data_2000620
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1673
_journal_page_last  1675
loop_
_publ_author_name
 'Ishida, H.'
 'Kashino, S.'
_chemical_formula_moiety  '2(C4 H12 N1),Cl6 Te1'
_chemical_formula_sum  'C8 H24 Cl6 N2 Te1'
_chemical_formula_weight  488.6
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 1 21/a 1'
_symmetry_space_group_name_Hall  '-P 2yab'
_cell_length_a  12.620(3)
_cell_length_b  15.719(5)
_cell_length_c  9.945(2)
_cell_angle_alpha  90.
_cell_angle_beta  90.14(2)
_cell_angle_gamma  90.
_cell_volume  1973.0(9)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.645
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  960
_exptl_absorpt_coefficient_mu  2.318
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Te .22715(5) .12633(4) .15023(5)
 Cl(1) .0696(2) .1188(2) -.0228(2)
 Cl(2) .2941(2) .26400(10)
       .0301(2)
 Cl(3) .3503(2) .0298(2) -.0057(2)
 Cl(4) .1565(3) -.0056(2) .2469(2)
 Cl(5) .3644(3) .1361(2) .3207(3)
 Cl(6) .1116(3) .2109(2) .2894(3)
 N(1) .3639(6) .4368(4) .1828(6)
 N(2) .5431(5) .1693(4) -.1023(6)
 C(1) .3284(8) .4512(5) .3292(8)
 C(2) .3880(10)
     .3887(7) .4170(10)
 C(3) .3500(10)
     .5427(6) .3640(10)
 C(4) .2066(8) .4318(8) .3320(10)
 C(5) .5393(7) .1749(6) -.2576(8)
 C(6) .5280(10)
     .0842(6) -.3140(10)
 C(7) .6452(8) .2145(6) -.3030(10)
 C(8) .4412(9) .2292(8) -.2920(10)