data_2000741
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1204
_journal_page_last  1207
loop_
_publ_author_name
 'Barris, G.C.'
 'Mackay, K.M.'
 'Nicholson, B.K.'
_chemical_formula_moiety  'C29 H20 Cl2 Co7 N1 O21 Si1'
_chemical_formula_sum  'C29 H20 Cl2 Co7 N1 O21 Si1'
_chemical_formula_weight  1230
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 21/c'
_symmetry_space_group_name_Hall  ?
_cell_length_a  9.110(4)
_cell_length_b  22.472(9)
_cell_length_c  21.010(10)
_cell_angle_alpha  90.
_cell_angle_beta  95.28(4)
_cell_angle_gamma  90.
_cell_volume  4283(3)
_cell_formula_units_Z  4
_exptl_crystal_density_diffrn  1.91
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  2424
_exptl_absorpt_coefficient_mu  2.9
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.7107
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Co(1) .3405(2) .60320(10)
       .39490(10)
          .016
 Co(2) .1140(2) .53890(10)
       .39580(10)
          .018
 Co(3) .0855(2) .64700(10)
       .37860(10)
          .020
 Co(4) .1719(2) .58470(10)
       .29430(10)
          .016
 Co(5) -.1189(2) .73590(10)
        .09550(10)
           .023
 Co(6) -.3149(2) .65930(10)
        .09240(10)
           .020
 Co(7) -.0915(2) .64280(10)
        .03460(10)
           .024
 Si(1) -.0160(5) .5747(2) .2208(2) .019
 Cl(1) -.2277(4) .5613(2) .2489(2) .024
 Cl(2) -.0006(4) .5059(2) .1542(2) .028
 O(1) -.0370(10)
      .6351(4) .1751(5) .019(3)
 O(11) .4260(10)
      .6142(5) .5325(6) .041(3)
 O(12) .5330(10)
      .5078(5) .3539(5) .028(3)
 O(13) .4810(10)
      .7106(5) .3504(6) .034(3)
 O(21) .2830(10)
      .4621(5) .4873(6) .036(3)
 O(22) -.1650(10)
       .4736(5) .3893(6) .038(3)
 O(23) .0380(10)
      .6074(5) .5073(6) .036(3)
 O(24) .2000(10)
      .4545(4) .2986(5) .025(3)
 O(31) .1810(10)
      .7550(5) .4445(6) .036(3)
 O(32) -.225(2) .6774(6) .3448(7) .059(4)
 O(34) .1690(10)
      .7123(5) .2640(5) .029(3)
 O(41) .3740(10)
      .5723(5) .1966(6) .036(3)
 O(51) -.2630(10)
       .8207(5) -.0004(6) .050(4)
 O(52) -.1730(10)
       .7854(5) .2201(6) .049(4)
 O(53) .1950(10)
      .7657(5) .1007(6) .043(3)
 O(61) -.5020(10)
       .7160(3) -.0135(7) .050(4)
 O(62) -.4280(10)
       .5377(5) .0883(6) .041(3)
 O(63) -.4530(10)
       .6957(5) .2072(6) .040(3)
 O(71) -.1560(10)
       .7037(6) -.0902(7) .058(4)
 O(72) -.1710(10)
       .5213(5) -.0034(6) .041(3)
 O(73) .2270(10)
      .6239(5) .0568(6) .046(3)
 C(1) -.114(2) .6542(7) .1227(8) .021(4)
 C(11) .390(2) .6104(7) .4793(8) .022(4)
 C(12) .460(2) .5454(7) .3708(7) .018(4)
 C(13) .427(2) .6687(7) .3675(8) .021(4)
 C(21) .217(2) .4932(7) .4497(9) .029(4)
 C(22) -.055(2) .5007(7) .3916(8) .029(4)
 C(23) .065(2) .6018(7) .4531(8) .020(4)
 C(24) .175(2) .5031(7) .3165(7) .017(4)
 C(31) .141(2) .7130(7) .4188(7) .018(4)
 C(32) -.102(2) .6631(8) .3606(9) .037(5)
 C(34) .152(2) .6686(7) .2936(8) .020(4)
 C(41) .295(2) .5781(7) .2344(8) .025(4)
 C(51) -.204(2) .7884(8) .0382(9) .033(5)
 C(52) -.151(2) .7679(7) .1696(8) .020(4)
 C(53) .072(2) .7551(7) .0975(8) .033(5)
 C(61) -.430(2) .6933(8) .0279(9) .038(5)
 C(62) -.384(2) .5841(8) .0911(8) .028(4)
 C(63) -.399(2) .6820(7) .1627(9) .029(4)
 C(71) -.133(2) .6789(7) -.0417(9) .0294(4)
 C(72) -.139(2) .5694(8) .0122(9) .032(5)
 C(73) .100(2) .6320(7) .0461(9) .037(5)
 N(1) .3950(10)
     .8772(5) .2859(6) .021(3)
 C(81) .509(2) .9266(6) .2981(8) .023(4)
 C(82) .653(2) .9069(8) .3332(9) .042(5)
 C(83) .364(2) .8476(8) .3494(8) .036(5)
 C(84) .308(2) .8897(8) .3968(9) .46(5)
 C(85) .257(2) .9057(7) .2547(8) .034(5)
 C(86) .127(2) .8661(8) .2394(9) .042(5)
 C(87) .450(2) .8285(6) .2443(7) .021(4)
 C(88) .481(2) .8500(8) .1791(8) .040(5)
 H(811) .462(2) .9608(6) .3260(8) ?
 H(812) .533(2) .9447(6) .2525(8) ?
 H(821) .689(2) .9526(8) .3321(9) ?
 H(822) .735(2) .8784(8) .3153(9) ?
 H(823) .637(2) .8945(8) .3817(9) ?
 H(831) .466(2) .8281(8) .3707(8) ?
 H(832) .283(2) .8131(8) .3393(8) ?
 H(841) .274(2) .8690(8) .4394(9) ?
 H(842) .212(2) .9038(8) .3667(9) ?
 H(843) .376(2) .9279(8) .4099(9) ?
 H(851) .284(2) .9255(7) .2104(8) ?
 H(852) .225(2) .9402(7) .2864(8) ?
 H(861) .041(2) .8971(8) .2228(9) ?
 H(862) .098(2) .8447(8) .2825(9) ?
 H(863) .139(2) .8329(8) .2030(9) ?
 H(871) .367(2) .7941(6) .2385(7) ?
 H(872) .550(2) .8101(6) .2679(7) ?
 H(881) .494(2) .8076(8) .1561(8) ?
 H(882) .577(2) .8773(8) .1737(8) ?
 H(883) .384(2) .8722(8) .1573(8) ?