .573(5)   .256(4)   .502(3)   .18(3)
 C(24) .465(4)   .197(3)   .4956(19) .14(2)
 O(3) .5029(18) .1468(13) .2511(11) .079(8)
 C(31) .647(3)   .076(3)   .275(2)   .130(18)
 C(32) .757(4)   .082(3)   .192(3)   .17(3)
 C(33) .668(6)   .148(4)   .126(3)   .21(4)
 C(34) .528(3)   .205(3)   .167(2)   .122(19)
 O(4) .2690(17) .0776(17) .2083(11) .083(8)
 C(41) .318(3)   -.032(3)   .205(2)   .118(18)
 C(42) .279(5)   -.056(3)   .125(3)   .17(3)
 C(43) .206(4)   .044(3)   .0778(19) .12(2)
 C(44) .178(4)   .125(2)   .1378(19) .118(17)
 O(5) .3334(17) .0367(12) .4014(10) .085(8)
 O(6) .1927(16) .2838(12) .2842(9) .079(7)
 U(2) .70980(10)
      .61620(10)
         .19820(10)
         .0800(10)
 Cl(2) .6423(10) .6906(8) .0392(5) .151(5)
 Cl(3) .7429(12) .4213(7) .1693(7) .156(6)
 Cl(4) .8034(10) .5464(8) .3523(5) .137(5)
 Cl(5) .7259(11) .8052(7) .2175(8) .164(6)
 Cl(6) .4308(8) .6468(8) .2693(5) .137(5)
 O(7) .9696(19) .5936(16) .1312(12) .104(9)
 C(71) 1.039(4)   .665(3)   .074(3)   .17(2)
 C(72) 1.202(4)   .633(4)   .084(3)   .16(3)
 C(73) 1.222(4)   .525(3)   .132(4)   .18(3)
 C(74) 1.083(4)   .500(3)   .144(3)   .17(2)