#------------------------------------------------------------------------------
#$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $
#$Revision: 14 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000740.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000740
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1202
_journal_page_last  1204
loop_
_publ_author_name
 'Taqui Khan, M.M.'
 'Bhadbhade, M.M.'
 'Venkatasubramanian, K.'
 'Siddiqui, M.R.H.'
_chemical_formula_moiety  'C10 H14 Cl2 N2 O8 Ru1,K1'
_chemical_formula_sum  'C10 H14 Cl2 K1 N2 O8 Ru1'
_chemical_formula_weight  501
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 1 21/n 1'
_symmetry_space_group_name_Hall  '-P 2yn'
_cell_length_a  10.4470(6)
_cell_length_b  13.947(2)
_cell_length_c  11.296(3)
_cell_angle_alpha  90.
_cell_angle_beta  106.100(10)
_cell_angle_gamma  90.
_cell_volume  1581.0(10)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  2.097
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  996
_exptl_absorpt_coefficient_mu  1.613
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 Ru1 .218890(10)
      .742410(10)
       .061010(10)
 K .88269(5) .64591(4) .12544(5)
 Cl21 .11669(5) .58970(3) .00566(5)
 Cl22 .01141(4) .81916(4) .00626(4)
 O13 .4696(3) 1.0595(2) .1613(4)
 O15 .2036(2) .8062(3) .4032(2)
 O16 .2068(2) .7288(2) .23580(10)
 O17 .3290(2) .68340(10)
        -.24430(10)
 O18 .24350(10)
     .75800(10)
        -.11020(10)
 O19 .6532(2) .56550(10)
        .1644(2)
 O20 .5494(2) .47680(10)
        .2761(2)
 O141 .2872(3) 1.1138(2) .0224(3)
 O142 .2611(7) 1.0868(5) .1313(7)
 N1 .32190(10)
    .86780(10)
       .13880(10)
 N4 .41200(10)
    .68410(10)
       .08790(10)
 C2 .4639(2) .83780(10)
       .1955(2)
 C3 .5056(2) .76700(10)
       .1123(2)
 C5 .3075(2) .94450(10)
       .0451(2)
 C6 .3616(2) 1.0417(2) .0960(3)
 C7 .2600(2) .8954(2) .2395(2)
 C8 .2219(2) .8061(3) .2996(2)
 C9 .4098(2) .63830(10)
       -.03160(10)
 C10 .3221(2) .69650(10)
        -.13750(10)
 C11 .4384(2) .61390(10)
        .1901(2)
 C12 .5606(2) .55140(10)
        .2080(2)
 H21 .467 .812 .279
 H22 .512 .896 .195
 H31 .500 .791 .029
 H32 .590 .750 .141
 H51 .213 .957 .000
 H52 .357 .918 .000
 H71 .180 .937 .195
 H72 .312 .937 .279
 H91 .379 .584 -.027
 H92 .490 .625 -.055
 H111 .367 .582 .195
 H112 .445 .646 .250
 H141 .299 1.188 .027
 H142 .277 1.146 .166
 H201 .609 .437 .277