#------------------------------------------------------------------------------ #$Date: 2020-03-17 11:34:05 +0000 (Tue, 17 Mar 2020) $ #$Revision: 249446 $ #$URL: svn://www.crystallography.net/cod/cif/2/00/07/2000736.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2000736 loop_ _publ_author_name 'Le Lay, L.' 'Powell, D. R.' 'Willis, T. C.' _publ_section_title ; Structure of Sn~0.854~Mo~6~S~8~ ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1179 _journal_page_last 1182 _journal_paper_doi 10.1107/S0108270191014609 _journal_volume 48 _journal_year 1992 _chemical_formula_sum 'Mo6 S8 Sn0.854' _chemical_formula_weight 933.5 _symmetry_cell_setting trigonal _symmetry_space_group_name_Hall '-P 3*' _symmetry_space_group_name_H-M 'R -3' _cell_angle_alpha 89.47(2) _cell_angle_beta 89.47(2) _cell_angle_gamma 89.47(2) _cell_formula_units_Z 1 _cell_length_a 6.5100(10) _cell_length_b 6.5100(10) _cell_length_c 6.5100(10) _cell_volume 275.86(7) _diffrn_radiation_type Mo _diffrn_radiation_wavelength 0.71073 _exptl_absorpt_coefficient_mu 9.777 _exptl_crystal_density_diffrn 5.619 _exptl_crystal_F_000 422.70 _cod_data_source_file cr0368.cif _cod_data_source_block cr0368a _cod_depositor_comments ; The unit cell information in this entry had apparently incorrect unit cell information: _symmetry_space_group_name_H-M 'R -3 {rhombohedral axes}' _symmetry_space_group_name_Hall '-P 3*' _cell_length_a 6.5100(10) _cell_length_b ? _cell_length_c ? _cell_angle_alpha 89.47(2) _cell_angle_beta 90 _cell_angle_gamma 90 The unit cell length and angle was corrected based on assumption of the rombohedral unit cell. Saulius Gra\