data_2000749
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1221
_journal_page_last  1223
loop_
_publ_author_name
 'Spirlet, M.R.'
 'Rebizant, J.'
 'Bettonville, S.'
 'Goffart, J.'
_chemical_formula_sum  'C45 H57 Cl1 U1'
_chemical_formula_weight  871.44
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
_symmetry_space_group_name_Hall  ?
_cell_length_a  10.081(4)
_cell_length_b  13.339(4)
_cell_length_c  15.083(3)
_cell_angle_alpha  85.24(4)
_cell_angle_beta  82.673(5)
_cell_angle_gamma  67.37(4)
_cell_volume  1856.0(10)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.560
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  872
_exptl_absorpt_coefficient_mu  4.2491
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
 U .12116(2) .23678(2) .222140(10)
 Cl -.1256(2) .21090(10)
        .23480(10)
 C(1) -.0265(7) .3629(5) .0715(5)
 C(2) -.0435(6) .4283(5) .1422(5)
 C(3) .0942(7) .4280(5) .1547(5)
 C(4) .3416(7) .3550(5) .0595(5)
 C(5) .4124(7) .2998(5) -.0189(5)
 C(6) .3356(7) .2627(5) -.0733(5)
 C(7) .1922(8) .2773(5) -.0511(5)
 C(8) .1188(7) .3282(5) .0327(5)
 C(9) .1941(6) .3680(4) .0845(4)
 C(1') -.1568(8) .3491(7) .0363(6)
 C(2') -.1865(8) .4930(6) .1933(6)
 C(4') .4085(7) .4114(6) .1121(5)
 C(5') .5683(8) .2844(6) -.0483(6)
 C(6') .4160(10)
      .2147(6) -.1611(6)
 C(7') .1048(9) .2531(6) -.1178(6)
 C(10) .1941(6) .0020(5) .2102(5)
 C(11) .2070(7) .0519(5) .1265(5)
 C(12) .3221(6) .0900(5) .1197(4)
 C(13) .5183(6) .0591(5) .2255(5)
 C(14) .5709(6) .0059(5) .3027(5)
 C(15) .4973(7) -.0546(5) .3580(5)
 C(16) .3694(7) -.0592(5) .3363(5)
 C(17) .3094(7) .0004(5) .2577(5)
 C(18) .3876(6) .0570(4) .2015(4)
 C(10') .0881(7) -.0533(5) .2364(6)
 C(11') .1207(8) .0537(6) .0502(5)
 C(13') .6020(7) .1109(5) .1583(5)
 C(14') .7128(7) .0044(6) .3301(6)
 C(15') .5701(9) -.1250(6) .4376(6)
 C(16') .3081(8) -.1360(5) .3871(6)
 C(19) -.0283(7) .3222(5) .3967(5)
 C(20) .0735(7) .2168(5) .4063(5)
 C(21) .2158(7) .2163(5) .3801(4)
 C(22) .3058(7) .3740(5) .3467(5)
 C(23) .2604(8) .4858(5) .3405(5)
 C(24) .1097(9) .5510(5) .3536(5)
 C(25) .0037(8) .5104(5) .3723(5)
 C(26) .0482(7) .3937(5) .3743(4)
 C(27) .1984(6) .3268(5) .3623(4)
 C(19') -.1901(8) .3518(7) .4219(6)
 C(20') .0412(8) .1188(6) .4441(5)
 C(22') .4664(7) .2997(6) .3469(6)
 C(23') .3741(9) .5385(6) .3245(6)
 C(24') .0630(10)
       .6792(6) .3479(7)
 C(25') -.1516(9) .5825(6) .4001(6)
 H3 .1093 .4785 .1875
 H12 .3593 .1250 .0625
 H21 .3320 .1445 .3750
 H1 -.2500 .3964 .0625
 H1' -.1093 .3320 -.0253
 H1" -.1982 .2970 .0525
 H2 -.2500 .4589 .2304
 H2' -.2773 .5429 .1464
 H2" -.1933 .5429 .2304
 H4 .4726 .3750 .1464
 H4' .3320 .4570 .1660
 H4" .4160 .4785 .0820
 H5 .6113 .2089 -.0625
 H5' .5839 .3339 -.0820
 H5" .6113 .3125 .0000
 H6 .3886 .1660 -.1679
 H6' .4160 .2695 -.2089
 H6" .5185 .1822 -.1621
 H7 .1933 .1875 -.1464
 H7' .0820 .1875 -.1054
 H7" .0292 .3339 -.1445
 H10 .1386 -.1250 .2285
 H10' .0546 -.0429 .2910
 H10" .0000 -.0195 .1875
 H11 .1660 .0820 .0000
 H11' .0273 .1035 .0625
 H11" .1181 -.0150 .0408
 H13 .5839 .1250 .1054
 H13' .6113 .1679 .1875
 H13" .6916 .0530 .1433
 H14 .6933 -.0253 .3964
 H14' .7226 .0625 .2929
 H14" .7792 -.0625 .3125
 H15 .6113 -.0820 .4804
 H15' .5273 -.1679 .4785
 H15" .6406 -.1875 .4179
 H16 .3886 -.2089 .3750
 H16' .3046 -.1250 .4570
 H16" .1933 -.1054 .3750
 H19 -.2207 .3964 .4804
 H19' -.2500 .3964 .3750
 H19" -.2207 .2929 .4179
 H20 -.0273 .1054 .4179
 H20' .0000 .1250 .5000
 H20" .1358 .0646 .4350
 H22 .5292 .3125 .2929
 H22' .5000 .3125 .3964
 H22" .4715 .2271 .3461
 H23 .3593 .5820 .2695
 H23' .3593 .5820 .3750
 H23" .4707 .5000 .2910
 H24 .1093 .7070 .3945
 H24' -.0392 .7120 .3591
 H24" .0925 .70002 .2894
 H25 -.1933 .6464 .3554
 H25' -.1660 .6250 .4589
 H25" -.2207 .5429 .3964