#------------------------------------------------------------------------------
#$Date: 2008-11-20 19:58:43 +0000 (Thu, 20 Nov 2008) $
#$Revision: 481 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000697.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000697
_journal_name_full 'Acta Crystallographica Section C'
_journal_year  1992
_journal_volume 48
_journal_page_first  1490
_journal_page_last  1491
loop_
_publ_author_name
 'Kane, C.J.'
 'Long, R.'
 'Pettit, W.E.'
 'Breneman, G.L.'
_chemical_formula_moiety  'C8 H20 Cl10 N2 Sn1'
_chemical_formula_sum  'C8 H20 Cl10 N2 Sn1'
_chemical_formula_weight  617.48
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'C 2/c'
_symmetry_space_group_name_Hall  ?
_cell_length_a  15.67(2)
_cell_length_b  13.54(2)
_cell_length_c  13.24(2)
_cell_angle_alpha  90.
_cell_angle_beta  127.9(2)
_cell_angle_gamma  90.
_cell_volume  2217
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.85
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  1208
_exptl_absorpt_coefficient_mu  2.370
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Sn .000 .08420(10)
      .250
 Cl(1) .1881(2) .0848(3) .3273(2)
 Cl(2) .0446(2) .2148(3) .4040(3)
 Cl(3) .0478(2) -.0419(3) .4082(3)
 Cl(4) .0901(2) .5303(3) .1992(4)
 Cl(5) .1423(3) .3324(4) .0044(3)
 N .2852(6) .3819(9) .2967(9)
 C(2) .2030(8) .3610(10)
        .3180(10)
 C(3) .3150(9) .2940(10)
        .2550(10)
 C(4) .1660(9) .4540(10)
        .3410(10)
 C(5) .2174(9) .2450(10)
        .1310(10)
 H(1) .3483 .4097 .3719
 H(2) .2545 .4318 .2293
 H(3) .2340 .3179 .3916
 H(4) .1407 .3270 .2460
 H(5) .3500 .2458 .3227
 H(6) .3663 .3127 .2406
 H(7) .1245 .4407 .3676
 H(8) .2302 .4902 .4068
 H(9) .2430 .1923 .1059
 H(10) .1723 .2152 .1485