data_2000716
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1533
_journal_page_last  1535
loop_
_publ_author_name
 'Belanger-Gariepy, F.'
 'Bennani, Y.'
 'Beaudoin, S.'
 'Hanessian, S.'
_chemical_formula_moiety  'C25 H41 N2 O2 P1'
_chemical_formula_sum  'C25 H41 N2 O2 P1'
_chemical_formula_weight  432.59
_symmetry_cell_setting  orthorhombic
_symmetry_space_group_name_H-M  'P 21 21 21'
_symmetry_space_group_name_Hall  ?
_cell_length_a  10.636(2)
_cell_length_b  12.7590(10)
_cell_length_c  18.185(2)
_cell_angle_alpha  90.
_cell_angle_beta  90.
_cell_angle_gamma  90.
_cell_volume  2467.8(5)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.164
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  944
_exptl_absorpt_coefficient_mu  1.138
_diffrn_radiation_type  Cu
_diffrn_radiation_wavelength  1.54178
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 P .56485(11) .12040(9) .47265(6) .042
 O(1) .4516(3) .1871(2) .4795(2) .052
 O(2) .7098(2) .3181(2) .46380(10)
         .043
 N(1) .5350(3) -.0074(2) .4646(2) .044
 N(2) .6584(3) .1056(3) .5450(2) .042
 C(1) .6286(4) -.0682(3) .5037(2) .048
 C(2) .5960(4) -.1798(3) .5258(3) .063
 C(3) .7107(5) -.2254(4) .5661(3) .081
 C(4) .7529(5) -.1571(4) .6299(3) .081
 C(5) .7751(5) -.0422(4) .6086(2) .066
 C(6) .6575(4) -.0033(3) .5706(2) .049
 C(7) .4704(5) -.0513(4) .4017(3) .075
 C(8) .6674(4) .1865(4) .6015(2) .059
 C(9) .6588(4) .1611(3) .3925(2) .039
 C(10) .6882(4) .2810(3) .3904(2) .039
 C(11) .8017(4) .3055(3) .3415(2) .042
 C(12) .8273(4) .4240(3) .3360(2) .044
 C(13) .7144(4) .4866(3) .3095(2) .044
 C(14) .5997(4) .4594(3) .3564(2) .053
 C(15) .5748(4) .3419(3) .3610(2) .051
 C(16) .7407(4) .6070(3) .3053(2) .048
 C(17) .8630(5) .6280(4) .2618(3) .080
 C(18) .7555(6) .6539(4) .3811(3) .073
 C(19) .6319(5) .6625(4) .2662(3) .089
 C(20) .7704(4) .0886(3) .3822(2) .039
 C(21) .8735(4) .0889(3) .4278(2) .047
 C(22) .9725(4) .0184(4) .4177(3) .062
 C(23) .9692(5) -.0523(4) .3611(3) .074
 C(24) .8676(5) -.0533(4) .3150(3) .074
 C(25) .7687(5) .0164(3) .3244(2) .052
 H(O2) .781(3) .316(2) .476(2) ?
 H(1) .705(3) -.074(2) .4750(10)
          ?
 H(2A) .516(3) -.176(3) .558(2) ?
 H(2B) .570(4) -.220(3) .487(2) ?
 H(3A) .693(3) -.298(3) .583(2) ?
 H(3B) .778(3) -.233(3) .531(2) ?
 H(4A) .683(4) -.156(3) .667(2) ?
 H(4B) .827(3) -.187(3) .652(2) ?
 H(5A) .791(3) .005(3) .656(2) ?
 H(5B) .848(3) -.036(3) .572(2) ?
 H(6) .588(3) -.014(2) .6050(10)
          ?
 H(7A) .527(4) -.079(4) .360(2) ?
 H(7B) .426(4) -.106(3) .415(2) ?
 H(7C) .399(4) .004(3) .384(2) ?
 H(8A) .642(4) .266(3) .575(2) ?
 H(8B) .755(4) .202(3) .618(2) ?
 H(8C) .611(4) .175(3) .642(2) ?
 H(9) .593(3) .143(2) .349(2) ?
 H(11A) .881(3) .270(3) .360(2) ?
 H(11B) .789(3) .277(2) .295(2) ?
 H(12A) .852(3) .445(3) .382(2) ?
 H(12B) .899(3) .429(2) .302(2) ?
 H(13) .696(3) .457(3) .258(2) ?
 H(14A) .632(4) .487(3) .408(2) ?
 H(14B) .515(4) .490(3) .337(2) ?
 H(15A) .565(3) .315(3) .315(2) ?
 H(15B) .506(3) .328(3) .393(2) ?
 H(17A) .852(5) .593(4) .213(2) ?
 H(17B) .941(6) .603(4) .287(3) ?
 H(17C) .865(4) .707(3) .250(2) ?
 H(18A) .821(4) .620(3) .412(2) ?
 H(18B) .665(6) .649(4) .410(3) ?
 H(18C) .774(4) .726(3) .373(2) ?
 H(19A) .641(5) .630(4) .215(3) ?
 H(19B) .554(3) .658(3) .295(2) ?
 H(19C) .651(4) .745(3) .266(2) ?
 H(21) .885(3) .142(3) .468(2) ?
 H(22) 1.048(4) .023(3) .453(2) ?
 H(23) 1.033(3) -.111(3) .356(2) ?
 H(24) .859(4) -.109(3) .279(2) ?
 H(25) .693(3) .024(2) .291(2) ?