data_2000696
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1488
_journal_page_last  1489
loop_
_publ_author_name
 'Cho, I.'
 'Yeo, H.'
 'Whang, D.'
 'Kim, K.'
_chemical_formula_sum  'C12 H17 Cl1 N2 O1 Pd1'
_chemical_formula_weight  347.135
_symmetry_cell_setting  orthorhombic
_symmetry_space_group_name_H-M  'P bca'
_symmetry_space_group_name_Hall  ?
_cell_length_a  10.7640(10)
_cell_length_b  12.557(4)
_cell_length_c  19.626(2)
_cell_angle_alpha  90.
_cell_angle_beta  90.
_cell_angle_gamma  90.
_cell_volume  2652.8(9)
_cell_formula_units_Z  8
_exptl_crystal_density_diffrn  1.737
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  1392
_exptl_absorpt_coefficient_mu  1.569
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.7093
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Pd .28741(5) .18608(5) .09834(3)
 Cl .1011(2) .1615(2) .15700(10)
 O1 .2237(6) .0654(5) .0425(3)
 N1 .3360(7) .3060(6) .1680(4)
 N2 .4423(6) .1974(6) .0392(3)
 C1 .2330(10)
      .3886(8) .1726(5)
 C2 .3510(10)
      .2549(9) .2368(5)
 C3 .4525(9) .3669(8) .1524(6)
 C4 .5575(8) .2966(8) .1308(5)
 C5 .5519(8) .2641(8) .0561(5)
 C6 .4527(8) .1487(8) -.0171(4)
 C7 .3688(8) .0758(7) -.0494(4)
 C8 .3983(9) .0400(8) -.1158(5)
 C9 .3250(10)
      -.0309(8) -.1510(5)
 C10 .2170(10)
    -.0682(8) -.1181(5)
 C11 .1862(9) -.0367(7) -.0527(5)
 C12 .2595(8) .0379(6) -.0170(4)
 H1 .157 .354 .182
 H2 .252 .438 .208
 H3 .227 .425 .130
 H4 .278 .216 .248
 H5 .420 .208 .236
 H6 .364 .308 .270
 H7 .477 .405 .192
 H8 .436 .416 .117
 H9 .556 .234 .158
 H10 .634 .333 .138
 H11 .549 .327 .029
 H12 .625 .225 .046
 H13 .527 .163 -.042
 H14 .472 .066 -.137
 H15 .346 -.054 -.196
 H16 .164 -.116 -.141
 H17 .114 -.066 -.032