#------------------------------------------------------------------------------
#$Date: 2008-01-13 22:15:36 +0000 (Sun, 13 Jan 2008) $
#$Revision: 14 $
#$URL: svn://www.crystallography.net/cod/cif/2/2000744.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000744
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1211
_journal_page_last  1214
loop_
_publ_author_name
 'Chen, X.-M.'
 'Mak, T.C.W.'
_chemical_formula_moiety  'C10 H30 Co1 N2 O8,2(Cl),4(H2 O1)'
_chemical_formula_sum  'C10 H38 Cl2 Co1 N2 O12'
_chemical_formula_weight  508.33
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'P 21/a'
_symmetry_space_group_name_Hall  ?
_cell_length_a  8.530(2)
_cell_length_b  11.9280(10)
_cell_length_c  12.118(3)
_cell_angle_alpha  90.
_cell_angle_beta  103.67(2)
_cell_angle_gamma  90.
_cell_volume  1204.9(2)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.401
_exptl_crystal_density_meas  1.405
_exptl_crystal_F_000  538
_exptl_absorpt_coefficient_mu  0.99
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Co(1) .0 .0 .0 .0277(2)
 Cl(1) .11640(10)
       -.13760(10)
        .36760(10)
           .0562(3)
 O(1w) .0682(2) .1465(2) .0929(2) .0400(10)
 O(2w) .1587(3) -.0983(2) .1209(2) .0380(10)
 O(3w) .1906(3) .1185(2) .3190(2) .0610(10)
 O(4w) .4164(3) -.2481(2) .5285(2) .0760(10)
 O(1) .1815(2) .0185(2) -.0890(2) .0380(10)
 O(2) .2349(3) .2007(2) -.0651(2) .0570(10)
 C(1) .2431(3) .1084(2) -.1114(2) .0360(10)
 C(2) .3351(4) .1106(2) -.2043(3) .0440(10)
 N(1) .3714(3) .0013(2) -.2557(2) .0380(10)
 C(3) .4785(4) -.0699(3) -.1674(3) .0580(10)
 C(4) .4598(5) .0289(3) -.3471(3) .0580(10)
 C(5) .2217(4) -.0621(3) -.3092(3) .0590(10)
 H(1wA) .1195 .1405 .1762 ?
 H(1wB) .1213 .1891 .0538 ?
 H(2wA) .1945 -.1705 .0973 ?
 H(2wB) .1314 -.1113 .1958 ?
 H(3wA) .1678 .0437 .3452 ?
 H(3wB) .0945 .1612 .3223 ?
 H(4wA) .3137 -.2186 .4829 ?
 H(4wB) .4830 -.2765 .4924 ?
 H(2A) .4375 .1515 -.1784 ?
 H(2B) .2881 .1540 -.2617 ?
 H(3A) .5980 -.0331 -.1309 ?
 H(3B) .4270 -.0849 -.0993 ?
 H(3C) .5196 -.1294 -.2045 ?
 H(4A) .4879 -.0503 -.3819 ?
 H(4B) .5495 .0694 -.2951 ?
 H(4C) .3889 .0753 -.3989 ?
 H(5A) .1707 -.0834 -.2558 ?
 H(5B) .2353 -.1167 -.3422 ?
 H(5C) .1581 -.0031 -.3586 ?